1、| | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | BRITISH STANDARD BS EN 1163 : 1997 The Eur
2、opean Standard EN 1163 : 1996 has the status of a British Standard ICS 59.040 NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW Feather and down Test methods Determination of the oil and fat contentBS EN 1163 : 1997 This British Standard, having been prepared under the direction
3、 of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on 15 April 1997 BSI 1997 The following BSI references relate to the work on this standard: Committee reference TCI/67 Draft for comment 93/312453 DC ISBN 0 580 27009 2 Am
4、endments issued since publication Amd. No. Date Text affected Committees responsible for this British Standard The preparation of this British Standard was entrusted to Techncial Committee TCI/67, Household textiles, upon which the following bodies were represented: British Apparel and Textile Confe
5、deration British Fire Services Association British Furniture Manufacturers Federation British Interior Textiles Association British Retail Consortium Child Accident Prevention Trust Confederation of British Wool Textiles Limited Consumer Policy Committee of BSI Fabric Care Research Association Ltd.
6、Institute of Trading Standards Adminstration National Childrens Wear Association Natural Fillings Producers Association North East Lancashire Textile Manufacturers Association Qualitas Furnishing Standards Ltd. Textile Finishers AssociationBS EN 1163 : 1997 BSI 1997 i Contents Page Committees respon
7、sible Inside front cover National foreword ii Foreword 2 Text of EN 1163 3ii BSI 1997 BS EN 1163 : 1997 National foreword This British Standard has been prepared by Technical Committee TCI/67 and is the English language version of EN 1163 : 1996 Feather and down Test methods Determination of the oil
8、 and fat content published by the European Committee for Standardization (CEN). Cross-references Publication referred to Corresponding British Standard EN 21039 : 1992 BS EN 20139 : 1992 Textiles. Standard atmospheres for conditioning and testing EN 20187 : 1993 BS EN 20187 : 1993 Paper, board and p
9、ulps. Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples ISO 3819 : 1985 BS 6523 : 1984 Specification for glass beakers for laboratory use ISO 4793 : 1980 BS 1752 : 1983 Specification for laboratory sintered or fritted filters inc
10、luding porosity grading ISO 4797 : 1981 BS 6352 : 1983 Specification for flasks with ground glass joints Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, the EN
11、 title page, pages 2 to 4, an inside back cover and a back cover.CEN European Committee for Standardization Comite Europe en de Normalisation Europa isches Komitee fu r Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1996 Copyright reserved to CEN members Ref. No. EN 1163 : 1996 E E
12、UROPEAN STANDARD EN 1163 NORME EUROPE ENNE EUROPA ISCHE NORM August 1996 ICS 67.120.20; 97.160 Descriptors: Stuffings, feathers, tests, extraction, oils, greases, soluble matter, solvents, dichloromethance English version Feather and down Test methods Determination of the oil and fat content Plumes
13、et duvets Me thodes dessai De termination du contenu en huiles et graisses Federn und Daunen Pru fverfahren Bestimmung des O l- und Fettgehaltes This European Standard was approved by CEN on 1996-05-09. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the con
14、ditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. This European Standard exists in thre
15、e official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the national standards bodies of Aus
16、tria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.Page 2 EN 1163 : 1996 BSI 1997 Foreword This European Standard has been prepared by the Technical Committee CEN/TC 222, Feather
17、and down as filling material for any article, as well as finished articles filled with feather and down, the Secretariat of which is held by UNI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by Fe
18、bruary 1997, and conflicting national standards shall be withdrawn at the latest by February 1997. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, Fra
19、nce, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Contents Page 0 Introduction 3 1 Scope 3 2 Normative references 3 3 Principle 3 4 Reagents 3 5 Apparatus 3 6 Conditioning and testing 3 7 Procedure 3 8 Express
