1、Designation: D5213 07 D5213 12 An American National StandardStandard Specification forPolymeric Resin Film for Electrical Insulation and DielectricApplications1This standard is issued under the fixed designation D5213; the number immediately following the designation indicates the year oforiginal ad
2、option or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1
3、. Scope*1.1 This specification covers requirements for the material, dimensions and tolerances, and property values of film, in sheet orstrip form, with or without heat-sealable coatings.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for inf
4、ormation only.NOTE 1This document is similar to IEC 60674, Part 3, Sheets 2, 4, 5, 6, and 7.2. Referenced Documents2.1 ASTM Standards:2D149 Test Method for Dielectric Breakdown Voltage and Dielectric Strength of Solid Electrical Insulating Materials atCommercial Power FrequenciesD883 Terminology Rel
5、ating to PlasticsD1711 Terminology Relating to Electrical InsulationD2305 Test Methods for Polymeric Films Used for Electrical InsulationD3636 Practice for Sampling and Judging Quality of Solid Electrical Insulating MaterialsD4088 Practice for Preparation for Shipment of Solid Electrical Insulating
6、Materials (Withdrawn 2003)32.2 IEC Standards:Publication 60674-3 Specification for Electrical Films for Electrical Purposes43. Terminology3.1 DefinitionsDefinitions are in accordance with Terminologies D1711 and D883 unless otherwise specified.3.2 Definitions of Terms Specific to This Standard:3.2.1
7、 sheet, nmaterial greater than 75 mm in width.3.2.2 strip, nmaterial 75 mm or less in width.4. Classification4.1 This specification covers the following:4.1.1 Type IGeneral purpose,4.1.2 Type IIHeat sealable,4.1.2.1 Grade 1One side coated, and4.1.2.2 Grade 2Two sides coated.4.2 Materials:4.2.1 Item
8、APoly(N,N-p,p-oxydiphenylene pyromellitimide),4.2.2 Item BPoly(N,N-p,p-oxydiphenylene biphenyltetracarboxylimide,4.2.3 Item CPoly(N,N-p-phenylene biphenyltetracarboxylimide),4.2.4 Item DFEP-fluorocarbon, and4.2.5 Item EPolyethylene terephthalate.4.2.6 Item FPolyethylene naphthalate.4.2.7 Item GPolye
9、therimide.5. Ordering Information5.1 Order the film covered by this specification stating the type, grade, class, thickness, width, and roll dimensions.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken
10、, PA 19428-2959. United States16. Materials6.1 Type I material is flexible, unsupported film.6.2 Type II material is film meeting all of the requirements of Type I, and having a heat-sealable coating on one or both sides.7. Requirements7.1 The film covered by this specification shall meet the proper
11、ty requirements given in Tables 1-7 and Table 8 when tested bythe methods given in Test Methods D2305.7.1.1 Type II films, prior to coating, shall meet all of the requirements given in Table 1 for films of the thicknesses given in Table9.7.1.2 Type II films, after coating, shall meet all of the requ
12、irements given in Table 1 for elongation, before and after heating,and for shrinkage as given in Table 1 for films of the thicknesses given in Table 9.7.2 Roll Diameters:7.2.1 The outside diameters of rolls of film shall not vary from the value specified on the purchase order by more than 6 6 mm(0.2
13、5 in.).7.2.2 The inside diameters of cores of standard rolls of film shall not vary from the value specified on the purchase order bymore than 6 1.5 mm (0.060 in.).7.3 The widths of film in rolls shall be within the following tolerances:7.3.1 Twenty-five mm (1 in.) wide or less, 6 0.4 mm (0.015 in.)
