1、Designation: D5267 97 (Reapproved 2017)Standard Test Method forDetermination of Extrudability of Cartridge Adhesives1This standard is issued under the fixed designation D5267; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the yea
2、r of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method measures the amount of force neces-sary to extrude an adhesive from a cartridge at a giventemper
3、ature.1.2 The values stated in inch-pound units are to be regardedas standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.3 This standard does not purport to address all of thesafety concerns, if any
4、, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety, health, and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.4 This international standard was developed in accor-dance with internationa
5、lly recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:2D907 Termino
6、logy of Adhesives3. Terminology3.1 DefinitionsMany terms in this test method are definedin Terminology D907.4. Significance and Use4.1 Cartridge adhesives are typically used at job sites in awide variety of temperature ranges. These products may beexposed to cold temperatures, where one of the limit
7、ingapplication factors is whether the product can be extruded fromthe cartridge.4.2 The test method quantitatively measures the force nec-essary to extrude a cartridge adhesive at a given temperature.This provides the formulator with results that can assist informulation development and the end user
8、 with information foruse in selecting a product for general usage.4.3 By measuring (the ease of) extrusion from the cartridge,the test method can also be used as a quality control tool tomeasure the shelf life stability of a product.5. Apparatus5.1 The test fixture is shown in Fig. 1. Details are sh
9、own inFigs. 2-4.3Make the framework from aluminum. Make the rodand plunger combination from steel.5.2 The test fixture is designed to be fitted onto a testmachine capable of measuring compressive strength.6. Conditioning6.1 Before measuring extrudability, condition the cartridgefilled with adhesive
10、until it reaches the desired constanttemperature.7. Procedure7.1 Mount the test fixture to the test machine for stability.7.2 After conditioning the cartridge, cut off enough of thetip, perpendicular to the cartridge, to ensure an inside diameterof14 in. (6.3 mm). If the cartridge has a foil or plas
11、tic liner,puncture it completely to allow passage of the material throughthe orifice. Record the temperature of the adhesive by insertinga thermometer or suitable thermocouple into the cartridge.7.3 Set the crosshead speed to 5.0 in. (127.0 mm) per min oranother acceptable rate.7.4 Activate the mach
12、ine to begin extrusion of the adhesivefrom the cartridge, measure the maximum force necessary tobegin the extrusion process as well as the force necessary tomaintain continued extrusion of the adhesive. The first value isthe force needed to release the plunger from the cartridge. Thesecond value is
13、the force needed to extrude the adhesive fromthe cartridge continuously.1This test method is under the jurisdiction of ASTM Committee D14 onAdhesives and is the direct responsibility of Subcommittee D14.10 on WorkingProperties.Current edition approved Nov. 1, 2017. Published November 2017. Originall
14、yapproved in 1992. Last previous edition approved in 2012 as D5267 97 (2012).DOI: 10.1520/D5267-97R17.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards
15、Document Summary page onthe ASTM website.3The apparatus is also available from Browning Technology, Inc., 1256 StanleyAve., Dayton, OH 45404.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in a
16、ccordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.18. Report8.1 Report the foll
17、owing information:8.1.1 Complete identification of the adhesive, includingtype, source, date of test, etc.8.1.2 Complete identification of the cartridge, includingtype, composition, liner used, plunger design, source, size, etc.8.1.3 Temperature of adhesive.8.1.4 Crosshead speed used for extrusion.8
18、.1.5 Force (in psi) used initially to extrude the adhesivefrom the cartridge and the average to maintain a constant flowof adhesive.9. Precision and Bias9.1 Precision:9.1.1 Table 1 presents round robin data generated from threelaboratories. Three different cartridge adhesives were used togenerate th
19、e data at two temperatures. The extrudability valueswere based on the average of three separate cartridge values.9.1.2 Repeatability at a given test site for the samplesyielded coefficients of variation from 2 to 18 % for Laboratory1, 1 to 10 % for Laboratory 2, and 2 to 13 % for Laboratory 3,with m
20、ost values in the range of 2 to 11 %.9.1.3 No statement of reproducibility from site to site isavailable at this time.9.2 BiasBias is the difference between the true forcenecessary to extrude an adhesive from a cartridge and the forcemeasured by a repeatable method. Bias arises from the consis-tency
21、 of the adhesive packaged in the cartridge, the method bywhich the plunger is assembled into the cartridge, and insidediameter variations that may exist when the cartridge tip is cut.10. Keywords10.1 adhesive; cartridge; extrusionD5267 97 (2017)2FIG. 1 Test Fixture for Measuring Extrusion from Cartr
22、idgeFIG. 2 Base Support for Test FixtureD5267 97 (2017)3FIG. 3 Cartridge Brace and Rear Support AssemblyFIG. 4 Rod and Follower Plate AssemblyD5267 97 (2017)4ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standa
23、rd. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewe
24、d every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible
25、technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Consh
26、ohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to p
27、hotocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 Cartridge Extrudability (in psi) for CartridgeAdhesivesRound Robin ResultsLaboratory1ALaboratory2BLaboratory3CRoom Temperature, 73 2F(23 1C)Adhesion A 67
28、 3 58 1 41 1Adhesion B 118 15 41 1 34 1Adhesion C 70 13 31 3 20 1Low TemperatureAdhesion A 70 10D672E532FAdhesion B 178 8 49 3 43 3Adhesion C 128 2 88 1 133 17ATested on an Instron 1120 machine.BTested on an Instron 1125 machine.CTested on a Thwing-Albert machine.DTested at 50 2F (10 1C).ETested at 45 2F (7 1C).FTested at 42 2F (5 1C).D5267 97 (2017)5
