1、LIST OF COMMITTEE D-19 DISCONTINUED AND SUPERSEDEDSTANDARDSD 51485 (1989), Test Method for Hydroxide Ion in Water.This test method covers the volumetric determination of freehydroxide ion in water. This test method was discontinued in1996.D 99271 (1978), Test Method for Nitrate Ion in Water. Thistes
2、t method covers the determination of nitrate ion in water.This test method was discontinued in 1984 and replaced byTest Method D 3867, Test Methods for Nitrite-Nitrate in Water.This test method was discontinued in 1984.D 99358 (1982)e1, Test Methods for Sulfate-Reducing Bac-teria in Water and Water-
3、Formed Deposits. These methodscover the detection of the presence of sulfate-reducing bacteriawhen present in deposits or water samples and the estimationof the number of bacteria present. These methods werediscontinued in 1987 and replaced by Test Methods D 4412,Test Methods for Sulfate-Reducing Ba
4、cteria in Water andWater-Formed Deposits.D 112860 (1974), Method for Identification of Types ofMicroorganisms and Microscopic Matter in Water and WasteWater. This method covers the procedure for identification bymicroscopical examination of bacterial cells, mold filaments,algae, protozoa and other s
5、mall animals, and such particles ofinert material as may be found in water and wastewater. Thismethod was discontinued in 1982.D 125467 (1974), Test Methods for Nitrite Ion in Water.These test methods cover the determination of nitrite ion inwater. Two methods are given as follows: Method A (Colori-
6、metric Method) and Method B (Volumetric Method). These testmethods were discontinued in 1981.D 133984, Test Methods for Sulfite Ion in Water. These testmethods cover the volumetric determination of sulfite ion inwater. These test methods were discontinued in 1990.D 142768 (1974), Test Methods for Re
7、sidual Chlorine inWaste Water. These test methods cover procedures for thedetermination of residual chlorine in wastewater. These testmethods were discontinued in 1982 and replaced by TestMethods D 1253, Test Method for Residual Chlorine in Water.D 142882e1, Test Methods for Sodium and Potassium inW
8、ater and Water-Formed Deposits by Flame Photometry.These test methods cover the determination of sodium andpotassium in water and water-formed deposits using directmeasuring-type flame photometers. These test methods werediscontinued in 1990.D 158860 (1974), Test Methods for Dissolved and GaseousHyd
9、rogen in Water. These test methods cover the collectionand measurement of dissolved and gaseous hydrogen in water.These test methods were discontinued in 1984.D 158980, Test Methods for Dissolved Oxygen in WasteWater. These test methods cover the determination of dissolvedoxygen in waste water in th
10、e presence of certain interferingsubstances. Common interfering substances which may occurin such water are nitrites, ferrous iron, organic material,sulfites, or other oxidizing or reducing substances. Provisionsincorporated in this method will, in most cases, lessen theinterference of such substanc
11、es in the determination of dis-solved oxygen. These test methods were discontinued in 1981and replaced by ASTM Methods D 888, Test Methods forDissolved Oxygen in Water.D 159060 (1977)e2, Test Method for Surface Tension ofWater. This test method covers quantitative measurement of thesurface tension o
12、f water and waste water. The test method isbased on instrumental measurement by the ring method andoffers the most precise and accurate determination. This testmethod was discontinued in 1995.D 169073, Test Method for Gamma Radioactivity of Water.This test method covers the measurement of gamma radi
13、oac-tivity of water. It is applicable to gamma emitters in the energyrange above 0.1 MeV and in the concentration range of 102to105Ci/mL of radioactively homogeneous water. This testmethod was discontinued in 1981.D 188878e2, Test Methods for Particulate and DissolvedMatter, Solids, or Residue in Wa
14、ter. These test methods coverthe determination of particulate, dissolved, and total matter,sometimes referred to as the suspended, dissolved, and totalsolids, in water. These test methods were discontinued in 1991.D 194280e1, Test Method for Morpholine in Water. Thistest method covers a colorimetric
15、 procedure for the determi-nation of morpholine in boiler feedwater and steam conden-sate. This test method was discontinued in 1990 and replacedby Test Method D 4983 for Cyclohexylamine, Morpholine, andDiethylaminoethanol in Water and Condensed Steam by DirectAqueous Injection Gas Chromatography.D
16、203268 (1982)e1, Specification for Deuterium Oxide.This specification covers minimum requirements for deuteriumoxide (D2O) to be used as a moderator in heavy watermoderated reactors. This specification was discontinued in1988.D 203373 (1979), Test Method for Consumption of Potas-sium Permanganate by
17、 Impurities in Deuterium Oxide. Thistest method covers a titrimetric measurement of the consump-tion of potassium permanganate by impurities in deuteriumoxide. It is one of the required methods intended for use inestablishing whether the deuterium oxide is of sufficient purityto meet specifications.