20、ion of results 4 9 Test report 4Page 3 EN 1163 : 1996 BSI 1997 0 Introduction Feather and down can contain varying quantities of oils and fats. It is suspected that adding mineral oil has the effect of binding impurities into the feathers and down, giving the impression of a cleaner product. 1 Scope
21、 This European Standard specifies a method for determining the amount of solvent soluble matter in dichloromethane. 2 Normative references This European Standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate pl
22、aces in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication ref
23、erred to applies. EN 20139 Textiles Standard atmospheres for conditioning and testing (ISO 139 : 1973) EN 20187 Paper, board and pulps Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples (ISO 187 : 1990) ISO 3074 Wool Determination
24、 of dichloromethane-soluble matter in combed sliver ISO 3819 Laboratory glassware Beakers ISO 4793 Laboratory sintered (fritted) filters Porosity grading, classification and designation ISO 4797 Laboratory glassware Flasks with conical ground joints ISO 4797-1 Laboratory apparatus Vocabulary relatin
25、g to apparatus made essentially from glass, porcelain or vitreous silica Part 1: Names for items of apparatus 3 Principle Extraction of a known amount of feathers and down in a Soxhlet apparatus with dichloromethane; filtration of the dichloromethane solution, evaporation of the solvent and determin
26、ation of the mass of the residue. 4 Reagents Purified, distilled dichloromethane (in accordance with ISO 3074). 5 Apparatus 5.1 Analytical balance, (with sensitivity of 0,1 mg). 5.2 Soxhlet extractor, capacity 100 ml with condenser (in accordance with ISO 4797-1). 5.3 Extractor flasks, capacity 250
27、ml (in accordance with ISO 4797). 5.4 Fat free paper thimbles, or sintered base glass. 5.5 Condenser. 5.6 Sintered (fritted) filter, P 100 (ISO 4793) or fat free paper filter of equal porosity. 5.7 Waterbath, or hot plate. 5.8 Desiccator, with desiccating agent. 5.9 Tared glass beaker, capacity 100
28、ml, dried at (105 2) C (in accordance with ISO 3819). 5.10 Drying oven, capable of being controlled at a temperature of (105 2) C. 6 Conditioning and testing Test specimens of a representative part of the laboratory bulk sample shall be conditioned for a minimum period of 24 h in accordance with EN
29、20139 and the temperature and relative humidity shall be measured in accordance with EN 20187. 7 Procedure 7.1 Take one conditioned test specimen of mass from 4 g 0,05 g to 5 g 0,05 g. 7.2 Put the conditioned test specimen into the extraction thimble, which is placed in the Soxhlet extractor. Attach
30、 the condenser and extraction flask, and put enough solvent to maintain siphoning. Place the connected flask in the waterbath or on the hot plate so that satisfactory siphoning occurs, at the rate of not less than 6 cycles per hour and then extract the individual sample. 7.3 Extract the test specime
31、n for not less than 20 siphonings. Filter the content of the extraction flask through a sintered filter or fat free paper filter into a tared beaker, remove the bulk of the solvent by distillation, dry to constant mass in a well ventilated oven at (105 2) C. 7.4 Repeat the operations in 7.1 to 7.3 o
32、n the second test specimen.Page 4 EN 1163 : 1996 BSI 1997 8 Expression of results The dichloromethane-soluble matter (in percent) is calculated as follows: M s = 3 100 A2 B C where: M s is the percentage of matter soluble in dichloromethane; A is the mass of the beaker containing the residue, in gra
33、ms; B is the mass of the beaker, in grams; C is the mass of the conditioned test specimen, in grams. The result is expressed as the average of at least two determinations, rounded to one decimal place. 9 Test report The test report shall include at least the following information: the reference to t
34、his standard; date and place of testing; identification mark of the individual sample tested; the mean result to one decimal place in accordance with 8; any departure from the procedure and any other circumstances that can have affected the result. BSI 1997 BS EN 1163 : 1997 List of references See n
35、ational foreword.BSI 389 Chiswick High Road London W4 4AL | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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