ASTM E1613-2012 Standard Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) Flame Atomic Absorption Spectrometry (FAAS) or GG.pdf
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1、Designation:E161304 Designation: E1613 12Standard Test Method forDetermination of Lead by Inductively Coupled PlasmaAtomic Emission Spectrometry (ICP-AES), Flame AtomicAbsorption Spectrometry (FAAS), or Graphite FurnaceAtomic Absorption Spectrometry (GFAAS) Techniques1This standard is issued under t
2、he fixed designation E1613; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the l
3、ast revision or reapproval.1. Scope1.1 This test method is intended for use with extracted or digested samples that were collected during the assessment,management, or abatement of lead hazards from buildings, structures, or other locations.1.2 This test method covers the lead analysis of sample ext
4、racts or digestates (for example, extracted or digested paint, soil, dust,and airborne particulate) using inductively coupled plasma atomic emission spectrometry (ICP-AES), flame atomic absorptionspectrometry (FAAS), or graphite furnace atomic absorption spectrometry (GFAAS).1.3 This test method con
5、tains directions for sample analysis, as well as quality assurance (QA) and quality control (QC), andmay be used for purposes of laboratory accreditation and certification.1.4 No detailed operating instructions are provided because of differences among various makes and models of suitableinstruments
6、. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument.1.5The values stated in SI units are to be regarded as the standard.1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this stan
7、dard.1.6 This practice contains notes which are explanatory and not part of the mandatory requirements of this standard.1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibilityof the user of this standard to establish appropr
8、iate safety and health practices and determine the applicability of regulatorylimitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D1193 Specification for Reagent WaterD3919 Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption SpectrophotometryD4210 Pra
9、ctice for Intralaboratory Quality Control Procedures and a Discussion on Reporting Low-Level DataD4697 Guide for Maintaining Test Methods in the Users LaboratoryD4840 Guide for Sample Chain-of-Custody ProceduresD6785 Test Method for Determination of Lead in Workplace Air Using Flame or Graphite Furn
10、ace Atomic AbsorptionSpectrometryD7144 Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Metals DeterminationE456 Terminology Relating to Quality and StatisticsE691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test MethodE1188 Practic
11、e for Collection and Preservation of Information and Physical Items by a Technical InvestigatorE1605 Terminology Relating to Lead in BuildingsE1644 Practice for Hot Plate Digestion of Dust Wipe Samples for the Determination of LeadE1645 Practice for Preparation of Dried Paint Samples by Hotplate or
12、Microwave Digestion for Subsequent Lead AnalysisE1726 Practice for Preparation of Soil Samples by Hotplate Digestion for Subsequent Lead AnalysisE1727 Practice for Field Collection of Soil Samples for Subsequent Lead DeterminationE1728 Practice for Collection of Settled Dust Samples Using Wipe Sampl
13、ing Methods for Subsequent Lead Determination1This test method is under the jurisdiction ofASTM Committee E06 on Performance of Buildings and is the direct responsibility of Subcommittee E06.23 on Lead HazardsAssociated with Buildings.Current edition approved August 1, 2004.July 15, 2012. Published
14、August 2004.2012. Originally approved in 1994. Last previous edition approved in 19992004 asE161399.E1613 04. DOI: 10.1520/E1613-04.10.1520/E1613-12.2For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standar
15、dsvolume information, refer to the standards Document Summary page on the ASTM website.1This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Becauseit may not be technically possible t
16、o adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versionof the standard as published by ASTM is to be considered the official document.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Con
17、shohocken, PA 19428-2959, United States.E1729 Practice for Field Collection of Dried Paint Samples for Subsequent Lead DeterminationE1741 Practice for Preparation of Airborne Particulate Lead Samples Collected During Abatement and Construction Activitiesfor Subsequent Analysis by Atomic Spectrometry
18、E1775 Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or SpectrophotometricAnalysis for LeadE1792 Specification for Wipe Sampling Materials for Lead in Surface DustE1864 Practice for Evaluating Quality Systems of Organizations Conducting Facility and Hazard
19、Assessments for Lead inPaint, Dust, Airborne Particulate, and Soil in and around Buildings and Related Structures E1973Practice for Collection ofSurface Dust by Air SamplingPump Vacuum Technique forSubsequent Lead Determina-tionE1979 Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air S
20、amples for Subsequent Determination of LeadE2239 Practice for Record Keeping and Record Preservation for Lead Hazard Activities3. Terminology3.1 Definitions: For definitions of terms not appearing here, see Terminology E1605.3.2 Definitions of Terms Specific to This Standard:3.2.1 analysis runa peri
21、od of measurement time on a given analytical instrument during which data are calculated from asingle calibration curve (or single set of curves).3.2.1.1 DiscussionRecalibration of a given instrument produces a new analysis run.3.2.2 calibration standardssolutions of known analyte concentrations use
22、d to calibrate instruments.3.2.2.1 DiscussionCalibration standards must be matrix matched to the acid content present in sample digestates or extractsand must be measured prior to analyzing samples.3.2.3 continuing calibration blank (CCB)a solution containing no analyte that is used to verify blank
23、response and freedomfrom carryover.3.2.3.1 DiscussionThe CCB must be analyzed after the CCV (see 3.2.4) and after the ICkS (see 3.2.9). The measured valueis to be (at most) less than five times the instrumental detection limit (IDL) (see 3.2.7).3.2.4 continuing calibration verification (CCV)a soluti
24、on (or set of solutions) of known analyte concentration used to verifyfreedom from excessive instrumental drift; the concentration is to be near the mid-range of a linear calibration curve.3.2.4.1 DiscussionThe CCV must be matrix matched to the acid content present in sample digestates or extracts.
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