18、 This test method was discontinued in1988.1D 203468 (1975), Method for Open Channel Flow Mea-surement of Water and Waste Water by Weirs. This methodcovers the measurement of the rate of flow of water and wastewater in open channels or streams at or near the ground surfaceusing the triangular (V-notc
19、h), rectangular and trapezoidal typeweirs having end and bottom contractions. This method wasdiscontinued in 1984.D 203768 (1973), Test Method for Evaluating Toxicity ofWaters to Diatoms. This is a nonreferee batch method forevaluating the inhibitory toxicity of wastewaters to diatoms. Itcan be perf
20、ormed with standard reference water and referencechemicals, and provides information on the toxicity of asample under prescribed experimental conditions. It is notintended to be a measure of acute toxicity for aquatic life. Thistest method was discontinued in 1981.D 203883, Test Method for Radioacti
21、ve Barium in Water.This test method covers the measurement of radioactive bariumcontained in water in concentrations above 107Ci/L. This testmethod was discontinued in 1989.D 203983, Test Method for Radioactive Manganese inWater. This method covers the measurement of radioactivemanganese in water in
22、 concentrations above 103Ci/L (37disintegrations/s L). It is limited to the manganese radioiso-topes of masses 54 and 56. This method was discontinued in1988.D 218481, Method of Testing Deuterium Oxide. Thismethod covers the measurement of the isotopic composition ofhydrogen in deuterium oxide (heav
23、y water) which is nominally99.75 atom percent deuterium (D), equal to D/(D + H) 3 100.The primary use of the heavy water is as a moderator inproduction, power, or research reactors in which a fissionablenuclide is consumed. In such reactors the percentage ofdeuterium in the heavy water usually excee
24、ds 95 %. Thismethod was discontinued in 1988.D 232780e1, Test Method for Mono- and Dioctadecy-lamines in Water. This test method covers a colorimetricprocedure for the determination of octadecylamine and diocta-decylamine in steam or steam condensate. This test methodwas discontinued in 1990 and rep
25、laced by Test Method D 4983for Cyclohexylamine, Morpholine, and Diethylaminoethanolin Water and Condensed Steam by Direct Aqueous InjectionGas Chromatography.D 233380, Test Method for Thorium in Water. This methodcovers a colorimetric determination of microgram amounts ofthorium in water and waste w
26、ater. It is sensitive to less than 13 109g of thorium in1gofwater. This method wasdiscontinued in 1988.D 233488e1, Test Methods for Radioactive Iodine in Water.These test methods cover the determination of radioactiveiodine in water in concentrations greater than 100 pCi/L.Concentration of the sampl
27、e can increase the sensitivity of thetest methods. Procedures for heterogeneous exchange, distilla-tion, and solvent extraction are included. These test methodswere discontinued in 1992.D 245869 (1975), Method of Flow Measurement of Waterby the Venturi Meter Tube. This method covers the measure-ment
28、 of the rate of flow of water in pipelines using the HerschelStandard Venturi meter tube. This method was discontinued in1983.D 245972 (1981)e1, Test Method for Gamma Spectrometryof Water. This method covers the measurement by means ofgamma spectrometry of gamma radioactivity of water. It isapplicab
29、le to nuclides emitting gamma rays with energiesgreater than 0.1 MeV. The count rate of the sample to becounted should be in the range from 105counts per minute totwice the background count rate. This method was discontin-ued in 1988.D 246169 (1982), Test Method for Iron-59 in Water. Thismethod cove
30、rs the measurement of radioactive iron containedin water in concentrations above 0.1 Ci/L. It is limited bychoice of radiation detector to the iron radioisotope of mass 59produced in nuclear reactors and which may also be used as atracer. Modifications in the analytical method are included formeasur
31、ement at higher and lower concentrations. This methodwas discontinued in 1988.D 247070 (1982), Method for Measurement of DelayedNeutron Emitting Fission Products in Nuclear Reactor CoolantWater During Reactor Operation. This method covers thedetection and measurement of delayed neutron-emitting fiss
32、ionproducts contained in nuclear reactor coolant water while thereactor is operating, and is limited to the measurement of thedelayed neutron-emitting bromine isotope of mass 87 and thedelayed neutron-emitting iodine isotope of mass 137. This testmethod was discontinued in 1989.D 247681 (1987), Test
33、 Method for Tritium in Water. Thistest method covers the liquid scintillation measurement oftritium radioactivity in water, T2O or HTO. The upper limit ofanalysis without dilution is dependent upon the efficiency ofthe scintillator solution and the overload characteristics of theinstrument. The mini
