1、BS EN1097-7:2008ICS 91.100.15NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBRITISH STANDARDTests for mechanicaland physicalproperties ofaggregatesPart 7: Determination of the particledensity of filler Pyknometer methodLicensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 20/
2、07/2009 03:14, Uncontrolled Copy, (c) BSIThis British Standardwas published under theauthority of the StandardsPolicy and StrategyCommittee on 30 April2009 BSI 2009ISBN 978 0 580 58931 7Amendments/corrigenda issued since publicationDate CommentsBS EN 1097-7:2008National forewordThis British Standard
3、 is the UK implementation of EN 1097-7:2008. Itsupersedes BS EN 1097-7:1999 which is withdrawn.The UK participation in its preparation was entrusted to TechnicalCommittee B/502/6, Test methods.A list of organizations represented on this committee can be obtained onrequest to its secretary.This publi
4、cation does not purport to include all the necessary provisionsof a contract. Users are responsible for its correct application.Compliance with a British Standard cannot confer immunityfrom legal obligations.Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 20/07/2009 03:14, Uncontrolled Copy,
5、(c) BSIBS EN 1097-7:2008EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN 1097-7March 2008ICS 91.100.15 Supersedes EN 1097-7:1999 English VersionTests for mechanical and physical properties of aggregates -Part 7: Determination of the particle density of filler - PyknometermethodEssais pour dterminer
6、 les caractristiques mcaniques etphysiques des granulats - Partie 7: Dtermination de lamasse volumique absolue du filler - mthode aupicnomtrePrfverfahren fr mechanische und physikalischeEigenschaften von Gesteinskrnungen - Teil 7:Bestimmung der Rohdichte von Fller - Pyknometer-VerfahrenThis European
7、 Standard was approved by CEN on 4 February 2008.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concern
8、ing such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own lan
9、guage and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Lux
10、embourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2008 CEN All right
11、s of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 1097-7:2008: ELicensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 20/07/2009 03:14, Uncontrolled Copy, (c) BSIBS EN 1097-7:2008EN 1097-7:2008 (E) 2 Contents Page Foreword3 1 Scope 4 2 Normative r
12、eferences 4 3 Terms and definitions .4 4 Principle5 5 Materials .5 6 Apparatus .5 7 Preparation of test portion6 8 Procedure .6 9 Calculation and expression of results.6 10 Test report 7 Annex A (normative) Calibration of the pyknometer.8 Annex B (normative) Procedure for the determination of the de
13、nsity of the liquid used to determine the particle density of the filler 10 Annex C (informative) Precision 12 Bibliography 13 Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 20/07/2009 03:14, Uncontrolled Copy, (c) BSIBS EN 1097-7:2008EN 1097-7:2008 (E) 3 Foreword This document (EN 1097-7:20
14、08) has been prepared by Technical Committee CEN/TC 154 “Aggregates”, the secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2008, and conflicting natio
15、nal standards shall be withdrawn at the latest by September 2008. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supers
16、edes EN 1097-7:1999. This European Standard forms part of a series of standards for tests for mechanical and physical properties of aggregates. Test methods for other properties of aggregates will be covered by parts of the following European Standards: EN 932, Tests for general properties of aggreg
17、ates EN 933, Tests for geometrical properties of aggregates EN 1367, Tests for thermal and weathering properties of aggregates EN 1744, Tests for chemical properties of aggregates EN 13179, Tests for filler aggregate used in bituminous mixtures The other parts of EN 1097 will be: Part 1: Determinati
18、on of the resistance to wear (micro-Deval) Part 2: Methods for the determination of resistance to fragmentation Part 3: Determination of loose bulk density and voids Part 4: Determination of the voids of dry compacted filler Part 5: Determination of the water content by drying in a ventilated oven P
19、art 6: Determination of particle density and water absorption Part 8: Determination of the polished stone value Part 9: Determination of the resistance to wear by abrasion from studded tyres - Nordic test Part 10: Determination of water suction height According to the CEN/CENELEC Internal Regulation
