1、DD CEN/TS14243:2010ICS 13.030.50; 83.160.01NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWDRAFT FOR DEVELOPMENTMaterials producedfrom end of life tyres Specification ofcategories based ontheir dimension(s)and impuritiesand methods fordetermining theirdimension(s) andimpurities
2、This Draft for Developmentwas published under theauthority of the StandardsPolicy and StrategyCommittee on 31 May2010. BSI 2010ISBN 978 0 580 53713 4Amendments/corrigenda issued since publicationDate CommentsDD CEN/TS 14243:2010National forewordThis Draft for Development is the UK implementation of
3、CEN/TS14243:2010.This publication is not to be regarded as a British Standard.It is being issued in the Draft for Development series of publications andis of a provisional nature. It should be applied on this provisional basis,so that information and experience of its practical application can beobt
4、ained.Comments arising from the use of this Draft for Development arerequested so that UK experience can be reported to the internationalorganization responsible for its conversion to an international standard.A review of this publication will be initiated not later than 3 years afterits publication
5、 by the international organization so that a decision can betaken on its status. Notification of the start of the review period will bemade in an announcement in the appropriate issue of Update Standards.According to the replies received by the end of the review period,the responsible BSI Committee
6、will decide whether to support theconversion into an international Standard, to extend the life of theTechnical Specification or to withdraw it. Comments should be sent tothe Secretary of the responsible BSI Technical Committee at BritishStandards House, 389 Chiswick High Road, London W4 4AL.The UK
7、participation in its preparation was entrusted to TechnicalCommittee PRI/73, Industrial rubber products.A list of organizations represented on this committee can be obtained onrequest to its secretary.This publication does not purport to include all the necessary provisionsof a contract. Users are r
8、esponsible for its correct application.Compliance with a British Standard cannot confer immunityfrom legal obligations.DD CEN/TS 14243:2010TECHNICAL SPECIFICATION SPCIFICATION TECHNIQUE TECHNISCHE SPEZIFIKATION CEN/TS 14243 April 2010 ICS 13.030.50; 83.160.01 Supersedes CWA 14243:2002English Version
9、 Materials produced from end of life tyres - Specification of categories based on their dimension(s) and impurities and methods for determining their dimension(s) and impurities Matriaux produits partir de pneumatiques en fin de vie - Spcification de catgories bases sur leur(s) dimension(s) et impur
10、ets et mthodes pour dterminer leur(s) dimension(s) et impurets Materialen aus Altreifen - Festlegung von Klassen anhand ihrer Abmessung(en) und Verunreinigungen und Verfahren zur Bestimmung ihrer Abmessung(en) und Verunreinigungen This Technical Specification (CEN/TS) was approved by CEN on 4 Januar
11、y 2010 for provisional application. The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard. CEN members are req
12、uired to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in parallel to the CEN/TS) until the final decision about the possible co
13、nversion of the CEN/TS into an EN is reached. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
14、 Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN All rights of exploitation in any form and
15、 by any means reserved worldwide for CEN national Members. Ref. No. CEN/TS 14243:2010: EDD CEN/TS 14243:2010CEN/TS 14243:2010 (E) 2 Contents Page Foreword 5Introduction .61 Scope 82 Normative references 83 Terms and definitions .84 Categories of products, based mainly on their dimensions, produced f
16、rom end-of-life tyres . 114.1 Categories . 114.2 Testing programme 125 Determination of dimensions for granulates and powders and for chips considered as very large granulates 125.1 General . 125.2 Preparation of the sampling plan 125.2.1 Principles of correct sampling 125.2.2 General . 135.2.3 Samp
