1、Designation: D975 13aD975 14Standard Specification forDiesel Fuel Oils1This standard is issued under the fixed designation D975; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses ind
2、icates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope*1.1 This specification covers seven grades of diesel fuel oils suitable for v
3、arious types of diesel engines. These grades aredescribed as follows:1.1.1 Grade No. 1-D S15A special-purpose, light middle distillate fuel for use in diesel engine applications requiring a fuelwith 15 ppm sulfur (maximum) and higher volatility than that provided by Grade No. 2-D S15 fuel.21.1.2 Gra
4、de No. 1-D S500A special-purpose, light middle distillate fuel for use in diesel engine applications requiring a fuelwith 500 ppm sulfur (maximum) and higher volatility than that provided by Grade No. 2-D S500 fuel.21.1.3 Grade No. 1-D S5000Aspecial-purpose, light middle distillate fuel for use in d
5、iesel engine applications requiring a fuelwith 5000 ppm sulfur (maximum) and higher volatility than that provided by Grade No. 2-D S5000 fuels.1.1.4 Grade No. 2-D S15A general purpose, middle distillate fuel for use in diesel engine applications requiring a fuel with15 ppm sulfur (maximum). It is es
6、pecially suitable for use in applications with conditions of varying speed and load.21.1.5 Grade No. 2-D S500A general-purpose, middle distillate fuel for use in diesel engine applications requiring a fuel with500 ppm sulfur (maximum). It is especially suitable for use in applications with condition
7、s of varying speed and load.21.1.6 Grade No. 2-D S5000Ageneral-purpose, middle distillate fuel for use in diesel engine applications requiring a fuel with5000 ppm sulfur (maximum), especially in conditions of varying speed and load.1.1.7 Grade No. 4-DA heavy distillate fuel, or a blend of distillate
8、 and residual oil, for use in low- and medium-speed dieselengines in applications involving predominantly constant speed and load.NOTE 1A more detailed description of the grades of diesel fuel oils is given in X1.2.NOTE 2The Sxxx designation has been adopted to distinguish grades by sulfur rather th
9、an using words such as “Low Sulfur” as previously becausethe number of sulfur grades is growing and the word descriptions were thought to be not precise. S5000 grades correspond to the so-called “regular” sulfurgrades, the previous No. 1-D and No. 2-D. S500 grades correspond to the previous “Low Sul
10、fur” grades. S15 grades were not in the previous grade systemand are commonly referred to as “Ultra-Low Sulfur” grades or ULSD.1.2 This specification, unless otherwise provided by agreement between the purchaser and the supplier, prescribes the requiredproperties of diesel fuels at the time and plac
11、e of delivery.1.2.1 Nothing in this specification shall preclude observance of federal, state, or local regulations which can be more restrictive.NOTE 3The generation and dissipation of static electricity can create problems in the handling of distillate diesel fuel oils. For more information onthe
12、subject, see Guide D4865.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.2. Referenced Documents2.1 ASTM Standards:3D56 Test Method for Flash Point by Tag Closed Cup TesterD86 Test Method for Distillation of Petroleum Prod
13、ucts at Atmospheric PressureD93 Test Methods for Flash Point by Pensky-Martens Closed Cup TesterD129 Test Method for Sulfur in Petroleum Products (General High Pressure Decomposition Device Method)1 This specification is under the jurisdiction ofASTM Committee D02 on Petroleum Products, Liquid Fuels
14、, and Lubricants and is the direct responsibility of SubcommitteeD02.E0 on Burner, Diesel, Non-Aviation Gas Turbine, and Marine Fuels.Current edition approved Dec. 1, 2013Feb. 1, 2014. Published December 2013February 2014. Originally approved in 1948. Last previous edition approved in 2013 asD975 13
15、.D975 13a. DOI: 10.1520/D0975-13A.10.1520/D0975-14.2 This fuel complies with 40 CFR Part 80Control of Air Pollution from New Motor Vehicles: HeavyDuty Engines and Vehicle Standards and Highway Diesel FuelSulfur Control Requirements: Final Rule. Regulation of Fuels and FuelAdditives: Fuel Quality Reg
16、ulations for Highway Diesel Fuel Sold in 1993 and Later Calendar Years.3 For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvolume information, refer to the standards Document Summary page on the AST
17、M website.This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Becauseit may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult
