1、Designation: D 5162 01Standard Practice forDiscontinuity (Holiday) Testing of Nonconductive ProtectiveCoating on Metallic Substrates1This standard is issued under the fixed designation D 5162; the number immediately following the designation indicates the year oforiginal adoption or, in the case of
2、revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice covers procedures for determining discon-tinuities using two types of test equipm
3、ent:1.1.1 Test Method ALow Voltage Wet Sponge, and1.1.2 Test Method BHigh Voltage Spark Testers.1.2 This practice addresses metallic substrates. For concretesurfaces, refer to Practice D 4787.21.3 The values stated in inch-pound units are to be regardedas the standard. The values given in parenthese
4、s immediatelyfollowing inch-pound units are for information only.1.4 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the appl
5、ica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:D 4787 Practice for Continuity Verification of Liquid orSheet Linings Applied to Concrete Substrates2G 62 Test Methods for Holiday Detection in Pipeline Coat-ings23. Terminology3.1 Definitions of Terms Specif
6、ic to This Standard:3.1.1 discontinuity, as used in this standard a void, crack,thin spot, foreign inclusion, or contamination in the coatingfilm that significantly lowers the dielectric strength of thecoating film. May also be identified as a holiday or pinhole.3.1.2 holiday, as used in this standa
7、rda term that identi-fies a discontinuity.3.1.3 holiday detector, as used in this standard a devicethat locates discontinuities in a nonconductive coating filmapplied to a conductive surface.3.1.4 pinhole, as used in this standarda film defectcharacterized by small porelike flaws in the coating whic
8、h,when extended entirely through the film, will appear as adiscontinuity. A pinhole in the finish coat may not appear as adiscontinuity.4. Significance and Use4.1 A coating is applied to a metallic substrate to preventcorrosion, reduce abrasion or reduce product contamination, orboth. The degree of
9、coating continuity required is dictated byservice conditions. Discontinuities in a coating are frequentlyvery minute and not readily visible. This practice provides aprocedure for electrical detection of minute discontinuities innonconductive coating systems.4.2 Electrical testing to determine the p
10、resence and numberof discontinuities in a coating film is performed on a noncon-ductive coating applied to a conductive surface. The allowablenumber of discontinuities should be determined prior toconducting this test since the acceptable quantity of disconti-nuities will vary depending on coating f
11、ilm thickness, design,and service conditions.4.3 The low voltage wet sponge test equipment is generallyused for determining the existence of discontinuities in coatingfilms having a total thickness of 20 mils (0.5 mm) or less. Highvoltage spark test equipment is generally used for determiningthe exi
12、stences of discontinuities in coating films having a totalthickness of greater than 20 mils (0.5 mm).4.4 Coatings that are applied at a thickness of less than 20mils (0.5 mm) may be susceptible to damage if tested with highvoltage spark testing equipment. Consult the coating manufac-turer for proper
13、 test equipment and inspection voltages.4.5 To prevent damage to a coating film when using highvoltage test instrumentation, total film thickness and dielectricstrength in a coating system shall be considered in selecting theappropriate voltage for detection of discontinuities. Atmo-spheric conditio
14、ns shall also be considered since the voltagerequired for the spark to gap a given distance in air varies withthe conductivity of the air at the time the test is conducted.Suggested starting voltages are provided in Table 1.1This practice is under the jurisdiction of ASTM Committee D33 on Protective
15、Coating and Lining Work for Power Generation Facilities and is the directresponsibility of Subcommittee D33.04 on Quality Systems and Inspection.Current edition approved June 10, 2001. Published August 2001. Originallypublished as D 5162 91. Last previous edition D 5162 00.2Annual Book of ASTM Stand
16、ards, Vol 06.02.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.4.6 The coating manufacturer shall be consulted to obtainthe following information, which would affect the accuracy ofthis test to determine discontinuities:4.6.1 Establ
17、ish the length of time required to adequately dryor cure the applied coating film prior to testing. Solventsretained in an uncured coating film may form an electricallyconductive path through the film to the substrate.4.6.2 Determine whether the coating contains electricallyconductive fillers or pig
18、ments that may affect the normaldielectric properties.4.7 This practice is intended for use with new liningsapplied to metal substrates. Its use on a lining previouslyexposed to an immersion condition has often resulted indamage to the lining and has produced erroneous detection ofdiscontinuities du
