1、| | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | BRITISH STANDARD BS EN 1162 : 1997 The Eur
2、opean Standard EN 1162 : 1996 has the status of a British Standard ICS 59.040 NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW Feather and down Test methods Determination of the oxygen index numberBS EN 1162 : 1997 This British Standard, having been prepared under the direction
3、 of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on 15 April 1997 BSI 1997 The following BSI references relate to the work on this standard: Committee reference TCI/67 Draft for comment 93/312452 DC ISBN 0 580 27005 X Am
4、endments issued since publication Amd. No. Date Text affected Committees responsible for this British Standard The preparation of this British Standard was entrusted to Technical Committee TCI/67, Household textiles, upon which the following bodies were represented: British Apparel and Textile Confe
5、deration British Fire Services Association British Furniture Manufacturers Federation British Interior Textiles Association British Retail Consortium Child Accident Prevention Trust Confederation of British Wool Textiles Limited Consumer Policy Committee of BSI Fabric Care Research Association Ltd.
6、Institute of Trading Standards Adminstration National Childrens Wear Association Natural Fillings Producers Association North East Lancashire Textile Manufacturers Association Qualitas Furnishing Standards Ltd. Textile Finishers AssociationBS EN 1162 : 1997 BSI 1997 i Contents Page Committees respon
7、sible Inside front cover National foreword ii Foreword 2 Text of EN 1162 3ii BSI 1997 BS EN 1162 : 1997 National foreword This British Standard has been prepared by Technical Committee TCI/67 and is the English language version of EN 1162 : 1996 Feather and down Test methods Determination of the oxy
8、gen index number published by the European Committee for Standardization (CEN). Cross-references Publication referred to Corresponding British Standard EN 21039 : 1992 BS EN 20139 : 1992 Textiles. Standard atmospheres for conditioning and testing EN 20187 : 1993 BS EN 20187 : 1993 Paper, board and p
9、ulps. Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples ISO 3696 : 1987 BS EN ISO 3696 : 1995 Water for analytical laboratory use. Specification and test methods ISO 3819 : 1985 BS 6523 : 1984 Specification for glass beakers for
10、laboratory use ISO 4793 : 1980 BS 1752 : 1983 Specification for laboratory sintered or fritted filters including porosity grading Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cove
11、r, page i and ii, the EN title page, pages 2 to 4, an inside back cover and a back cover.CEN European Committee for Standardization Comite Europe en de Normalisation Europa isches Komitee fu r Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1996 All rights or reproduction and commun
12、ication in any form and by any means reserved in all countries to CEN and its members. Ref. No. EN 1162 : 1996 E EUROPEAN STANDARD EN 1162 NORME EUROPE ENNE EUROPA ISCHE NORM August 1996 ICS 67.120.20; 97.160 Descriptors: Stuffings, feathers, tests, measurements, oxygen index, titration English vers
13、ion Feather and down Test methods Determination of the oxygen index number Plumes et duvets Me thodes dessai Mesure de lindice doxyge ne Federn und Daunen Pru fverfahren Bestimmung der Sauerstoffzahl This European Standard was approved by CEN on 1996-05-09. CEN members are bound to comply with the C
14、EN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or t
15、o any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official version
16、s. CEN members are the national standards bodies of Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.Page 2 EN 1162 : 1996 BSI 1997 Foreword This European Standard has been p
17、repared by the Technical Committee CEN/TC 222, Feather and down as filling material for any article, as well as finished articles filled with feather and down, the Secretariat of which is held by UNI. This European Standard shall be given the status of a national standard, either by publication of a
18、n identical text or by endorsement, at the latest by February 1997, and conflicting national standards shall be withdrawn at the latest by February 1997. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this Eur
19、opean Standard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Contents Page 1 Scope 3 2 Normative references 3 3 Definitions 3 4 Principle 3 5 Reagents 3 6 Apparatus