17、ling plan . 135.2.4 Definition of lot size 135.2.5 Sampling point and apparatus 135.2.6 Size of a sample increment 145.2.7 Number of increments 145.2.8 Metrological characteristics of sampling . 145.2.9 Visual assessment 145.3 Storage and transport of sample(s) 155.4 Preparation of the laboratory sa
18、mple(s) and test portion(s) 155.4.1 Principles of correct sample preparation and sample division . 155.4.2 Test portion preparation 155.4.3 Apparatus for sample division 155.4.4 Procedure 165.5 Particle size analysis 165.5.1 General principles. 165.5.2 Sieves . 165.5.3 Flat brush . 175.5.4 Mechanica
19、l vibrating equipment . 175.5.5 Scales . 175.5.6 Procedure 175.5.7 Calculation . 175.6 Metrological characteristics 185.7 Test Report 186 Determination of dimensions for shreds and cuts and for chips considered as very small shreds 186.1 Definition of shreds 186.2 Principles of sampling . 196.3 Prep
20、aration of the sampling plan for determining dimensions . 196.4 Procedure for taking the field sample and producing the laboratory sample(s) . 206.5 List of symbols and abbreviations 206.6 Principle of determining the dimension(s) . 216.7 Equipment . 226.8 Procedure for quantification of maximum pro
21、jected length (manual) 22DD CEN/TS 14243:2010CEN/TS 14243:2010 (E) 3 6.9 Metrological characteristics . 236.10 Measurement report 237 Determination of characteristics of the separated fractions steel and textiles 247.1 General . 247.2 Preparation of sampling plan for steel and textiles and method fo
22、r sampling . 247.2.1 Principle of sampling 247.2.2 Sampling plan 247.2.3 Definition of a lot and determining lot size . 257.2.4 Determination of the number of increments . 257.2.5 Determination of minimum sample size 257.2.6 Determination of the minimum increment size 257.3 Handling and storage of s
23、amples 267.4 Determination of characteristic of the separated fractions steel and textiles by manual sorting of all components. 267.4.1 General principles . 267.4.2 Equipment 267.4.3 Procedure . 267.5 Calculation . 277.6 Metrological characteristics . 277.7 Report . 27Annex A (normative) Evaluation
24、of protruding filaments for shreds and cuts and chips considered as very small shreds . 28A.1 General . 28A.2 Principle of the evaluation 28A.3 Sampling. 28A.4 List of symbols and abbreviations 28A.5 Principle for determining dimension(s) by image analysis 29A.6 Equipment 29A.7 Procedure . 29A.8 Met
25、rological characteristics . 30A.9 Measurement report 30Annex B (normative) Determination of free steel content for granulates and powders and chips considered as very large granulates by the method of magnetic separation . 32B.1 General . 32B.2 Principle of the determination 32B.3 Sampling. 32B.4 Eq
26、uipment 32B.5 Procedure . 32B.6 Calculation . 33B.7 Metrological characteristics . 33B.8 Measurement report 33Annex C (normative) Determination of free textile content for granulates and powders and chips considered as very large granulates by the method of the “small ball“ agglomeration . 35C.1 Gen
27、eral . 35C.2 Principle of the determination 35C.3 Sampling. 35C.4 Equipment 35C.5 Procedure . 35C.6 Calculations . 36C.7 Metrological characteristics . 36C.8 Measurement report 36Annex D (normative) Determination of other impurities content for granulates and powders and chips considered as very lar
28、ge granulates by the method of a saline solution . 38D.1 General . 38D.2 Principle of the determination 38D.3 Sampling. 38D.4 Equipment 38DD CEN/TS 14243:2010CEN/TS 14243:2010 (E) 4 D.5 Procedure 39D.6 Calculations . 39D.7 Metrological characteristics 39D.8 Measurement report . 40Annex E (informativ
29、e) Example of applications of Clause 7 to steel and textiles . 41E.1 Example for textiles 41E.1.1 Sampling 41E.1.2 Sample . 41E.1.3 Separation of fractions textile, steel, rubber . 41E.1.4 Separation of steel using hand magnet . 42E.1.5 Sorted fractions 42E.1.6 Results . 42E.2 Example on steel. 42E.