19、e to permeation or moisture absorption of thelining. Deposits may also be present on the surface causingtelegraphing. The use of a high voltage tester on a previouslyexposed lining has to be carefully considered because ofpossible spark through which will damage an otherwise soundlining. Although a
20、low voltage tester can be used withoutdamaging the lining, it may also produce erroneous results.5. Test MethodsTEST METHOD ALOW VOLTAGE WET SPONGETESTING5.1 Apparatus5.1.1 Low Voltage Holiday Detectoran electronic devicepowered by a self-contained battery with voltages ranging from5 to 90 V dc, dep
21、ending on the equipment manufacturerscircuit design. It is used to locate discontinuities in a noncon-ductive coating applied to a conductive substrate. Operationincludes the use of an open-cell sponge electrode wetted witha solution for exploring the coating surface, a ground connec-tion, and an au
22、dible or visual indicator, or both, for signaling apoint of coating discontinuity.5.1.2 Low Voltage Wet Sponge Tester a sensitivity devicewith the operating voltage being of little importance other thanbeing part of the particular electronic circuit design.5.1.3 Wet Sponge Type Instrumentsa number o
23、f commer-cially available, industry-accepted, instruments are available.The following electronic principle describes two types ofdevices generally used; others may be available but are notdescribed in this practice.5.1.3.1 Lightweight, Self-Contained, Portable Devicesbased on the electrical principl
24、e of an electromagnetic sensitiverelay or a solid-state electronic relay circuit that energizes anaudible or visual indicator when a coating discontinuity isdetected. Generally this equipment is capable of being recali-brated in the field by the user.5.1.3.2 Lightweight, Self-Contained, Portable Dev
25、icesalso based on the principle of an electronic relaxation oscillatorcircuit that reacts significantly to the abrupt drop in electricalresistance between the high dielectric value of the coating filmand the conductive substrate at the point of coating filmdiscontinuity. This results in a rise in os
26、cillator frequency aswell as in the audible signal from the device. Generally, thisequipment is incapable of being recalibrated in the field by theuser.5.2 Procedure5.2.1 Sufficient drying or curing of the coating shall beallowed prior to conducting a test. The length of time requiredshall be obtain
27、ed from the coating manufacturer. Solventsretained in the coating film could produce erroneous indicators.5.2.2 The surface shall be clean, dry, and free of oil, dirt andother contaminates. Measure the film thickness of the coatingwith a nondestructive dry film thickness gage. If the coatingfilm exc
28、eeds 20 mils (0.5 mm), use the procedures for highvoltage spark testing described in Test Method B, High VoltageSpark Testing.5.2.3 Test the instrument for sensitivity in accordance with5.3.5.2.4 Attach the ground wire from the instrument groundoutput terminal to the metallic substrate and ensure po
29、sitiveelectrical contact.5.2.5 Attach the exploring sponge lead to the other outputterminal.5.2.6 Wet the sponge with a solution consisting of tap waterand a low sudsing wetting agent, combined at a ratio of notmore than12 fluid oz of wetting agent to 1 gal water. Anexample of a low sudsing wetting
30、agent is one used inphotographic development. The sponge shall be wetted suffi-ciently to barely avoid dripping of the solution while thesponge is moved over the coating. The wetting agent residuemust be removed prior to executing repairs.5.2.7 Sodium chloride (salt) shall not be added to thewetting
31、 solution because of the potential erroneous indicationsof discontinuities. The salt, after drying on the coated surface,may form a continuous path of conductivity. It will alsointerfere with intercoat adhesion of additional coats.5.2.8 Contact a bare spot on the conductive substrate withthe wetted
32、sponge to verify that the instrument is properlygrounded. This procedure shall be repeated periodically duringthe test.5.2.9 Move the sponge over the surface of the coating at amoderate rate approximately 1 ft/s (0.3 m/s), using a doublepass over each area.Apply sufficient pressure to maintain a wet
33、surface. If a discontinuity is detected, turn the sponge on end todetermine the exact location of the discontinuity.5.2.10 Discontinuities that require repair shall be identifiedwith a marker that is compatible with the repair coating or onethat is easily removed.TABLE 1 Suggested Voltages for High
34、Voltage Spark TestingTotal Dry Film ThicknessSuggested Inspection, Vmils mm812 0.200.31 1 5001318 0.320.46 2 0001930 0.470.77 2 5003140 0.781.03 4 0004160 1.041.54 5 0006180 1.552.04 7 50081100 2.052.55 10 000101125 2.563.19 12 000126160 3.204.07 15 000161200 4.085.09 20 000201250 5.106.35 25 000D 5