20、s, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherland
21、s, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 20/07/2009 03:14, Uncontrolled Copy, (c) BSIBS EN 1097-7:2008EN 1097-7:2008 (E) 4 1 Scope This standard describes the reference method u
22、sed for type testing and in cases of dispute for the determination of the particle density of filler by means of a pyknometer. For other purposes, in particular factory production control, other methods may be used provided that an appropriate working relationship with the reference method has been
23、established. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 932-2, Tes
24、ts for general properties of aggregates - Part 2: Methods for reducing laboratory samples EN 932-5, Tests for general properties of aggregates - Part 5: Common equipment and calibration ISO 3507, Laboratory glassware - Pyknometers 3 Terms and definitions For the purposes of this document, the follow
25、ing terms and definitions apply. 3.1 laboratory sample reduced sample derived from a bulk sample for laboratory testing 3.2 test portion sample used as a whole in a single test 3.3 test specimen sample used in a single determination when a test method requires more than one determination of a proper
26、ty 3.4 constant mass successive weighings after drying at least 1 h apart not differing by more than 0,1 % NOTE In many cases constant mass can be achieved after a test portion has been dried for a pre-determined period in a specified oven (see 6.6) at (110 5) C. Test laboratories can determine the
27、time required to achieve constant mass for specific types and sizes of sample dependent upon the drying capacity of the oven used. 3.5 particle density of filler mass per volume unit of filler excluding any trapped air 3.6 filler aggregate aggregate, most of which passes a 0,063 mm sieve, which can
28、be added to construction materials to provide certain properties Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 20/07/2009 03:14, Uncontrolled Copy, (c) BSIBS EN 1097-7:2008EN 1097-7:2008 (E) 5 4 Principle The pyknometer method is a well known method for determining the volume of irregularly
29、 formed samples, e.g., aggregate. When the mass of the sample is known, the density can be calculated. The principle is based on the replacement of a certain amount of liquid of known density with the test portion. A pyknometer with known volume, containing the test portion, is topped up with the li
30、quid. The volume of this liquid is calculated by dividing the mass of the liquid added by the liquid density. The volume of the test portion is then calculated by subtraction of this volume from the pyknometer volume. 5 Materials 5.1 Suitable liquid, in which the filler does not dissolve and with wh
31、ich the filler does not react. NOTE Water, denatured ethanol, redistilled kerosene or toluene have been found to be suitable for different types of filler. 5.2 Demineralized water, boiled and cooled, for calibration (see Annex A). 5.3 Acetone, for calibration (see Annex A). 6 Apparatus 6.1 All appar
32、atus, unless otherwise stated, shall conform to the general requirements of EN 932-5. 6.2 Pyknometer, of nominal capacity 50 ml, conforming to ISO 3507. The stopper shall be concave at the underside, and shall include a thick-walled capillary (riser pipe) whose top has been ground to a level surface
33、. NOTE The pyknometer can be fitted with a thermometer. 6.3 Water bath, capable of being maintained at (25 0,1) C. 6.4 Balance, accurate to the nearest 0,001 g for the determination. 6.5 Balance, accurate to the nearest 0,000 1 g for calibration (see Annex A). 6.6 Drying oven, thermostatically contr
34、olled to maintain a temperature of (110 5) C. 6.7 Desiccator, filled with an appropriate amount of desiccant. 6.8 Vacuum desiccator. 6.9 Vacuum pump, capable of achieving a residual pressure of less than 3,0 kPa. 6.10 Spatula. 6.11 Test sieve, 0,125 mm and suitable receiver. Licensed Copy: Wang Bin,
35、 ISO/EXCHANGE CHINA STANDARDS, 20/07/2009 03:14, Uncontrolled Copy, (c) BSIBS EN 1097-7:2008EN 1097-7:2008 (E) 6 7 Preparation of test portion Reduce the size of the laboratory sample in accordance with EN 932-2. The test portion before drying shall have a minimum mass of 50 g. Dry the test portion
