1、Designation: D 5552 00 (Reapproved 2005)Standard Test Method forResistance of Colored Leather to Bleeding1This standard is issued under the fixed designation D 5552; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last
2、revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers the determination of the resis-tance of colored leather to bleeding. This test method does notappl
3、y to wet blue.1.2 This test method is intended for use on finished upperleather for shoes or similar end use, or the leather article suchas shoe, handbag, etc.1.3 The values stated in inch-pound units are to be regardedas the standard. The values given in parentheses are forinformation only.1.4 This
4、 standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents
5、2.1 ALCA Method:K12Method for Testing Resistance of Colored Leather toBleeding23. Terminology3.1 Definitions of Terms Specific to This Standard:3.1.1 bleedingthe transfer of color from a finished leathersample onto or into another medium.4. Significance and Use4.1 Bleed resistance is considered to b
6、e an important char-acteristic in leather used to make lined and unlined items thatmay come in contact with water.5. Apparatus5.1 Air-Tight Oven.5.2 Bleached Cotton Sheeting,32 in. squares (51.6 by 51.6mm).5.3 Glass Plates, two 6 in. squares (152.4 by 152.4 mm) and0.125 in. (3.18 mm) thick.6. Test S
7、pecimen6.1 The test specimen shall be a 4 in. square (101.6 by 101.6mm) of finished leather.7. Procedure7.1 Place the unfinished side of the leather specimen on thecenter of one of the glass plates. Thoroughly soak the foursquares of cotton sheeting in distilled water for 5 min. Stackthem on top of
8、each other on the other glass plate. Invert thisplate with the cotton cloths, and place on top of the other plateholding the leather specimen. The cloths should line upapproximately in the center of the leather specimen.7.2 The cloth in immediate contact with the leather ismarked Number 1, the next
9、cloth Number 2, the next Number3 and the top cloth Number 4. Place this entire sandwich in anoven at 120F (49C) for 12 h. Remove the glass plates andobserve the individual cloths for discoloration.8. Report8.1 Migration of BleedingObserve each of the four clothsfor coloration and report migration as
10、 0, 1, 2, 3, or 4. Thenumbers indicate the cotton cloth that discoloration hasreached by migration.8.2 HueNote the predominant hue of the colors that bledon each cloth.8.3 IntensityObserve each cloth Number 1 for this pur-pose. The degrees of intensity shall be termed none, slight,moderate, or consi
11、derable as determined by comparing the testcloth discoloration to the AATCC Grey Scale for EvaluatingStaining.4Intensity shall be reported using AATCC Grey Scalenumbering.1This test method is under the jurisdiction of ASTM Committee D31 on Leatherand is the direct responsibility of Subcommittee D31.
12、06 on Chemical AnalysisGeneral.Current edition approved Sept. 1, 2005. Published September 2005. Originallyapproved in 1994. Last previous edition approved in 2000 as D 555200.2Developed by and available from the American Leather Chemists Association(ALCA), University of CincinnatiM.L. 14, Cincinnat
13、i, OH 45221-0014.3The sole source of supply of the sheeting known to the committee at this timeis Testfabrics Inc., 200 Blackford Avenue, P.O. Box 420, Middlesex, NJ 08846-0420. If you are aware of alternative suppliers, please provide this information toASTM Headquarters.Your comments will receive
14、careful consideration at a meetingof the responsible technical committee,1which you may attend.4Available from American Association of Textile Chemists and Colorists, P.O.Box 12215, Research Triangle Park, NC 27709.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken,
15、 PA 19428-2959, United States.9. Precision and Bias9.1 This test method is adopted from Method K12of theAmerican Leather ChemistsAssociation where it has long beenin use and was approved for publication before the inclusion ofprecision and bias statements was mandated. The originalinterlaboratory te
16、st data are no longer available. The user iscautioned to verify by the use of reference materials, ifavailable, that the precision and bias (or reproducibility) of thistest method is adequate for the contemplated use.10. Keywords10.1 bleed resistance; bleeding; migrationASTM International takes no p
17、osition respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsib
18、ility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to
19、ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the addre
20、ss shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).D 5552 00 (2005)2