35、16225.2.11 To prevent telegraphing (current traveling through amoisture path to a discontinuity, giving an erroneous indica-tion), take care to ensure that the solution is wiped dry from apreviously detected discontinuity before continuing the test.5.2.12 The wetting agent must be completely removed
36、 byrinsing the holiday area prior to repair.5.2.13 Wet sponge holiday detection is not recommendedbetween coats of a multicoat system. However, when a test isconducted between coats of a multicoat system, a wetting agentshall not be used and all residue left by the test water must becompletely remov
37、ed prior to applying additional coats.5.3 Verifying Operation of Equipment5.3.1 The instrument shall be tested for sensitivity prior toinitial use and periodically thereafter, in accordance with theequipment manufacturers instructions.5.3.2 Test the battery for proper voltage output. Refer to theman
38、ufacturers instructions.5.3.3 Switch the instrument to the “on position,” if appli-cable.5.3.4 Wet the sponge with a wetting solution consisting oftap water and a wetting agent (see 5.2.6).5.3.5 Connect the ground cable to the instrument groundoutput terminal.5.3.6 Touch the ground cable alligator c
39、lip to the wettedsponge. The instrument signal should actuate in accordancewith the instrument manufacturers instructions.5.3.7 If the instrument should fail to signal, it shall beconsidered defective.5.4 Verifying Instrument Calibration5.4.1 Verify instrument calibration in accordance with themanuf
40、acturers latest published instructions. If out of calibra-tion, the instrument shall be calibrated in accordance with theinstrument manufacturers latest published instructions, orreturned for calibration.TEST METHOD BHIGH VOLTAGE SPARKTESTING5.5 Apparatus5.5.1 High Voltage Detector (in excess of 800
41、 V)Anelectronic device used to locate discontinuities in a noncon-ductive protective coating applied to a conductive substrate. Itconsists of an electrical energy source, an exploring electrode,and a ground wire connection from the indicator signalingcurrent flow through a coating film discontinuity
42、 to thesubstrate. The detector shall be equipped with a visual oraudible indicator, or both.5.5.2 Exploring Electrode, shall be of the type capable ofmaintaining continuous contact with the surface being in-spected, such as bolts, raised areas, etc. It shall be kept cleanand free of coating material
43、.5.5.3 High Voltage Electrical Detector, can be identified aseither a pulse or direct current type. A pulse type detectordischarges a cycling, high voltage pulse, while a direct currenttype discharges continuous voltage.5.6 Procedure5.6.1 Sufficient drying or curing of the coating shall beallowed pr
44、ior to conducting a holiday test. The length of timerequired shall be obtained from the coating manufacturer.Solvents retained in the coating film could produce erroneousresults, as well as a fire hazard.5.6.2 The surface shall be clean, dry, and free of oil, dirt andother contaminates. Measure thic
45、kness of the coating with anondestructive dry film thickness gage. If the coating film isless than 20 mils (0.5 mm), consider using procedures for lowvoltage testing (see Test Method A, Low Voltage Wet SpongeTesting). Although the high voltage spark tester is suitable fordetermining discontinuities
46、in coating films of less than 20 mils(0.5 mm), it is recommended that the coating manufacturer beconsulted before using this test. Certain coatings may bedamaged if tested with this equipment.5.6.3 Verify test instrument operation in accordance with5.7.5.6.4 Adjust the test instrument to the proper
47、voltage for thecoating thickness being tested. In selecting the inspectionvoltage, it is important to provide sufficient voltage to break theair gap that exists at the holiday. The air gap will varydepending on the total applied film thickness. The voltagerequired to break a given air gap may also v
48、ary due toatmospheric conditions such as relative humidity. Ensure thatthe voltage is high enough to break the air gap equivalent to thehighest coating film thickness by separating the exploringelectrode from the bare metal substrate using a nonconductivespacer equal to the maximum coating thickness
49、. The voltage isset high enough to conduct the holiday test only if the sparkwill jump the gap formed by the spacer. Excessive voltage mayproduce a holiday in the coating film. The maximum voltagefor the applied coating shall be obtained from the coatingmanufacturer. Table 1 contains suggested voltages that can beused as guides.An alternative to Table 1 voltages is representedby the expression:V 5 C=Tc (1)where:V = test voltage,Tc = coating thickness, andC = dielectric constant established by the coating manu-facturer3.5.6.5 Attach ground wire
