1、Designation: D6012 03 (Reapproved 2013)Standard Test Method forDetermination of Resistance of Leather to (Bleeding) ColorStain Transfer1This standard is issued under the fixed designation D6012; the number immediately following the designation indicates the year oforiginal adoption or, in the case o
2、f revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope1.1 This test met
3、hod2covers the determination of whetherleather bleeds (exudes coloring matter) when in intimatecontact with wet surfaces, as indicated by staining produced onwet cloth in contact with the leather. This test method does notapply to wet blue.1.2 The values stated in inch-pound units are to be regarded
4、as standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of
5、this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:3D1610 Practice for Conditioning Leather and Leather Prod-ucts for Testing3. Terminology3.1 Definitions of Terms Speci
6、fic to This Standard:3.1.1 bleedingthe transfer of color from a finished leathersample onto or into another medium.4. Significance and Use4.1 Bleed resistance is considered to be an important char-acteristic in leather used to make lined and unlined items thatmay come in contact with water.5. Appara
7、tus5.1 One or More Assemblies, consisting of a flat glass orplastic square, and same size as transfer pad with a suitableweight placed on top of the square. The combined weight shallbe 100 6 5 g. (An assembly consisting of a plastic or glassplate and a 1 fluid oz (29 cc) plastic or glass jar with pl
8、astic lidto which the appropriate amount of lead shot or steel balls isadded has been found suitable. The plate and jar may be heldtogether by a suitable cement or pressure-sensitive adhesivetape.)5.2 Container, flat-bottomed, heat-resistant plastic or othersimilar material with cover of sufficient
9、size to accommodate amaximum of 15 specimens. A container 12 in. (300 mm) long,9 in. (230 mm) wide and 4 in. (100 mm) high has been foundsuitable.5.3 Forced Circulating-Air Oven, capable of maintainingthe required temperature of 38 6 2C (100.4 6 3.6F).5.4 Balance, single beam or high speed.5.5 Bleac
10、hed Cotton Sheeting,42-in. (51.6-mm) squares.6. Test Specimen6.1 The specimen shall be a square of leather 1.0 by 1.0 in.(25 by 25 mm).6.2 Number of DeterminationsUnless otherwise specifiedin the material specification, one specimen from each sampleunit shall be tested.7. Procedure7.1 Bring the leat
11、her specimen and the color transfer padmade of 4 layers of cotton sheeting to moisture equilibrium inaccordance with standard atmospheric conditions (see PracticeD1610). Weigh the conditioned pad to the nearest 0.05 g. Afterweighing, wet the pad with enough distilled water to double theweight of the
12、 conditioned pad.1This test method is under the jurisdiction of ASTM Committee D31 on Leatherand is the direct responsibility of Subcommittee D31.04 on Apparel.Current edition approved Nov. 1, 2013. Published November 2013. Originallyapproved in 1996. Last previous edition approved in 2008 as D60120
13、3(2008).DOI: 10.1520/D6012-03R13.2This test method was developed from Federal Test Method Standard No. 311Method 3021.2 in cooperation with the U.S. Army Natick Research Developmentand Engineering Center, Natick, MA, and the Defense Personnel Support CenterDirectorate of Clothing and Textiles, Phila
14、delphia, PA.3For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.4The sole source of supply of the color transfer
15、cloth known to the committee atthis time is Test Fabrics, Inc., P.O. Box 53, 200 Blackford Ave., Middlesex, NJ08846. If you are aware of alternative suppliers, please provide this information toASTM Headquarters.Your comments will receive careful consideration at a meetingof the responsible technica
16、l committee, which you may attend.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1NOTE 1The dry weight of the conditioned pad is usually 1.0 to 1.1 g,and the weight of the wet pad is usually 2.0 to 2.2 g.If necessary, remove excess wa
17、ter from the pad in order toattain the proper weight. Place the wet pad in the bottom of theplastic container, and place the leather specimen approximatelyin the center of the pad. Unless otherwise specified, the grainside of the leather shall be in contact with the pad. Immediatelyplace the load as
18、sembly on top of the specimen. Care should betaken to ensure the plastic or glass square portion of the loadassembly completely covers the specimen and transfer pad.Cover the container and place on a shelf in the circulating-airoven at 38 6 2C (100.46 3.6F) for 6 h. At the end of therequired time, t
19、ake the container from the oven. Remove thepad and allow it to dry at a temperature of 23 6 2C (73.4 63.6F). Rate the darkest stain on the pad in indirect light bymatching it with the color on the AATCC Chromatic Transfer-ence Scale5that is closest to it in chromaticity and hue.8. Report8.1 Report t
20、he staining result according to the followingexpanded AATCC ratings:Comparison of Test Pad Stain withNumerical AATCC ValuesExpanded AATCCRating ValueStain heavier than 1 0Stain equivalent to 1 1Stain lighter than 1 but heavier than 2 +1Stain equivalent to 2 2Stain lighter than 2 but heavier than 3 +
21、2Stain equivalent to 3 3Stain lighter than 3 but heavier than 4 +3Stain equivalent to 4 49. Precision and Bias9.1 This test method is adopted from Federal Test StandardNo. 311, Method 3021.2 where it has long been in use and wasapproved for publication before the inclusion of precision andbias state
22、ments was mandated. The original interlaboratory testdata are no longer available. The user is cautioned to verify bythe use of reference materials, if available, that the precisionand bias (or reproducibility) of this test method is adequate forthe contemplated use.10. Keywords10.1 bleed resistance
23、; bleeding; leather; migrationASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof in
24、fringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this stan
25、dard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your v
26、iews known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contac
27、ting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).5The sole source of supply of the appa
28、ratus known to the committee at this timeis AATCC National Headquarters, P.O. Box 12215, Research Triangle Park, NC22709. If you are aware of alternative suppliers, please provide this information toASTM Headquarters.Your comments will receive careful consideration at a meetingof the responsible technical committee,1which you may attend.D6012 03 (2013)2
