1、Designation: D5329 15Standard Test Methods forSealants and Fillers, Hot-Applied, for Joints and Cracks inAsphalt Pavements and Portland Cement ConcretePavements1This standard is issued under the fixed designation D5329; the number immediately following the designation indicates the year oforiginal a
2、doption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 These test methods cover tests for hot-applied types ofjoint and crac
3、k sealants and fillers for portland cement concreteand asphaltic concrete pavements. There are numerous stan-dard material specifications that use these test methods. Referto the respective standard material specification of interest todetermine which of the following test methods to use. Forsample
4、melting and concrete block preparation see theirrespective standard practices.1.2 The test methods appear in the following sections:SectionArtificial Weathering 13Asphalt Compatibility 12Bond, Non-Immersed 8Bond, Water-Immersed 9Cone Penetration, Non-Immersed 6Flexibility 15Flow 7Resilience 10Resili
5、ence, Oven-Aged 11Tensile Adhesion 141.3 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.4 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the us
6、er of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D5 Test Method for Penetration of Bituminous MaterialsD217 Test Methods for Cone Penetration of LubricatingGrea
7、seD618 Practice for Conditioning Plastics for TestingD1074 Test Method for Compressive Strength of Bitumi-nous MixturesD1561 Practice for Preparation of Bituminous Mixture TestSpecimens by Means of California Kneading CompactorD1985 Practice for Preparing Concrete Blocks for TestingSealants, for Joi
8、nts and CracksD3381 Specification for Viscosity-Graded Asphalt Cementfor Use in Pavement ConstructionD5167 Practice for Melting of Hot-Applied Joint and CrackSealant and Filler for EvaluationD6690 Specification for Joint and Crack Sealants, HotApplied, for Concrete and Asphalt PavementsE145 Specific
9、ation for Gravity-Convection and Forced-Ventilation OvensG151 Practice for Exposing Nonmetallic Materials inAccel-erated Test Devices that Use Laboratory Light SourcesG154 Practice for Operating Fluorescent Ultraviolet (UV)Lamp Apparatus for Exposure of Nonmetallic MaterialsG155 Practice for Operati
10、ng Xenon Arc Light Apparatus forExposure of Non-Metallic Materials3. Significance and Use3.1 These test methods describe procedures for determiningspecification conformance for hot-applied, field-molded jointand crack sealants and fillers.4. Sample Melting4.1 See Practice D5167.5. Standard Condition
11、s5.1 The laboratory atmospheric conditions, hereinafter re-ferred to as standard conditions, shall be in accordance withPractice D618 (23 6 2C, 50 6 10 % Relative Humidity).6. Cone Penetration, Non-Immersed6.1 ScopeThis test method covers determination of conepenetration of bituminous joint and crac
12、k sealers and fillers.1These test methods are under the jurisdiction of ASTM Committee D04 onRoad and Paving Materials and are the direct responsibility of SubcommitteeD04.33 on Formed In-Place Sealants for Joints and Cracks in Pavements.Current edition approved Dec. 15, 2015. Published February 201
13、6. Originallyapproved in 1992. Last previous edition approved in 2009 as D5329 09. DOI:10.1520/D5329-15.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standard
14、s Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States16.2 Significance and UseThe cone penetration, non-immersed is a measure of consistency. Higher values indicatea softer consistency.6.3 Apparatu
15、sConduct this test using the apparatus de-scribed in Test Method D5, except as specified herein. Use apenetration cone in place of the standard penetration needle.The cone shall conform to the requirements given in TestMethods D217, except that the interior construction may bemodified as desired. Th
16、e total moving weight of the cone andattachments shall be 150.0 6 0.1 g.6.4 Specimen PreparationPour a portion of the sampleprepared in accordance with Practice D5167 into a cylindrical,metal, flat bottom container of essentially 60 to 75 mm indiameter and 45 to 55 mm in depth and fill flush with th
17、e rimof the container. Allow the specimen to cure under standardconditions as specified in its respective material specification.6.5 ProcedurePlace the specimen in a water bath main-tained at 25 6 0.1C for 2 h immediately before testing.Remove the specimen from the bath and dry the surface. Usingthe
18、 apparatus described in 6.3, make determinations at threelocations on approximately 120 radii, and halfway betweenthe center and outside of the specimen. Take care to ensure thecone point is placed on a point in the specimen that isrepresentative of the material itself and is free of dust, water,bub
