1、BSI Standards PublicationBS EN 16602-70-13:2015Space product assurance Measurements of the peel andpull-off strength of coatingsand finishes using pressure-sensitive tapesBS EN 16602-70-13:2015 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN16602-70-13:2015. It
2、supersedes BS EN 14099:2001 which iswithdrawn.The UK participation in its preparation was entrusted to TechnicalCommittee ACE/68, Space systems and operations.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include
3、 all the necessaryprovisions of a contract. Users are responsible for its correctapplication. The British Standards Institution 2015. Published by BSI StandardsLimited 2015ISBN 978 0 580 86499 5ICS 49.140Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Sta
4、ndard was published under the authority of theStandards Policy and Strategy Committee on 28 February 2015.Amendments issued since publicationDate Text affectedBS EN 16602-70-13:2015EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 16602-70-13 January 2015 ICS 49.040; 49.140 Supersedes EN 14099:20
5、01 English version Space product assurance - Measurements of the peel and pull-off strength of coatings and finishes using pressure-sensitive tapes Assurance produit des projets spatiaux - Mesure de la force darrachement des revtements et apprts de rubans auto-adhsifs Raumfahrtproduktsicherung - Erm
6、ittlung der Schl- und Abziehfestigkeit von berzgen und Beschichtungen unter Anwendung von Haftbndern This European Standard was approved by CEN on 11 October 2014. CEN and CENELEC members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this Eur
7、opean Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN and CENELEC member. This European Standard exists in three off
8、icial versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN and CENELEC member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN and CENELEC members are the nat
9、ional standards bodies and national electrotechnical committees of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlan
10、ds, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2015 CEN/CENELEC All rights of exploitation in any form and by any means reserved worldwide for CEN national Members and
11、for CENELEC Members. Ref. No. EN 16602-70-13:2015 E BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 2 Table of contents Foreword 4 1 Scope . 5 2 Normative references . 6 3 Terms, definitions and abbreviated terms 7 3.1 Terms from other standards 7 3.2 Terms specific to the present standard . 7 3.3 Abb
12、reviated terms. 7 4 Principles 8 5 Requirements 10 5.1 Preparatory conditions 10 5.1.1 Hazards, health and safety precautions 10 5.1.2 Preparation of samples . 10 5.1.3 Facilities 12 5.1.4 Equipment . 12 5.2 Test procedure . 14 5.2.1 Preparation . 14 5.2.2 Peel and pull-off test . 14 5.2.3 Handling
13、and packaging of tested samples . 15 5.3 Acceptance criteria . 15 5.4 Quality assurance . 16 5.4.1 Data 16 5.4.2 Nonconformance . 16 5.4.3 Calibration . 16 5.4.4 Traceability . 16 Annex A (normative) Test result sheet - DRD . 17 Annex B (informative) Peel and pull-off test procedure. 20 Annex C (inf
14、ormative) Fracture lines . 22 BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 3 Bibliography . 23 Figures Figure 4-1 Test procedure flow diagram . 9 Figure 5-1: Side view of the test fixtures . 13 Figure A-1 : Example of test result sheet 19 Figure C-1 : Schematic cross-section of a coated substrate s
15、howing various fracture lines dependent on the weakest layer 22 BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 4 Foreword This document (EN 16602-70-13:2015) has been prepared by Technical Committee CEN/CLC/TC 5 “Space”, the secretariat of which is held by DIN. This standard (EN 16602-70-13:2015) ori
16、ginates from ECSS-Q-ST-70-13C Rev.1. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by July 2015, and conflicting national standards shall be withdrawn at the latest by July 2015. Attention is drawn
17、 to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document has been prepared under a mandate given to CEN by the European Commission and the European
18、 Free Trade Association. This document supersedes EN 14099:2001. This document has been developed to cover specifically space systems and has therefore precedence over any EN covering the same scope but with a wider domain of applicability (e.g. : aerospace). According to the CEN-CENELEC Internal Re
19、gulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland,