18、 prior editions as appropriate. In all cases only the current versionof the standard as published by ASTM is to be considered the official document.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA
19、 19428-2959. United States1D130 Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip TestD445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)D482 Test Method for Ash from Petroleum ProductsD524 Test Method for Ra
20、msbottom Carbon Residue of Petroleum ProductsD613 Test Method for Cetane Number of Diesel Fuel OilD1266 Test Method for Sulfur in Petroleum Products (Lamp Method)D1319 Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator AdsorptionD1552 Test Method for Sulfur in Pe
21、troleum Products (High-Temperature Method)D1796 Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)D2274 Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)D2500 Test Method for Cloud Point of Petroleum ProductsD2622 Test Method
22、 for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence SpectrometryD2624 Test Methods for Electrical Conductivity of Aviation and Distillate FuelsD2709 Test Method for Water and Sediment in Middle Distillate Fuels by CentrifugeD2880 Specification for Gas Turbine Fuel OilsD2887
23、 Test Method for Boiling Range Distribution of Petroleum Fractions by Gas ChromatographyD3117 Test Method for Wax Appearance Point of Distillate Fuels (Withdrawn 2010)4D3120 Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative MicrocoulometryD3828 Test Metho
24、ds for Flash Point by Small Scale Closed Cup TesterD4057 Practice for Manual Sampling of Petroleum and Petroleum ProductsD4177 Practice for Automatic Sampling of Petroleum and Petroleum ProductsD4294 Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence S
25、pectrometryD4306 Practice for Aviation Fuel Sample Containers for Tests Affected by Trace ContaminationD4308 Test Method for Electrical Conductivity of Liquid Hydrocarbons by Precision MeterD4539 Test Method for Filterability of Diesel Fuels by Low-Temperature Flow Test (LTFT)D4737 Test Method for C
26、alculated Cetane Index by Four Variable EquationD4865 Guide for Generation and Dissipation of Static Electricity in Petroleum Fuel SystemsD5304 Test Method for Assessing Middle Distillate Fuel Storage Stability by Oxygen OverpressureD5453 Test Method for Determination of Total Sulfur in Light Hydroc
27、arbons, Spark Ignition Engine Fuel, Diesel Engine Fuel,and Engine Oil by Ultraviolet FluorescenceD5771 Test Method for Cloud Point of Petroleum Products (Optical Detection Stepped Cooling Method)D5772 Test Method for Cloud Point of Petroleum Products (Linear Cooling Rate Method)D5773 Test Method for
28、 Cloud Point of Petroleum Products (Constant Cooling Rate Method)D5842 Practice for Sampling and Handling of Fuels for Volatility MeasurementD5854 Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum ProductsD6078 Test Method for Evaluating Lubricity of Diesel Fuels by the S
29、cuffing Load Ball-on-Cylinder Lubricity Evaluator(SLBOCLE)D6079 Test Method for Evaluating Lubricity of Diesel Fuels by the High-Frequency Reciprocating Rig (HFRR)D6217 Test Method for Particulate Contamination in Middle Distillate Fuels by Laboratory FiltrationD6371 Test Method for Cold Filter Plug
30、ging Point of Diesel and Heating FuelsD6468 Test Method for High Temperature Stability of Middle Distillate FuelsD6469 Guide for Microbial Contamination in Fuels and Fuel SystemsD6751 Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate FuelsD6890 Test Method for Determination o
31、f Ignition Delay and Derived Cetane Number (DCN) of Diesel Fuel Oils by Combustionin a Constant Volume ChamberD6898 Test Method for Evaluating Diesel Fuel Lubricity by an Injection Pump RigD7039 Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gas
32、oline-EthanolBlends by Monochromatic Wavelength Dispersive X-ray Fluorescence SpectrometryD7042 Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of KinematicViscosity)D7094 Test Method for Flash Point by Modified Continuously Closed Cup (MCCCFP) T
33、esterD7170 Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel OilsFixed Range Injection Period,Constant Volume Combustion Chamber MethodD7345 Test Method for Distillation of Petroleum Products at Atmospheric Pressure (Micro Distillation Method)D7371 Test Method for Determina
34、tion of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid InfraredSpectroscopy (FTIR-ATR-PLS Method)4 The last approved version of this historical standard is referenced on www.astm.org.D975 142D7467 Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)D7619 Test Met