19、bles or other foreign material. Clean and dry the cone pointafter each determination.6.6 ReportAverage the three results and record the valueas the penetration of the specimen in110 mm units.6.7 Precision and Bias:6.7.1 For Specification D6690 Type I materials, the follow-ing precision statement is
20、based on an interlaboratory study of12 laboratories that tested five different Specification D6690Type I materials.6.7.1.1 Within ContainerSingle-Operator Precision (forpenetration between 40 and 80): The single-operator deviationhas been found to be 0.994. Therefore, results of two properlyconducte
21、d tests by the same operator should not differ by morethan three penetration units.6.7.1.2 Within LaboratoriesSingle-Operator Precision(penetrations 40 to 80): The single-operator standard deviationof a single test (test result is defined as the average of threepenetrations) has been found to be 0.9
22、24. Therefore, the resultsof two properly conducted tests by the same operator on thesame material should not differ by more than three penetrationunits.6.7.1.3 Multilaboratory Precision(penetration 40 to 80):The multilaboratory standard deviation of a single test (testresult is defined as the avera
23、ge of three penetrations) has beenfound to be 3.249. Therefore, the results of two properlyconducted tests in different laboratories should not differ bymore than nine penetration units.6.7.2 For Specification D6690 Type II materials, the follow-ing precision statement is based on an interlaboratory
24、 study ofeleven laboratories that tested six different Specification D6690Type II materials.6.7.2.1 Within ContainerSingle-Operator Precision (forpenetration between 55 and 85): The single-operator deviationhas been found to be 0.974. Therefore, results of two properlyconducted tests by the same ope
25、rator should not differ by morethan three penetration units.6.7.2.2 Within LaboratoriesSingle-Operator Precision(penetrations 50 to 70): The single-operator standard deviationof a single test (test result is defined as the average of threepenetrations) has been found to be 1.0865. Therefore, theresu
26、lts of two properly conducted tests by the same operator onthe same material should not differ by more than threepenetration units.6.7.2.3 Single-Operator Precision(penetrations 71 to 85):The single-operator standard deviation of a single test (testresult is defined as the average of three penetrati
27、ons) has beenfound to be 2.237. Therefore, the results of two properlyconducted tests by the same operator on the same materialshould not differ by more than six penetration units.6.7.2.4 Multilaboratory Precision(penetration 50 to 70):The multilaboratory standard deviation of a single test (testres
28、ult is defined as the average of three penetrations) has beenfound to be 5.2609. Therefore, the results of two properlyconducted tests in different laboratories should not differ bymore than 15 penetration units.6.7.2.5 Multilaboratory Precision(penetration 71 to 85):The multilaboratory standard dev
29、iation of a single test (testresult is defined as the average of three penetrations) has beenfound to be 16.8831. Therefore, the results of two properlyconducted tests in different laboratories should not differ bymore than 48 penetration units.7. Flow7.1 ScopeThis test method measures the amount of
30、 flowof bituminous joint and crack sealants when held at a 75 angleat elevated temperatures.7.2 Significance and UseThis test method is a means ofmeasuring the ability of a sealant to resist flow from the jointor crack at high ambient temperatures.7.3 Apparatus:7.3.1 MoldConstruct a mold (see Note 1
31、) 40 mm wide by60 mm long by 3.2 mm deep and place it on a bright tin panel.The tin plate must be free of dirt, oil, and so forth and bebetween 0.25 to 0.64 mm in thickness.NOTE 1A release agent should be used to coat molds and spacers toprevent them from bonding to the sealants. Extreme care should
32、 beexercised to avoid contaminating the area where the joint sealant makescontact with the blocks.Anon-toxic release agent is recommended for thispurpose. Two examples that have been found suitable for this purpose areKY jelly (available at drug stores) and a release agent prepared bygrinding a mixt
33、ure of approximately 50 % talc, 35 % glycerine, and 15 %by weight, of a water-soluble medical lubricant into a smooth paste.7.3.2 OvenForced draft type conforming to SpecificationE145 and capable of controlling its temperature 61C.7.4 Specimen PreparationPour a portion of the sampleprepared in accor
34、dance with Practice D5167 for meltingsamples into the mold described in 7.3. Fill the mold with anexcess of material. Allow the test specimen to cool at standardconditions for at least12 h, then trim the specimen flush withthe face of the mold with a heated metal knife or spatula andD5329 152remove