20、 Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 5 1 Scope This Standard details a test in which pressure-sensitive tapes are used
21、 to assess the suitability of, for example, coatings, paints, films and other thin materials, proposed for use on spacecraft and associated equipment. Surface coatings, such as thermal control paints and corrosion protection coatings, are affected, both on the ground and after launch, by exposure to
22、 the environment. It is therefore important that the adhesion of the coating to the relevant substrate remains at an acceptable level after exposure to the relevant environmental condition. The following materials and assemblies are covered by this test method: organic coating, e.g. varnishes, paint
23、s and plastic films; metallic finishes on, for example, printed circuit boards, second-surface mirrors, thermal radiators, plastic films; adhesive layers; composite thin films; small assemblies, e.g. solar cells having attached glass covers. This standard may be tailored for the specific characteris
24、tics and constrains of a space project in conformance with ECSS-S-ST-00. BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 6 2 Normative references The following normative documents contain provisions which, through reference in this text, constitute provisions of this ECSS Standard. For dated reference
25、s, subsequent amendments to, or revision of any of these publications do not apply, However, parties to agreements based on this ECSS Standard are encouraged to investigate the possibility of applying the more recent editions of the normative documents indicated below. For undated references, the la
26、test edition of the publication referred to applies. EN reference Reference in text Title EN 16601-00-01 ECSS-S-ST-00-01 ECSS system Glossary of terms EN 16602-10-09 ECSS-Q-ST-10-09 Space product assurance Nonconformance control system EN 16602-20 ECSS-Q-ST-20 Space product assurance Quality assuran
27、ce EN 16602-40 ECSS-Q-ST-40 Space product assurance Safety EN 16602-70-02 ECSS-Q-ST-70-02 Space product assurance Thermal vacuum outgassing test for the screening of space materials BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 7 3 Terms, definitions and abbreviated terms 3.1 Terms from other standa
28、rds For the purpose of this Standard, the terms and definitions from ECSS-S-ST-00-01 apply, in particular for the following terms: requirement 3.2 Terms specific to the present standard 3.2.1 batch quantity produced at one operation. NOTE One batch can be subdivided into several lots. 3.3 Abbreviate
29、d terms For the purpose of this Standard, the abbreviated terms from ECSS-S-ST-00-01 and the following apply: Abbreviation Meaning RH relative humidity BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 8 4 Principles This Standard details a test in which pressure-sensitive tapes are used to assess the s
30、uitability of, for example, coatings, paints, films and other thin materials, proposed for use on spacecraft and associated equipment. This test has nine test steps as outlined in Figure 4-1. BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 9 3. Prepare tape holder: Locate tape over rubber block and cl
31、amp in place, see Annex B a.3 - 5. 4. Mount sample and tape holders in test machine, see Annex B a.6 and 7. 5. Raise jig until sample touches surface of tape, see Annex B a.8. Peel and pull-off test: See 5.2.2 2. Condition for nominal 24 hours at (22 3) C, RH (55 10) %, see 5.2.1.2. Preparation: See
32、 5.2.1 6. Compress sample onto tape with load of nominal 5 kg for a nominal 60 seconds, see Annex B a.9. 7. Reverse compression by pulling apart tape and sample at a nominal 0,2 cm/min until separation occurs, see Annex B a.10. 8. Additional test: If separation is between tape and sample surface wit
33、hout damage, repeat steps 3 to 7 above using tape with higher peel strength, see Annex B a.11. - 13. 9. Acceptance criteria, see 5.3. 1. Mount sample in sample holder, see 5.2.1.1. Figure 4-1 Test procedure flow diagram BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 10 5 Requirements 5.1 Preparatory
34、conditions 5.1.1 Hazards, health and safety precautions a. The supplier shall identify, manage and process materials and parts with hazardous characteristics according to ECSSQ-ST-40. b. The supplier shall keep the health and safety precautions according to the suppliers national safety regulations.
