1、Designation: F 1104 02 (Reapproved 2008)Standard Test Method forPreparing Aircraft Cleaning Compounds, Liquid Type, WaterBase, for Storage Stability Testing1This standard is issued under the fixed designation F 1104; the number immediately following the designation indicates the year oforiginal adop
2、tion or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers the determination of the stabil-ity in storage,
3、 of liquid, water-base chemical cleaning com-pounds, used to clean the exterior surfaces of aircraft.1.2 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and hea
4、lth practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 U.S. Government Documents:2Federal Specification PPP-P-704 Pails, Metal (Shipping,Steel, 1 through 12 Gallons)3. Summary of Test Method3.1 Storage stability is determined by evaluation of
5、 theeffect of time, temperature, and environmental conditions onthe cleaning compound. Samples used for testing are filledcontainers taken from the manufacturers controlled productionformulation, packaged and delivered to the purchaser fornormal use. The sample container shall be subjected to thespe
6、cified storage environment for a period of 12 months. Thetest shall be completed prior to 24 months from date ofpackaging.4. Significance and Use4.1 This test method determines the procedure to be used toensure the long term storage stability of aircraft cleaning andmaintenance products, in order to
7、 ensure their ability to meetthe shelf-life requirements called up in specifications or con-tract documents. The subsequent testing requirements aredetailed in the specification or contract.5. Sampling5.1 The sample for storage stability testing shall be takenfrom a controlled production formula, pa
8、ckaged lot, or batchdelivered in a sealed, filled container to the purchaser for use.This sample is normally a 1 gal can conforming to FederalSpecification PPP-P-704. This material shall have previouslybeen tested and passed all other specification requirements forqualification or acceptance. The sa
9、mple container selected forthe test shall be kept sealed and unopened for the duration ofthe test. The sample container shall be durably and legiblymarked with the following minimum information:Storage Stability Test SampleSupplierFormula numberDate of packagingCold test periodHot test periodBatch/l
10、ot No.Test beganTest ends6. Procedure6.1 Storage EnvironmentPlace the sample container in astorage area where a temperature of 50 to 91F (10 to 33C) ismaintained at least 80 % of the total storage test time. Do notsubject the storage test sample to temperature over 150F(66C) or under 10F (12C) durin
11、g the entire test. Maintainthe sample container in a static condition not subject tovibration, rolling, inversion, or other movement. Movement tothe necessary temperature-controlled area for cold- and hot-temperature testing is excepted, but accomplish such transferwith minimum (or no) disturbance o
12、f container contents.6.1.1 Cold-Temperature Storage EnvironmentSubject thesample container to a 15-day time interval 17 6 3F (8 62C). Conduct this cold test interval during the period 90 to120 days after start of the storage stability test time.6.1.2 Hot-Temperature Storage EnvironmentSubject thesam
13、ple container to a 15-day time interval at 120 6 18F (496 10C). Conduct this hot test interval after 270 days ofelapsed test time but 60 days prior to the termination of thestorage test.1This test method is under the jurisdiction of ASTM Committee F07 onAerospace and Aircraft and is the direct respo
14、nsibility of Subcommittee F07.07 onQualification Testing of Aircraft Cleaning Materials.Current edition approved April 1, 2008. Published April 2008. Originallyapproved in 1987. Last previous edition approved in 2002 as F 1104 02.2Available from Standardization Documents Order Desk, Bldg. 4 Section
15、D, 700Robbins Ave., Philadelphia, PA 19111-5098, Attn: NPODS.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.6.1.3 Completion of TestAfter 12 months storage test timecarefully remove the sample container (if necessary), withoutagitat
16、ion, rolling, or inversion, from the storage area and placein a room, in a stable location for 48 6 1 h at a temperature of71 to 80F (22 to 27C). At the end of 48 h, remove the top ofthe container and examine the internal surface for corrosion orsediment. Disregard discoloration of the interior surf
17、ace of thecontainer. Take samples of the product and test in accordancewith the relevant specification or contract requirements.7. Precision and Bias7.1 No statement can be made relating to precision and biassince the only nonvariables are the environmental conditions.The pass or fail requirement is
18、 determined by the subsequenttests called up by the specification or contract.8. Keywords8.1 stability; storage; waterbaseASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expre
19、ssly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised
20、, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may a
21、ttend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).F 1104 02 (2008)2