14、.7.3.2 Over 25 to 100 mm (over 1 to 4 in.), 6 0.8 mm (0.030 in.).7.3.3 Over 100 mm (4 in.), 6 1.6 mm (0.062 in.).7.4 The number of splices in standard rolls shall not exceed the values given in Table 10 for Type I film or Table 11 and Table12 for Type II films.7.5 The thicknesses shall be within the
15、 tolerances specified in Table 13 for Type I film or Table 3 for Type II film.7.6 The color of the sheet or strip shall be uniform within a given lot, as determined by visual examination.7.7 The film shall be uniform in appearance, as determined by visual examination. The film shall be clean and fre
16、e fromcontamination, wrinkles, holes, scratches, and other defects that might affect either appearance or serviceability. The heat-sealablecoating for Type II material shall be uniform in appearance.1 This specification is under the jurisdiction of ASTM Committee D09 on Electrical and Electronic Ins
17、ulating Materials and is the direct responsibility of SubcommitteeD09.07 on Flexible and Rigid Insulating Materials.Current edition approved Oct. 1, 2007Nov. 1, 2012. Published October 2007November 2012. Orginally approved in 1991. Last previous edition approved in 20042007as D5213 04.D5213 07. DOI:
18、 10.1520/D5213-07.10.1520/D5213-12.2 For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvolume information, refer to the standards Document Summary page on the ASTM website.3 The last approved ver
19、sion of this historical standard is referenced on www.astm.org.4 Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http:/www.ansi.org.TABLE 1 Property Values for Type I, Class A Film poly(N,N*-p-p*-oxydiphenylene pyromellitimide)Average Prope
20、rty ValueNominal Thickness, m (mils)7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)Tensile strength, min MPa (psi),machine direction and transversedirection69(10 000)97(14 000)138(20 000)138(20 000)138(20 000)138(20 000)138(20 000)138(20 000)Elongation, min percent, machin
21、eand transverse direction10 20 35 35 40 45 45 45Shrinkage, max percent, afterexposure to 200 C (392 F),machine and transverse direction. . 0.30 0.30 0.35 0.35 0.35 0.35Moisture absorption, max percent, 100 % RH 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0Dielectric strength, min kV/mm(V/mil), 60 HzA,B120(3000)12
22、0(3000)180(4500)180(4500)150(3800)140(3600)100(2500)100(2500)Volume resistivity, min -cm,B ,C 1015 1015 1015 1015 1015 1015 1015 1015Permittivity, max at 1 kHzB 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0Dissipation factor, max at 1 kHzB 0.007 0.005 0.005 0.004 0.004 0.004 0.004 0.004AUse Type 3 electrodes in a
23、ir of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shouldshall be used for compliance.D5213 1228. Sampling8.1 Sample in accordance with Practice D3636, unless otherwise agreed upon between the supplier and the purchaser.8.
24、2 For purposes of sampling, an inspection lot for examination shall consist of all film of the same type, grade, class, andnominal thickness submitted for inspection at one time. If a single shipment contains film having different lot numbers assignedby the film manufacturer, sample each lot number
25、separately.8.3 The total quantity of material to be taken from each lot shall be approximately twice that estimated to be required for thetests that are to be made, in order to permit repeat tests without resampling.8.4 These materials are normally made in master rolls of approximately 360 kg (800 l
26、b) in weight. Take samples for examinationand testing from the end of the master rolls.9. Number of Tests9.1 Unless otherwise agreed upon by the purchaser and the seller, routine lot inspection tests shall consist of evaluation of allof the properties specified in 7.4-7.7. For these properties, each
27、 master roll shall be considered a lot for sampling. All samples mustpass inspection.9.2 Routine lot inspection tests for properties specified in 7.1, including definition of the number of master rolls per lot, shallbe agreed upon between the purchaser and the seller. All samples must pass inspectio
28、n.9.3 The number of specimens tested from each sample for properties specified in 7.1 and 7.5 shall be in accordance with therequirements of the individual test method. The test result on a sample shall be the average of the results on individual specimensprepared from that sample, unless otherwise
29、stated in the test method.TABLE 2 Property Values for Type I, Class B Film poly(N,N*-p-p*-oxydiphenylene biphenyltetracarboxylimide)Average Property ValueNominal Thickness, m (mils)7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 40 (1.6) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)Tensile strength, min MPa (psi),mach
30、ine direction and transversedirection110(15 000)138(20 000)196(28 000)196(28 000)196(28 000)196(28 000)196(28 000)196(28 000)196(28 000)Elongation, min percent, machineand transverse direction24 40 80 80 80 80 80 80 80Shrinkage, max percent, afterexposure to 200 C (392 F),machine and transverse dire
31、ction. . 0.30 0.30 0.35 0.35 0.35 0.35 0.35Moisture absorption, max percent, 100 % RH 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0Dielectric strength, min kV/mm(V/mil), 60 HzA,B120(3000)120(3000)180(4500)180(4500)150(3800)140(3500)130(3300)100(2500)95(2400)Volume resistivity, min -cm,B ,C 1015 1015 1015 1015