30、2.1 Sampling 42E.2.2 Sample . 42E.2.3 Separation of fractions . 43E.2.4 Separation of steel using hand magnet . 43E.2.5 Sorted fractions 43E.2.6 Results . 44Annex F (informative) Example of scoop . 45Annex G (informative) Sieving 46Bibliography . 48DD CEN/TS 14243:2010CEN/TS 14243:2010 (E) 5 Forewor
31、d This document (CEN/TS 14243:2010) has been prepared by Technical Committee CEN/TC 366 “Project Committee - Tyre recycling”, the secretariat of which is held by UNI. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENE
32、LEC shall not be held responsible for identifying any or all such patent rights. This document supersedes CEN/CWA 14243:2002. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to announce this Technical Specification: Austria
33、, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. DD
34、CEN/TS 14243:2010CEN/TS 14243:2010 (E) 6 Introduction This Technical Specification is the first in a foreseen series of Technical Specifications. Such series would cover the testing programmes needed to characterise each product category as shown on the figure below. “in the field“ “in the field“Typ
35、ical scheme for a testing programmeconcerning several characteristicswith testing steps in the field (1-2-3)and in the laboratory (3-4-5-6-7)Testing Programme on characteristics A, B, C, DA = Characteristic of the “dimension“ typeB, C = Characteristic of the “content“ typeD = Characteristic of the “
36、apparent density“ typeDefine the Sampling Planfor Properties A, B, C,DTake a field sample for characteristics A, B, Cin accordance with the Sampling PlanWORK FILELaboratory sample and recordfor characteristics A, B, C Test sample and test portionpreparation for characteristic A WORK FILE Test sample
37、 and test portionpreparation for characteristics B, C WORK FILE Customer and/or manufacturer evaluates the dataand report against theTesting Programme ObjectivesWORK FILES collection - Productionof the overall Measurements - Testing Report for characteristics A, B, C, DExtraction for characteristics
38、 B, CWORK FILE Analysis for characteristics B, CWORK FILE Overall Report of Measurements -Testing for Properties A, B, C, D Quantification for characteristic AWORK FILE Quantification for characteristic DWORK FILE Test sample and test portionpreparation for characteristic D WORK FILE Storage, Transp
39、ort,storageWORK FILE Storage, Transport,storageWORK FILE Laboratory sample and recordfor characteristic DTake a field sample for characteristic Din accordance with the Sampling PlanWORK FILEClustomer and/or manufacturer defines the Testing Programmeand its objectives, which are the Term of Reference
40、for the testing laboratory(ies)1234567“in the laboratory“ “in the laboratory“Figure 1 Typical scheme for a testing programme concerning several characteristics with testing steps in the field and in the laboratory End-of-life tyres consist mainly of passenger and commercial vehicle tyres, and truck
41、tyres manufactured for distribution in the European market. Products from end-of-life tyres are used as a secondary raw material finding a wide range of applications. The principal categories of materials from end-of-life tyres are defined on the basis of their dimension(s) according to this Technic
42、al Specification. Determination of additional dimensions/impurities according to the test methods specified in normative Annexes A, B, C and D may be performed if required by agreement between the producer and the customer or at the producers own will. European Standards are needed for the productio
43、n, trade and use of the materials from end-of-life tyres. They are also useful for buyers of materials, regulators, controllers and laboratories. DD CEN/TS 14243:2010CEN/TS 14243:2010 (E) 7 The materials produced at different stages of the treatment processes, primarily by size reduction, of end-of-
44、life tyres are as follows: cuts: typically 300 mm and above; shreds: typically 20 mm 400 mm; chips: typically 10 mm 50 mm; granulates: typically 0,8 mm 20 mm; powders: typically under 0,8 mm; steel; textiles. They may be distinguished mainly according to their dimension(s). DD CEN/TS 14243:2010CEN/T
45、S 14243:2010 (E) 8 1 Scope This Technical Specification provides definitions for the categories of materials produced from end-of-life tyres based on their dimension(s) or impurities. It also provides test methods for the determination of the dimension(s) of the materials produced from all categorie
46、s of end-of-life tyres at all steps of the treatment process as well as for the determination of impurities. The test methods described in this Technical Specification include sample collection and the preparation of a representative sample based on a sampling plan for the purpose of determining dim
47、ensions and impurities. This Technical Specification does not cover the operational performance or fitness for use of the materials which are deemed to be a function of agreement between the producer and the customer. NOTE This Technical Specification does not cover downstream products prepared from
48、 the materials, including reclaimed or devulcanized rubber, surface-modified powders and pyrolytic output. This Technical Specification does not purport to address safety concerns associated with its use. It is the responsibility of the user of this Technical Specification to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2