36、at (110 5) C to constant mass and leave it to cool down in the desiccator (see 6.7) for at least 90 min. Check the test portion for the presence of lumps and, if present, pulverize them carefully with the spatula and mix the pulverized lumps. Dry sieve the filler using the 0,125 mm sieve. Retain all
37、 the particles which pass the sieve. 8 Procedure Carry out the determination of density using three separate test specimens, using a calibrated pyknometer or pyknometers (see Annex A) and a liquid of a known density (see Annex B). Carry out all weighing with an accuracy of 0,001 g. Proceed as follow
38、s for each of the three determinations. Weigh the clean and dry pyknometer with stopper (mo). Fill the pyknometer with (10 1) g of filler taken from the test portion and weigh it again (m1). Add sufficient liquid to completely submerge the test specimen. NOTE Add the liquid very carefully allowing i
39、t to percolate through the filler in the pyknometer. Put the stopper in the pyknometer, place the pyknometer in the vacuum desiccator and evacuate it with the vacuum pump in approximately 5 min to less than 3,0 kPa. Leave the pyknometer for at least 30 min in the vacuum desiccator at a pressure less
40、 than 3,0 kPa. After restoring the air pressure in the desiccator, take the pyknometer out and fill it with liquid. Place the pyknometer without stopper in the water bath at (25 0,1) oC so that the top protrudes between 2 mm to 3 mm above the water level in the bath. After 60 min, put the stopper in
41、 the pyknometer causing an amount of liquid to come out of the capillary. Dry the top of the capillary and remove the pyknometer from the water bath. Quickly cool the pyknometer in cold (running) water, to prevent liquid expanding out of the capillary due to warm handling. Carefully dry the outside
42、and weigh the pyknometer filled with test specimen and liquid (m2). 9 Calculation and expression of results Calculate the particle density of the filler, in megagrams per cubic metre, in accordance with the following equation: flmmVmm=1021(1) where m0 is the mass of the empty pyknometer with stopper
43、, in grams; m1 is the mass of the pyknometer with the filler test portion, in grams; Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 20/07/2009 03:14, Uncontrolled Copy, (c) BSIBS EN 1097-7:2008EN 1097-7:2008 (E) 7 m2 is the mass of the pyknometer with the filler test portion, topped up with
44、liquid (see 5.1), in grams; V is the volume of the pyknometer, in millilitres (see Annex A); l is the density of liquid at 25 C, in megagrams per cubic metre (see Annex B); fis the particle density of the filler at 25 C, in megagrams per cubic metre. Calculate the particle density of the filler as t
45、he mean of the three determinations, and round off to the nearest 0,01 Mg/m3. NOTE A statement on the precision of this test is given in Annex C. 10 Test report 10.1 Required data The test report shall include the following information: a) particle density fof the filler; b) reference to this Europe
46、an Standard (EN 1097-7:2008); c) brand name or type/source of the filler; d) name and location of the sample source; e) liquid used for the determination and its density l(see Annex B); f) date of the determination. 10.2 Optional data The test report can include the following information: a) descrip
47、tion of the material; b) description of the sampling procedure; c) weighing data and the densities from the three individual determinations. Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 20/07/2009 03:14, Uncontrolled Copy, (c) BSIBS EN 1097-7:2008EN 1097-7:2008 (E) 8 Annex A (normative) Ca
48、libration of the pyknometer A.1 General The pyknometer (see 6.2) shall be calibrated by determining its volume. A.2 Procedure A.2.1 Clean the pyknometer by thoroughly rinsing it several times with acetone (see 5.3) and dry it. A.2.2 Weigh the pyknometer together with the stopper (mO). Carry out both
49、 weighings with an accuracy of 0,0001 g. A.2.3 Fill the pyknometer with demineralized water (see 5.2). A.2.4 Place the pyknometer (without stopper) in the water bath at (25 0,1) oC, so that the top protrudes between 2 mm and 3 mm above the water level in the bath. A.2.5 After 60 min, place the stopper on the pyknometer, causing an amount of water to come out of the capillary. A.2.6 Dry the top of the capillary and remove the pyknometer from the water bath. A.2.7 Quickly cool the pyknometer in cold (running) water, to prevent demineralized
