1、BRITISH STANDARD BS EN ISO 105-S03:1996 Textiles Tests for colour fastness Part S03: Colour fastness to vulcanization Open steam The European Standard EN ISO 105-S03:1995 has the status of a British Standard ICS 59.080.10BSENISO105-S03:1996 This British Standard, having been prepared under the direc
2、tionof the Sector Board forMaterials and Chemicals, waspublished under the authorityof the Standards Boardand comes into effect on 15 February 1996 BSI 09-1999 The following BSI references relate to the work on this standard: Committee reference TCI/25 Draft announced in BSI News February 1995 ISBN
3、0 580 23978 0 Committees responsible for this British Standard The preparation of this British Standard was entrusted to Technical Committee TCI/25, Chemical properties, upon which the following bodies were represented: Association of Consulting Scientists Association of Suppliers to the British Clo
4、thing Industry British Apparel and Textile Confederation British Clothing Industry Association British Measurement and Testing Association British Retail Consortium Chemical Industries Association Consumer Policy Committee of BSI Fabric Care Research Association Ltd. Home Laundering Consultative Cou
5、ncil International Wool Secretariat Mail Order Traders Association Ministry of Defence National Wool Textile Export Corporation SATRA Footwear Technology Centre Soap and Detergent Industry Association Society of Dyers and Colourists Textile Finishers Association Participation in the detailed technic
6、al work was undertaken by the Society of Dyers and Colourists Amendments issued since publication Amd. No. Date CommentsBSENISO105-S03:1996 BSI 09-1999 i Contents Page Committees responsible Inside front cover National foreword ii Foreword 2 1 Scope 3 2 Normative references 3 3 Principle 3 4 Apparat
7、us and materials 3 5 Test specimen 4 6 Procedure 4 7 Test report 4 Annex ZA (normative) References to international publications with their relevant European publications 5 List of references Inside back coverBSENISO105-S03:1996 ii BSI 09-1999 National foreword This British Standard has been prepare
8、d by Technical Committee TCI/25 and is the English language version of ENISO105-S03:1995 Textiles Tests for colour fastness Part S03 Colour fastness to vulcanization: Open steam published by the European Committee for Standardization (CEN). It was derived by CEN from ISO105-S03:1993, published by th
9、e International Organization for Standardization (ISO). This British Standard supersedes the corresponding method in BS1006:1990, which is withdrawn by amendment. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for
10、 their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Cross-references Publication referred to Corresponding British Standard ISO 105-A01:1989 a BS EN ISO 105 Textiles Tests for colour fastness Part A01:1996 General principles of te
11、sting ISO 105-A02:1993 BS EN 20105 Textiles Tests for colour fastness Part A02:1995 Grey scale for assessing change in colour ISO 105-A03:1993 Part A03:1995 Grey scale for assessing staining ISO 105-F:1985 BS 1006:1990 Methods of test for colour fastness of textiles and leather (Section F) ISO 105-F
12、10:1989 BS 1006:1990 Methods of test for colour fastness of textiles and leather (Section F10) ISO 139:1973 BS EN 20139:1992 Textiles Standard atmospheres for conditioning and testing a Superseded by ISO 105-A01:1994. Summary of pages This document comprises a front cover, an inside front cover, pag
13、es i and ii, theEN ISO title page, pages 2 to 6, an inside back cover and a back cover. This standard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover.EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE N
14、ORM EN ISO 105-S03 November 1995 ICS 59.080.10 Descriptors: Textiles, dyes, tests, vulcanizing tests, determination, colour fastness English version Textiles Tests for colour fastness Part S03: Colour fastness to vulcanization: Open steam (ISO 105-S03:1993) Textiles Essais de solidit des teintures P
15、artie S03: Solidit la vulcanisation: Vapeur sature (ISO 105-S03:1993) Textilien Farbechtheitsprfungen Teil S03: Farbechtheit gegen Vulkanisieren: Offener Dampf (ISO 105-S03:1993) This European Standard was approved by CEN on 1995-07-28. CEN members are bound to comply with the CEN/CENELEC Internal R
16、egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. Thi
17、s European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are th
18、e national standards bodies of Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normalisation Europisches Komitee