35、 5.1.2 Preparation of samples 5.1.2.1 Configuration a. The supplier shall prepare the material samples according to the process specifications or manufacturers data. b. The material samples shall be representative of batch variance. c. If it is not practicable to test completed assemblies, the suppl
36、ier shall submit samples made from the same materials and by the same processes as those used in the manufacture of the assemblies. d. The sample for testing shall have clean flat surfaces which do not overlap the sample holder described in clause 5.1.4. e. The width of the test sample surface face
37、shall be at least equal to the width of the tape used in the test procedure. f. The nominal tape width shall be 20 mm. g. The supplier shall specify the number of samples to be taken from a qualification batch, test programme, or production batch at the start of the test in conformance with the DRD
38、in Annex A h. The supplier shall test at least ten test samples. i. If it is not practicable to obtain test samples from the finished article, the supplier shall furnish bonded test samples for the test. NOTE These samples are not used for any other purpose than the designated test. j. The supplier
39、shall furnish a certificate of conformity for the purpose of traceability. BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 11 NOTE This certificate of conformity is delivered by the manufacturer in order to provide evidence that the product is compliant with the manufacturers process. k. The supplier
40、shall mark all test samples with identification to maintain traceability but in such a way as not to degrade the quality of the sample during testing. 5.1.2.2 Cleaning a. The suppler shall perform the same cleaning and other treatments of the sample as that applied to the finished article, which the
41、 sample is intended to represent, prior to integration into the spacecraft. b. The supplier shall not carry out further cleaning or other treatments. 5.1.2.3 Handling and storage a. The supplier shall handle the samples only with clean nylon or lint-free gloves. b. The supplier shall store the sampl
42、es in a controlled area, with an ambient temperature of (22 3) C and relative humidity of (55 10) %. c. The supplier shall shield coated surfaces from contact by using polyethylene or polypropylene bags or sheets. d. The supplier shall avoid physical damage by packing the polyethylene or polypropyle
43、ne-wrapped workpieces in clean, dust- and lint-free material. e. The supplier shall label limited-life materials with their shelf lives and dates of manufacture, or date of delivery if date of manufacture is not known. 5.1.2.4 Identification 5.1.2.4.1 Materials a. The supplier shall identify materia
44、ls submitted for testing in conformance to annex A of ECSS-Q-ST-70-02. 5.1.2.4.2 Assemblies a. The supplier shall identify assemblies submitted for testing, as a minimum, by: 1. trade name and batch number; 2. name of manufacturer or supplier through whom the purchase was made; 3. configuration cont
45、rol status of the assembly. BS EN 16602-70-13:2015EN 16602-70-13:2015 (E) 12 5.1.3 Facilities 5.1.3.1 Cleanliness a. The work area shall be clean and free of dust. b. The supplier shall filter the air used for ventilation to prevent contamination of the sample. 5.1.3.2 Sample conditioning a. The sup
46、plier shall environmentally condition the sample for a nominal 24 hour period at (22 3) C with a relative humidity of (55 10) %. NOTE 1 The humidity requirement can be achieved either in a conditioning room, or by dessicators filled with silica gel or a saturated salt solution. NOTE 2 A saturated sa
47、lt solution of calcium nitrate gives approximately 51 % relative humidity at the testing temperature. 5.1.4 Equipment 5.1.4.1 Special equipment a. The supplier shall use the equipment as detailed in clauses 5.1.4.2 and 5.1.4.3. 5.1.4.2 Testing machine a. The supplier shall employ a power-driven mach
48、ine capable of maintaining a specified constant rate of loading and able to be used for both tensile and compressive testing. b. The machine shall have a fixed or essentially stationary member supporting a load cell and the tape holder. c. A movable member shall carry the sample holder. d. The appli
49、ed compressive and tensile loads, as measured and recorded, shall be accurate within 1 percent of the load. e. The rate of travel of the sample holder shall be at a nominal rate of 0,2 cm/min. 5.1.4.3 Fixtures a. The tape holder should be of a design similar to that depicted in Figure 5-1. b. The part shall be screwed into the fixed member of the testing machine or be located firmly on it. c. The supplier shall clamp a length of pressure-sensitive tape from one tape holder over the rubber block to the other tape holder. d. The surface of th
