1、Designation: D841 12D841 13Standard Specification forNitration Grade Toluene1This standard is issued under the fixed designation D841; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parenthes
2、es indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope*1.1 This specification covers nitration grade toluene.1.2 The following applies to all specified limits in this standard: for purposes of determining conform
3、ance with this standard,an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressingthe specification limit, in accordance with the rounding-off method of Practice E29.1.3 Consult OSHA regulations, suppliers Material Safety Data S
4、heets, and local regulations for all materials used in thisspecification.2. Referenced Documents2.1 ASTM Standards:2D848 Test Method for Acid Wash Color of Industrial Aromatic HydrocarbonsD849 Test Method for Copper Strip Corrosion by Industrial Aromatic HydrocarbonsD850 Test Method for Distillation
5、 of Industrial Aromatic Hydrocarbons and Related MaterialsD1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)D2360 Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas ChromatographyD3437 Practice for Sampling and Handling Liquid Cyclic ProductsD5386 Test Meth
6、od for Color of Liquids Using Tristimulus ColorimetryD7504 Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography and Effective CarbonNumberE29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications2.2 Federal Specification
7、:3PPP-C-2020 Packaging of Chemicals, Liquid, Dry, and Paste2.3 Other Document:OSHA Regulations, 29 CFR paragraphs 1910.1000 and 1910.1200 41 This specification is under the jurisdiction ofASTM Committee D16 on Aromatic Hydrocarbons and Related Chemicals and is the direct responsibility of Subcommitt
8、eeD16.01 on Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives.Current edition approved Nov. 1, 2012Feb. 1, 2013. Published December 2012February 2013. Originally approved in 1945. Last previous edition approved in 20112012as D841 11.D841 12. DOI: 10.1520/D0841-12.10.1520/D0841-13.2 For re
9、ferencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvolume information, refer to the standards Document Summary page on the ASTM website.3 Available from Standardization Documents Order Desk, DODSSP, Bldg.
10、4, Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:/www.dodssp.daps.mil.4 Available from U.S. Government Printing Office Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http:/www.access.gpo.gov.This document is not an ASTM standard and is int
11、ended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Becauseit may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the curr
12、ent versionof the standard as published by ASTM is to be considered the official document.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States13. Properties3.1 Nitration Grad
13、e Toluene shall conform to the following requirements:Property Specification ASTM TestMethodANonaromatic hydrocarbons, max, volume %(wt %)1.5 (1.2) D2360 orD7504Nonaromatic hydrocarbons, max, volume %(wt %)1.5 (1.2) D2360,D7504Purity, min. wt% 98.8 D2360 orD7504Acid wash color, max pass with 2 D848C
14、opper corrosion pass (1A or 1B) D849Appearance B .Color, Pt/Co scale, max 20 D1209 orD5386Color, Pt/Co scale, max 20D5386Distillation range including the temperature110.6C at 101.3 kPa (760 mm Hg pressure),max, C 1.0 D850A If more than one method is listed for a property the producer and user should
15、 agree on the reference method.B Clear liquid free of sediment and haze when observed at 18.3 to 25.6C (65 to 78F).3.2 See Section 6 for non-mandatory supplementary requirements.4. Sampling4.1 The material shall be sampled in accordance with Practice D3437.5. Packaging and Labeling for U.S. Governme
16、nt Procurements5.1 United States Government procurements shall be packaged and labeled in accordance with the applicable paragraphs of Fed.Spec. PPP-C-2020.6. Supplementary Requirements (Non-mandatory)6.1 The following supplementary requirements shall apply only when specified by the purchaser in th
17、e purchase order orcontract:Property ASTM Test Method1,4-dioxane, max, mg/kg D75047. Keywords7.1 tolueneSUMMARY OF CHANGESCommittee D16 has identified the location of selected changes to this standard since the last issue (D841 11)12) that may impact the use of this standard. (Approved NovemberFebru
18、ary 1, 2012.)2013.)(1) Modified Table 3.1 to eliminate non-mandatory requirements.Added 3.2 and Section 6 to indicate non-mandatory items.AddedTest Method D7504 to table in 3.1.(2) Moved 1,4 dioxane to non-mandatory section.(3) Deleted reference to Test Method D1209.(4) Removed Test Method D850 Dist
19、illation requirement.Committee D16 has identified the location of selected changes to this standard since the last issue(D841 10D841) 11) that may impact the use of this standard. (Approved JulyNovember 1, 2011.)2012.)(1) Added 1,4-dioxane and Test Method D7504 to Table in 3.1. Modified Table 3.1 to
20、 eliminate non-mandatory requirements.Added 3.2 and Section 6 to indicate non-mandatory items.D841 132ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that de
21、termination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved
22、or withdrawn.Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel th
23、at your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints
24、 (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).D841 133