19、 fr Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1995 All rights of reproduction and communication in any form and by any means reserved in all countries to CEN and its members Ref. No. EN ISO 105-S03:1995 EENISO105-S03:1995 BSI 09-1999 2 Foreword The text of the International St
20、andard from ISO/TC38, Textiles, of the International Organization for Standardization (ISO) has been taken over as a European Standard by the Technical Committee CEN/TC248, Textiles and textile products. This European Standard shall be given the status of a national standard, either by publication o
21、f an identical text or by endorsement, at the latest by May1996, and conflicting national standards shall be withdrawn at the latest by May1996. According to CEN/CENELEC Internal Regulations, the following countries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, F
22、rance, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. NOTENormative references to International Standards are listed inAnnex ZA (normative).ENISO105-S03:1995 BSI 09-1999 3 1 Scope This part of ISO105 specifies a
23、 method for determining the resistance of the colour of textiles of all kinds and in all forms to the action of a typical rubber compound such as may be used in the proofing industry, and to its decomposition products, during vulcanization in open steam, either a) under conditions that prevent live
24、steam from coming into contact with the specimen to be tested (method A) or b) under conditions that allow live steam to infiltrate into the adjacent fabric to be tested (method B). 2 Normative references The following standards contain provisions which, through reference in this text, constitute pr
25、ovisions of this part of ISO105. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this part of ISO105 are encouraged to investigate the possibility of applying the most recent editions of the standards indicated
26、below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 105-A01:1989, Textiles Tests for colour fastness Part A01: General principles of testing. ISO 105-A02:1993, Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour. ISO 105
27、-A03:1993, Textiles Tests for colour fastness Part A03: Grey scale for assessing staining. ISO 105-F:1985, Textiles Tests for colour fastness Part F: Standard adjacent fabrics. ISO 105-F10:1989, Textiles Tests for colour fastness Part F10: Specification for adjacent fabric: Multifibre. ISO 139:1973,
28、 Textiles Standard atmospheres for conditioning and testing. 3 Principle A specimen of the textile under test is heated in live steam in direct contact with an (initially) unvulcanized rubber compound, the textile material being wrapped in either a) sheeting impermeable to steam and water (method A)
29、 or b) undyed bleached cotton fabric, but ensuring that live steam is not prevented from infiltration into the specimen (method B). The change in colour of the specimen and the staining of the adjacent fabric are assessed with the grey scales. 4 Apparatus and materials 4.1 Jacketed autoclave, capabl
30、e of holding a steam pressure on both jacket and pan of390kPa. 4.2 Stainless-steel open-ended tube, of diameter40mm3mm and wall thickness2,5mm 0,5mm. 4.3 Sheet of uncured rubber compound, 2,5mm 1,5mm thick, consisting of the following 100 parts pale crepe; 5 parts zinc oxide; 1 part stearic acid; 2
31、parts sulfur; 1 part mercaptobenzothiazole; 0,2 parts zinc diethyldithiocarbamate; 15 parts titanium oxide; 75 parts barium sulfate. If it is necessary to transport the rubber compound, cover it with thin polyethylene film. NOTE 1It should be borne in mind that this test employs a basic rubber compo
32、und. Other compounding ingredients are frequently used in production and may have specific effects on colour fastness not revealed by this test. 4.4 Adjacent fabrics (see ISO105-A01:1989, sub-clause8.3). Either 4.4.1 Multifibre adjacent fabric, complying with ISO105-F10. Or 4.4.2 Single-fibre adjace
33、nt fabric, complying with the relevant section of sections F01 to F08 of ISO105-F, of the same generic kind of fibre as that in the textile to be tested, or that predominating in the case of blends. 4.5 Undyed bleached cotton 4.6 For method A only (ingress of steam prevented): sheeting which is impe
34、rmeable to steam and water, for example rubber-proofed fabric sheeting or plastics sheeting such as polyester, capable of withstanding a temperature of140 C. 4.7 Grey scale for assessing change in colour, complying with ISO105-A02, and grey scale for assessing staining, complying with ISO105-A03. 4.