35、hod for Sizing and Counting Particles in Light and Middle Distillate Fuels, by Automatic Particle CounterD7688 Test Method for Evaluating Lubricity of Diesel Fuels by the High-Frequency Reciprocating Rig (HFRR) by VisualObservationD7220 Test Method for Sulfur inAutomotive, Heating, and Jet Fuels by
36、Monochromatic Energy Dispersive X-ray FluorescenceSpectrometryE29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications2.2 Other Documents:26 CFR Part 48 Manufacturers and Realtors Excise Taxes540 CFR Part 80 Regulation of Fuels and Fuel Additives5API RP 200
37、3 Protection Against Ignitions Arising Out of Static, Lightning, and Stray Currents6EN 14078 Liquid petroleum products - Determination of fatty acid methyl esters (FAME) in middle distillates - Infraredspectroscopy method73. Terminology3.1 Definitions:3.1.1 biodiesel, nfuel comprised of mono-alkyl e
38、sters of long chain fatty acids derived from vegetable oils or animal fats,designated B100.3.1.2 biodiesel blend (BXX), nblend of biodiesel fuel with diesel fuel oils.3.1.2.1 DiscussionIn the abbreviation, BXX, the XX represents the volume percentage of biodiesel fuel in the blend.3.1.3 switch loadi
39、ng, nof liquid fuels, the practice of loading low vapor pressure product (for example, diesel fuel) into anempty or near-empty fixed or portable container that previously held a high or intermediate vapor pressure product (such asgasoline or solvent) without prior compartment cleaning treatment and
40、inert gas purging; and the reverse procedure where a highvapor pressure product is added to a container that previously held a low vapor pressure product.3.1.3.1 DiscussionSince middle distillate fuels have flash points above 38C, during normal distribution of these fuels, the atmosphere above the f
41、uelsin a container such as a tanker truck, rail car, or barge, is normally below the lower explosive limit, so there is low risk of fire orexplosion should an electrostatic discharge (spark) occur. However, when the previous load in the compartment was a volatile,flammable fuel such as gasoline, and
42、 if some residual fuel vapor or mist remains in the compartment, and the container has amixture of air and fuel vapor or mist (that is, not purged with an inert gas), then there is a risk that the atmosphere in the containerbeing filled could be in the explosive range creating a hazard should an ele
43、ctrostatic discharge occur.3.2 Definitions of Terms Specific to This Standard:3.2.1 hydrocarbon oil, nhomogeneous mixture or solution with elemental composition primarily of carbon and hydrogen andalso containing sulfur, oxygen or nitrogen from residual impurities and contaminants and excluding adde
44、d oxygenated materials.(See Note 5.)3.2.1.1 DiscussionNeither macro nor micro emulsions are included in this definition since neither are homogeneous mixtures or solutions.3.2.1.2 DiscussionExamples of excluded oxygenated materials are alcohols, esters, ethers and triglycerides.3.2.2 S(numerical spe
45、cification maximum)indicates the maximum sulfur content, in weight ppm (g/g), allowed by thisspecification in a diesel fuel grade.3.2.2.1 Discussion5 Available from U.S. Government Printing Office, Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401.6 Available
46、from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http:/www.ansi.org.7 Available from the National CEN members listed on the CEN website (www.cenorm.be) or from the CEN/TC 19 Secretariat (astm.nen.nl).D975 143Of the seven diesel fuel grades specified i
47、n this standard, six have important distinguishing maximum sulfur regulatoryrequirements. These are Grades No. 1-D S15, No. 1-D S500, No. 1-D S5000, No. 2-D S15, No. 2-D S500 and No. 2-D S5000.The seventh grade, No. 4-D, is distinguished from these other grades by many major properties in addition t
48、o sulfur (unregulatedmaximum), and therefore is not included in this designation system. Thus, Grade No. 4-D does not have the designation S20000as part of its grade name.4. Sampling, Containers, and Sample Handling4.1 It is strongly advised to review all test methods prior to sampling to understand
49、 the importance and effects of samplingtechnique, proper containers, and special handling required for each test method.4.2 Correct sampling procedures are critical to obtaining a representative sample of the diesel fuel oil to be tested. Refer toAppendix X2 for recommendations. The recommended procedures or practices provide techniques useful in the proper samplingor handling of diesel fuels.5. Test Methods5.1 The requirements enumerated in this specification shall be determined in accordance with the following methods:5.1.1 Flash PointTest Methods