32、 1015 1015 1015 1015 1015Permittivity, max at 1 kHzB 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0Dissipation factor, max at 1 kHzB 0.007 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005A Use Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe
33、 median value of 5 measurements shouldshall be used for compliance.TABLE 3 Property Values for Type I, Class C Film poly(N,N*-p-phenylene biphenyltetracarboxylimide)Average Property ValueNominal Thickness, m (mils)7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 40 (1.6) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)Ten
34、sile strength, min MPa (psi),machine direction and transversedirection133(19 000)176(25 000)241(34 000)241(34 000)241(34 000)241(34 000)241(34 000)241(34 000)241(34 000)Elongation, min percent, machineand transverse direction25 25 25 25 25 25 25 25 25Shrinkage, max percent, afterexposure to 200 C (3
35、92 F),machine and transverse direction. . 0.15 0.15 0.15 0.20 0.20 0.20 0.20Moisture absorption, max percent, 100 % RH 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8Dielectric strength, min kV/mm(V/mil), 60 HzA,B120(3000)120(3000)180(4500)180(4500)150(3800)140(3500)120(3000)100(2500)95(2400)Volume resistivity,
36、 min -cm,B ,C 1015 1015 1015 1015 1015 1015 1015 1015 1015Permittivity, max at 1 kHzB 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0Dissipation factor, max at 1 kHzB 0.007 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005A Use Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods
37、).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shouldshall be used for compliance.D5213 1239.4 For slit rolls and full-width rolls other than master rolls, the number of samples taken for properties specified in 7.2-7.4 shallbe subject to agreement between the purchaser and the sel
38、ler.10. Certification10.1 The purchase order or contract shall state any requirements for certification by the producer. If required, a certification shallstate that the film was sampled in accordance with Section 8, tested in accordance with Test Methods D2305, and found to be inconformance with th
39、e requirements shown in Section 7. If required by the purchase order, or contract, the producer shall furnisha report of the testing used as the basis for the certification.11. Identification and Marking11.1 IdentificationMarking of the material shall show the name of the material, type and grade, d
40、imensions, and quantity.11.2 Shipping ContainersBoxes or crates shall be marked with the name of the material, type and grade, and dimensions andlot number; and the name and address of the supplier.11.3 All packing, packaging, and marking provisions of Practice D4088 shall apply to this specificatio
41、n.12. Keywords12.1 conditioning; dielectric strength; dissipation factor; elongation; FEP fluorocarbon; film; fluorinated poly(ethylene-propylene); heat-seal strength; heatsealable; permittivity; polyetherimide; polyethylene naphthalate; polyethylene terephthalate;TABLE 4 Property Values for Type I,
42、 Class D Film (FEPFluorocarbon)Average Property ValueNominal Thickness, m (mils)13(0.50)25(1.0)51(2.0)76(3.0)102(4.0)127(5.0)254(10.0)356(14.0)508(20.0)762(30.0)1016(40.0)1524(60.0)2413(95.0)Tensile strength, min MPa (psi),machine direction and transversedirection13.8(2000)17.25(2500)17.25(2500)17.2
43、5(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)Elongation, min, %, machinedirection and transversedirection175 250 250 250 250 250 250 250 250 250 250 250 250Shrinkage, max percent, afterexposure to 200 C (392 F)5.0 5.0 3.0 2.0 2.0 2.0 2.0 2
44、.0 2.0 4.0 4.0 4.0 5.0Moisture absorption, max percent,100 %, RH0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1Dielectric strength, min at 60 HzkV/mm (V/mil)A,B160(4000)160(4000)140(3500)120(3000)110(2750)100(2500)72(1800)64(1600)56(1400). . . .Volume resistivity, min, -cmB ,C 1017 1017 1017 101
45、7 1017 1017 1017 1017 1017 1017 1017 1017 1017Permittivity, max at 1 kHzB 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15Dissipation factor, max at 1 kHzB 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003A Use Type 3 electrodes in air of Tabl
46、e 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shouldshall be used for compliance.TABLE 5 Property Values for Type I, Class E Film (Polyethylene Terephthalate)Average Property ValueNominal Thickness, m (mils)12 (0.48) 15 (0.60)
47、23 (0.92) 36 (1.42) 75 (3.00) 100 (4.00) 190 (7.50) 250 (10.00)19 (0.75) 50 (2.00) 125 (5.00) 225 (9.00) 250Tensile strength, min MPa (psi),machine direction and transversedirection145 (21 000) 145 (21 000) 138 (20 000) 138 (20 000) 138 (20 000) 138 (20 000) 138 (20 000) 110(16 000)Elongation, min %
48、 machinedirection and transverse direction60 60 65 70 70 70 70 70Shrinkage, max percent afterexposure to 150 C (302 F), 30 min3.5 3.0 3.0 3.0 3.0 3.0 3.0 2.0Moisture absorption, max %, 100 % RH 0.8 0.8 0.8 0.8 0.8 0.8 0.8 0.8Dielectric strength, min at 60 Hz,kV/mm (V/mil)A,B208 (5300) 190 (4800) 174
49、 (4400) 130 (3300) 105 (2700) 80 (2000) 60 (1500) 50 (1300)Volume resistivity, min, -cmB ,C 1015 1015 1015 1015 1015 1015 1015 1015Permittivity, max at 1 kHzB 3.5 3.5 3.5 3.5 3.5 3.5 3.5 3.5Dissipation factor, max at 1 kHzB 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006A Use Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shouldshall be used for compliance.D5213 124TABLE 6 Property Values for Type I, Class F Film (Polyet