35、8 Petroleum spiritENISO105-S03:1995 4 BSI 09-1999 5 Test specimen 5.1 Remove any polyethylene film from the sheet of uncured rubber compound(4.3) and moisten the compound with petroleum spirit (4.8). 5.2 If the textile to be tested is fabric, place a specimen measuring 40mm 100mm on the sheet of unc
36、ured rubber compound. To ensure a uniform degree of adhesion, “roll” the specimen on to the rubber with a metal roller. 5.3 If the textile to be tested is yarn, knit it into a fabric and use a specimen measuring40mm 100mm, or stick a number of lengths flat and side by side on the rubber sheet to obt
37、ain the specified area of40mm 100mm (see5.2). 5.4 If the textile to be tested is loose fibre, comb and compress enough of it to form a sheet measuring40mm 100mm and stick this to the rubber sheet(see5.2). 6 Procedure 6.1 Wrap the composite specimen round the stainless-steel open-ended tube(4.2), rub
38、ber face inside. 6.1.1 For method A (ingress of steam prevented), cover the specimen by tightly wrapping with one layer of adjacent fabric(4.4.1 or4.4.2), three layers of undyed bleached cotton fabric (4.5) and two layers of impermeable sheeting(4.6), taking care that the wrapping projects beyond th
39、e edges of the composite specimen on the tube. Securely bind the edges with string to prevent direct ingress of steam. 6.1.2 For method B (ingress of steam permitted), cover the specimen by tightly wrapping with one layer of adjacent fabric(4.4.1 or4.4.2) and two layers of undyed bleached cotton fab
40、ric(4.5). 6.2 Place the tube in the preheated autoclave(4.1), ensuring that the temperature of the jacket is142 C 1 C (380kPa steam pressure) and that of the pan139 C 1 C (350kPa steam pressure). Carry out the test for20min. 6.3 Remove the tube, cool in air, remove the wrapping fabric and the adjace
41、nt fabric and condition the composite specimen and the adjacent fabric for4h in a standard atmosphere for testing complying with ISO139. 6.4 Assess the change in colour of the treated specimen by comparing it with a piece of the original dyeing laid on a sheet of vulcanized rubber, and the staining
42、of the adjacent fabric on the side in direct contact with the specimen, using the grey scales(4.7). 7 Test report The test report shall include the following particulars: a) the number and date of publication of this part of ISO105, i.e.ISO105-S03:1993; b) all details necessary for the identificatio
43、n of the sample tested; c) the numerical ratings for change in colour of the specimen (see6.4); d) the adjacent fabric used; e) if a multifibre adjacent fabric was used, the stairing of each type of fibre in the multifibre adjacent fabric and the type of multifibre adjacent fabric used; f) the metho
44、d of wrapping used(6.1.1 or6.1.2).ENISO105-S03:1995 BSI 09-1999 5 Annex ZA (normative) Normative references to international publications with their relevant European publications This European Standard incorporates by dated or undated reference, provisions from other publications. These normative r
45、eferences are cited at the appropriate places in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references
46、the latest edition of the publication referred to applies. IEC publication Date Title EN/HD Date ISO 105-A01 1994 Textiles Tests for colour fastness Part A01: General principles of testing EN ISO 105-A01 1994 ISO 105-A02 1993 Textiles Tests for colour fastness Part A02: Grey scale for assessing chan
47、ge in colour EN 20105-A02 1994 ISO 105-A03 1993 Textiles Tests for colour fastness Part A03: Grey scale for assessing staining EN 20105-A03 1994 ISO 139 1973 Textiles Standard atmospheres for conditioningand testing EN 20139 19926 blankBSENISO105-S03:1996 BSI 09-1999 List of references See national
48、foreword.BS EN ISO 105-S03:1996 BSI 389 Chiswick High Road London W4 4AL BSIBritishStandardsInstitution BSI is the independent national body responsible for preparing BritishStandards. It presents the UK view on standards in Europe and at the international level. It is incorporated by Royal Charter.
49、 Revisions BritishStandards are updated by amendment or revision. Users of BritishStandards should make sure that they possess the latest amendments or editions. It is the constant aim of BSI to improve the quality of our products and services. We would be grateful if anyone finding an inaccuracy or ambiguity while using this BritishStandard would inform the Secretary of the technical committee responsible, the identity of which can be found on the inside front cover. Tel:02089969