34、mum detectable activity is 0.4 pCi/mL fora 10-mL sample counted for 100 min in a counter where thebackground is 20 cpm and the efficiency is 18 %. This testmethod was discontinued in 1992 and replaced by Test MethodD 4107 for Tritium in Drinking Water.D 257786, Test Method for Radioactive Cesium in
35、Water.This test method covers the determination of radioactivecesium in water in concentrations greater than 1 Ci/L. Thistest method was discontinued in 1989.D 279083e1, Methods of Analysis of Solvent Systems Usedfor Removal of Water-Formed Deposits. These methods coverthe analysis of both the solve
36、nts and the deposit constituents inthe solvents used for the chemical cleaning of industrialequipment. Included are methods for determining the concen-trations of the principal active ingredients in the solvents andthe dissolved deposit constituents derived from corrosionproducts and scale formation
37、s. Procedures are also included foralkaline boil-out solutions, such as sodium carbonate andsodium hydroxide.D 290980e1, Test Method for Cyclohexylamine in Water.This test method covers a colorimetric procedure for thedetermination of cyclohexylamine in boiler feedwater andsteam condensate. This tes
38、t method was discontinued in 1990and replaced by Test Method D 4983 for Cyclohexylamine,Morpholine, and Diethylaminoethanol in Water and CondensedSteam by Direct Aqueous Injection Gas Chromatography.2D 291085, Practice for Concentration and Recovery ofOrganic Matter from Water by Activated Carbon. T
39、his practiceprovides a technique for the concentration and recovery oforganic matter from water for analytical purposes. The organicmatter is adsorbed from the water onto activated carbon whichis solvent-extracted to recover the organic constituents. Thispractice was discontinued in 1993.D 308575 (1
40、983), Practice for Measurement of Low-LevelActivity in Water. This practice describes the process necessaryto obtain meaningful data from water samples that contain lowlevels ( 10 pCi) of radioactivity. This practice was discontin-ued in 1989.D 308685 (1990), Test Method for Organochlorine Pesti-cid
41、es in Water. This test method covers the gas chromato-graphic determination of various organochlorine pesticides,including some pesticidal degradation products and relatedcompounds in water and waste water. This test method wasdiscontinued in 1996 and replaced by Test Method D 5812,Test Method for D
42、etermination of Organochlorine Pesticides inWater by Capillary Column Gas Chromatography.D 325077 (1982)e2, Test Method for Total Oxygen Demandin Water. This test method covers the determination of totaloxygen demand in the ranges from 10 to 200, 25 to 500, 50 to1000 mg/L, in water including brackis
43、h waters and brines.Larger concentrations may be determined by suitable dilutionof the sample. This test method was discontinued in 1991.D 331586, Test Method for Radioactive Zirconium inWater. This test method covers the determination of radioactivezirconium in water in concentrations greater than
44、100 pCi/L.This test method was discontinued in 1989.D 332779e1, Test Methods for Analysis of Selected Ele-ments in Waterborne Oils. These test methods cover thedetermination of nitrogen (0.01 to 1 weight %), sulfur (above0.0010 weight %), nickel (0.5 ppm to 0.1 weight %), andvanadium (0.5 ppm to 0.1
45、 weight %) in waterborne oils for thepurpose of aiding in the identification of such oils.D 335783e1, Test Method for Radioactive Nickel in Water.This test method covers the measurement of radioactive nickelin water at concentrations above 1100 pci/L (40.7disintegrations/sL). It is limited to the ni
46、ckel isotope of mass63, which is produced in nuclear reactor materials. This testmethod was discontinued in 1991.D 347885e1, Test Method for Chlorinated Phenoxy AcidHerbicides in Water. This test method covers a gas chromato-graphic procedure for the quantitative determination of chlori-nated phenox
47、y acid herbicides in water. The compounds2,4-D2,4-dichlorophenoxyacetic acid, silvex 2-(2,4,5-trichlororophenoxy) propionic acid, and 2,4,5-T 2,4,5-trichlorophenoxy acetic acid and similar chemicals such aschlorinated organic acids may be determined by this procedure.This test method was discontinue
48、d in 1992 and replaced byTest Method D 5317 for Determination of Chlorinated OrganicCompounds in Water by Gas Chromatography with an ElectronCapture Detector.D 356083e1, Test Method for Oxygen Demand in Water byCombustion-Infrared Analysis. This test method covers thedetermination of oxygen demand i
49、n the range from 25 to 300mg/L in water. Higher oxygen demands may be determined bysuitable dilution of the sample. This test method was discon-tinued in 1991.D 358983e1, Test Method for Total Nitrogen in Water byMicrocoulometry. This test method covers the determination ofthe total nitrogen in water in concentrations from 0.5 to 100mg/L. Higher nitrogen concentration may be determined byusing appropriate diluents. This test method is applicable towater samples containing less than 20 % halogen or 5 % sulfur.This test method was discont