20、3 7 Conditioning and testing 3 8 Procedure 3 9 Expression of results 4 10 Test report 4Page 3 EN 1162 : 1996 BSI 1997 1 Scope This European Standard specifies a method for determining the oxygen index number of feathers and down by means of a titration method. 2 Normative references This European St
21、andard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate places in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply
22、to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication referred to applies. EN 20139 Textiles Standard atmospheres for conditioning and testing (ISO 139 : 1973) EN 20187 Paper, board and pulps Standard atmosphere
23、for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples (ISO 187 : 1990) ISO 385-3 Laboratory glassware Burettes Part 3: Burettes for which a waiting time of 30 s is specified ISO 648 Laboratory glassware One-mark pipettes ISO 835-3 Laboratory glassware G
24、raduated pipettes Part 3: Pipettes for which a waiting time of 15 s is specified ISO 3696 Water for analytical laboratory use Specification and test methods ISO 3819 Laboratory glassware Beakers ISO 4793 Laboratory sintered (fritted) filters Porosity grading, classification and designation 3 Definit
25、ions For the purposes of this standard the following definition applies: oxygen index number (of feather and down) Quantity of oxidizable and soluble material present in the filtrate of the aqueous extract of the material. It provides an index of the cleanliness of the material being tested, and is
26、expressed as milligrams oxygen per 100 g of the individual sample. 4 Principle The aqueous extract obtained at room temperature is titrated with a 0,02 mol/l solution of potassium permanganate. 5 Reagents 5.1 Water Grade 3, in accordance with ISO 3696. 5.2 3 mol/l sulfuric acid. 5.3 0,02 mol/l potas
27、sium permanganate. 6 Apparatus 6.1 Analytical balance, (with sensitivity of 0,1 mg). 6.2 Tumbler jar, capacity 2000 ml. 6.3 Beaker, capacity 2000 ml (in accordance with ISO 3819). 6.4 Beaker, capacity 400 ml (in accordance with ISO 3819). 6.5 Shaking machine, with 150 shakes per min and with shaking
28、 swing of 40 mm or tumbling machine with 150 min 21 . 6.6 Sintered (fritted) filter, pore size index P 160 (equal to G-1) 10 cm diameter (in accordance with ISO 4793). 6.7 One-mark pipette, class A capacity 100 ml (in accordance with ISO 648). 6.8 Graduated pipette, capacity 5 ml (in accordance with
29、 ISO 835-3). 6.9 Microburette, graduated in 0,02 ml (in accordance with ISO 385-3) 6.10 Stopwatch. 7 Conditioning and testing Test specimens of a representative part of the laboratory bulk sample shall be conditioned for a minimum period of 24 h in accordance with EN 20139 and the temperature and re
30、lative humidity shall be measured in accordance with EN 20187. 8 Procedure 8.1 A conditioned test specimen of mass of (10 0,1) g shall be placed in the tumbler jar; after adding 1000 ml of water (5.1), the jar shall be tumbled at room temperature for at least 60 min. 8.2 The resulting suspension sha
31、ll be filtered through the P 160 sintered filter into the 2000 ml beaker (6.3); do not squeeze excess water from the feathers. 8.3 With the pipette transfer 100 ml of the filtrate into a 400 ml beaker, add 3 ml of 3 mol/l sulfuric acid and titrate with 0,02 mol/l potassium permanganate, adding appro
32、ximately 0,02 ml at a time until a pink colour persists for 60 s. 8.4 A bank test of 100 ml water (5.1) shall be mixed with 3 ml of 3 mol/l sulfuric acid and titrated with 0,02 mol/l potassium permanganate, adding approximately 0,02 ml at a time until a pink colour persists for 60 s. 8.5 Repeat the
33、test on another test specimen at least.Page 4 EN 1162 : 1996 BSI 1997 9 Expression of results The oxygen index number is calcuated as follows: l =8 03(A2B ) where: l is the oxygen index number; A is the quantity of 0,02 mol/l potassium permanganate used for the test specimen, in millilitres; B is th
34、e quantity of 0,02 mol/l potassium permanganate used for the blank test, in millilitres. Calculate the mean of the two determinations with the approximation to the nearest integer. 10 Test report The test report shall include at least the following information: the reference to this standard; date a
35、nd place of testing; identification mark of the individual sample tested; the arithmetic mean result to the nearest integer in accordance with clause 9; any departure from the procedure and any other circumstances (for example the presence of antistatic agent) that can have affected the result. BSI
36、1997 BS EN 1162 : 1997 List of references See national foreword.BSI 389 Chiswick High Road London W4 4AL | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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