35、the mold. Allow the specimen to cure under standardconditions as specified in its respective material specification.7.5 ProcedureMark reference lines on the panel at thebottom edge of the sealant. Then place the panel containing thesample in a forced-draft oven maintained for the time and at thetemp
36、erature specified in its respective material specification.During the test, mount the panel so that the longitudinal axis ofthe specimen is at an angle of 75 6 1 with the horizontal, andthe transverse axis is horizontal.After the specified test period,remove the panel from the oven and measure the m
37、ovement ofthe specimen below the reference lines in millimetres.7.6 ReportReport the measurement obtained in 7.5 inmillimetres.7.7 Precision and Bias:7.7.1 For Specification D6690 Type I materials, the follow-ing precision statement is based on an interlaboratory study of12 laboratories that tested
38、five different Specification D6690Type I materials.7.7.1.1 Single-Operator Precision (flow 0 to 5)The single-operator standard deviation has been found to be 0.255.Therefore, the results of two properly conducted tests by thesame operator should not differ by more than one flow unit.7.7.1.2 Single-O
39、perator Precision (flow 5 to 10)Thesingle-operator standard deviation has been found to be 1.024.Therefore, the results of two properly conducted tests by thesame operator should not differ by more than three flow units.7.7.1.3 Multilaboratory Precision (flow 0 to 5)The multi-laboratory standard dev
40、iation has been found to be 4.256.Therefore, the results of two properly conducted tests indifferent laboratories should not differ by more than 12 flowunits.7.7.1.4 Multilaboratory Precision (flow 5 to 10)The mul-tilaboratory standard deviation has been found to be 5.326.Therefore, the results of t
41、wo properly conducted tests indifferent laboratories should not differ by more than 15 flowunits.7.7.2 For Specification D6690 Type II materials, the follow-ing precision statement is based on an interlaboratory study ofeleven laboratories that tested six different Specification D6690Type II materia
42、ls.7.7.2.1 Single-Operator Precision (flow 0 to 1)The single-operator standard deviation has been found to be 0.2494.Therefore, the results of two properly conducted tests by thesame operator should not differ by more than one flow unit.7.7.2.2 Single-Operator Precision (flow 1.1 to 4)Thesingle-oper
43、ator standard deviation has been found to be 0.7616.Therefore, the results of two properly conducted tests by thesame operator should not differ by more than three flow units.7.7.2.3 Multilaboratory Precision (flow 0 to 1)The multi-laboratory standard deviation has been found to be 0.5644.Therefore,
44、 the results of two properly conducted tests indifferent laboratories should not differ by more than three flowunits.7.7.2.4 Multilaboratory Precision (flow 1.1 to 4)The mul-tilaboratory standard deviation has been found to be 2.3508.Therefore, the results of two properly conducted tests indifferent
45、 laboratories should not differ by more than seven flowunits.8. Bond, Non-Immersed8.1 ScopeThis test method is used to evaluate the bond toconcrete.8.2 Significance and UseBond to concrete is necessary fora sealant to maintain proper field performance.8.3 Apparatus:8.3.1 Extension MachineThe extensi
46、on machine used inthe bond test shall be so designed that the specimen can beextended a minimum of 12.5 mm at a uniform rate of 3.1 6 0.3mm per hour. It shall consist essentially of one or more screwsrotated by an electric motor through suitable gear reductions.Self aligning plates or grips, one fix
47、ed and the other carried bythe rotating screw or screws, shall be provided for holding thetest specimen in position during the test.38.3.2 Cold ChamberThe cold chamber shall be capable ofmaintaining the required cold test temperature within 61C.8.4 Concrete-Block PreparationThe concrete blocks shall
48、be prepared in accordance with Practice D1985.8.5 Specimen Preparation:8.5.1 Prepare three test specimens (3 specimens2=6blocks) as follows: On removal from the storage container,again scrub the 50 by 75 mm saw-cut faces of the blocks underrunning water. When all blocks are scrubbed, lightly blot th
49、emwith an oil-free, soft, absorbent cloth or paper towel to removeall free surface water and condition them by air drying on the25 by 50 mm ends for 1 h 6 10 min.8.5.2 Take these blocks and mold the test specimen betweenthem as follows (see Fig. 1): Place four treated (see Note 1)brass or TFE-fluorocarbon spacer strips, approximately 6 mmthick, on a treated metal plate base to enclose an open spaceaccording to the width specified in the respective materialspecification by 50 mm long. Place the blocks on the spacerstrips and space them the
