1、Designation: F 1105 03Standard Test Method forPreparing Aircraft Cleaning Compounds, Liquid-Type,Temperature-Sensitive, or Solvent-Based, for StorageStability Testing1This standard is issued under the fixed designation F 1105; the number immediately following the designation indicates the year ofori
2、ginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers the determination of the stabil-ity i
3、n storage of liquid enzyme-based, terpene-based, andsolvent-based chemical cleaning compounds used to clean theexterior surfaces of aircraft.1.2 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.1.3 This standard does not purport
4、 to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 U.S. Government Docume
5、nt:Federal Specification PPP-P-704 Pails, Metal Shipping,Steel 1 through 12 Gallons23. Summary of Test Method3.1 Storage stability is determined by evaluation of theeffect of time, temperature, and environmental conditions onthe cleaning compound. Samples used for testing are filledcontainers taken
6、from the manufacturers controlled productionformulation, packaged, and delivered to the purchaser fornormal use.3.2 The sample container shall be subjected to the specifiedstorage environment for a period of 12 months. The test shallbe completed prior to 24 months from date of packaging.4. Significa
7、nce and Use4.1 This test method determines the procedure to be used toensure the long-term storage stability of aircraft cleaning andmaintenance products in order to ensure their ability to meetthe shelf-life requirements called up in specifications or con-tract documents. The subsequent testing req
8、uirements aredetailed in the specification or contract.5. Sampling5.1 The sample for storage stability testing shall be takenfrom a controlled production formula, packaged lot, or batchdelivered in a sealed, filled container to the purchaser for use.This sample is normally a 1-gal can conforming to
9、FederalSpecification PPP-P-704. This material shall have previouslybeen tested and passed all other specification requirements forqualification or acceptance. The sample container selected forthe test shall be kept sealed and unopened for the duration ofthe test. The sample container shall be durabl
10、y and legiblymarked with the following minimum information:Storage Stability Test SampleSupplierFormula numberDate of packagingCold test periodHot test periodBatch/Lot No.Test beganTest ends6. Procedure6.1 Storage EnvironmentPlace the sample container in astorage area where a temperature of 10 to 27
11、C (50 to 80F) ismaintained at least 80 % of the total storage test time. Do notsubject the storage test sample to temperature over 32C (90F)or under 12C (10F) during the entire test. Maintain thesample container in a static condition not subject to vibration,rolling, inversion, or other movement. Mo
12、vement to thenecessary temperature-controlled area for cold- and hot-temperature testing is accepted, but accomplish such transferwith minimum (or no) disturbance of container contents.6.1.1 Cold-Temperature Storage EnvironmentSubject thesample container to a 15-day time interval at 8 6 2C (17 63F).
13、 Conduct this cold test interval during the period 90 to 120days after start of the storage stability test time.1This test method is under the jurisdiction of ASTM Committee F07 onAerospace and Aircraft and is the direct responsibility of Subcommittee F07.07 onQualification Testing of Aircraft Clean
14、ing Materials.Current edition approved Mar. 10, 2003. Published March 2003. Originallyapproved in 1987. Last previous edition approved in 1999 as F 1105 95 (1999)e1.2Available from Standardization Documents Order Desk, Bldg. 4 Section D, 700Robbins Ave., Philadelphia, PA 19111-5094 Attn: NPODS.1Copy
15、right ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.6.1.2 Hot-Temperature Storage EnvironmentSubject thesample container to a 15-day time interval at 32 6 2C (90 65F). Conduct this hot test interval after 270 days of elapsedtest time but 60 d
16、ays before the termination of the storage test.6.1.3 Completion of TestAfter 12 months storage testtime, carefully remove the sample container (if necessary),without agitation, rolling, or inversion, from the storage areaand place in a room, in a stable location for 48 6 1hatatemperature of 22 to 27
17、C (71 to 80F). At the end of 48 h,remove the top of the container and examine the internalsurface for corrosion or sediment. Disregard discoloration ofthe interior surface of the container. Take samples of theproduct and test in accordance with the relevant specificationor contract requirements.7. P
18、recision and Bias7.1 No statement can be made relating to precision and biassince the only nonvariables are the environmental conditions.The pass or fail requirement is determined by the subsequenttests called up by the specification or contract.8. Keywords8.1 cold test period; hot test period; solv
19、ent-based cleaningcompounds; storage stabilityASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, a
20、nd the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revis
21、ion of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you s
22、houldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).F1105032
