1、BRITISH STANDARD BS EN ISO 105-X01:1996 Textiles Tests for colour fastness Part X01: Colour fastness to carbonizing: Aluminium chloride The European Standard EN ISO 105-X01:1995 has the status of a BritishStandard ICS 59.080.10BSEN ISO 105-X01:1996 This British Standard, having been prepared under t
2、he directionof the Sector Board forMaterials and Chemicals, waspublished under the authorityof the Standards Boardand comes into effect on 15 March 1996 BSI 11-1999 The following BSI references relate to the work on this standard: Committee reference TCI/25 Draft announced in BSI News February 1995
3、ISBN 0 580 23983 7 Committees responsible for this British Standard The preparation of this British Standard was entrusted to Technical Committee TCI/25, Chemical properties, upon which the following bodies were represented: Association of Consulting Scientists Association of Suppliers to the Britis
4、h Clothing Industry British Apparel and Textile Confederation British Clothing Industry Association British Measurement and Testing Association British Retail Consortium Chemical Industries Association Consumer Policy Committee of BSI Fabric Care Research Association Ltd. Home Laundering Consultativ
5、e Council International Wool Secretariat Mail Order Traders Association Ministry of Defence National Wool Textile Export Corporation SATRA Footwear Technology Centre Soap and Detergent Industry Association Society of Dyers and Colourists Textile Finishers Association Participation in the detailed te
6、chnical work was undertaken by the Society of Dyers and Colourists. Amendments issued since publication Amd. No. Date CommentsBSEN ISO 105-X01:1996 BSI 11-1999 i Contents Page Committees responsible Inside front cover National foreword ii Foreword 2 1 Scope 3 2 Normative references 3 3 Principle 3 4
7、 Apparatus and materials 3 5 Test specimen 3 6 Procedure 3 7 Test report 4 Annex ZA (normative) Normative references to international publicationswiththeir relevant European publications 5 List of references Inside back coverBSEN ISO 105-X01:1996 ii BSI 11-1999 National foreword This British Standar
8、d has been prepared by Technical Committee TCI/25 and is the English language version of EN ISO 105-X01:1995 Textiles Tests for colour fastness Part X01: Colour fastness to carbonizing: Aluminium chloride, published by the European Committee for Standardization (CEN). It was derived by CEN from ISO
9、105-X01:1993 published by the International Organization for Standardization (ISO). This British Standard supersedes the corresponding method in BS 1006:1990, which is withdrawn by amendment. In Annex ZA, the reference to ISO 105-A03 is an error and should be ignored. A British Standard does not pur
10、port to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Cross-references Publication referred to Corresponding British Standard
11、ISO 105-A01:1989 BS EN ISO 105 Textiles Tests for colour fastness Part A01:1996 General principles of testing ISO 105-A02:1993 BS EN 20105 Textiles Tests for colour fastness Part A02:1995 Grey scale for assessing change in colour Summary of pages This document comprises a front cover, an inside fron
12、t cover, pages i and ii, theEN ISO title page, pages 2 to 6, an inside back cover and a back cover. This standard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover.EUROPEAN STANDARD NORME EUROPENNE
13、EUROPISCHE NORM EN ISO 105-X01 November 1995 ICS 59.080.10 Descriptors: Textiles, dyes, tests, carbonizing tests, determination, colour fastness English version Textiles Tests for colour fastness Part X01: Colour fastness to carbonizing: Aluminium chloride (ISO 105-X01:1993) Textiles Essais de solid
14、it des teintures Partie X01: Solidit au carbonisage: Chlorure daluminium (ISO 105-X01:1993) Textilien Farbechtheitsprfungen TeilX01: Farbechtheit gegen das Karbonisiern: Aluminiumchlorid (ISO 105-X01:1993) This European Standard was approved by CEN on 1995-07-28. CEN members are bound to comply with
15、 the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretaria
16、t or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official v
17、ersions. CEN members are the national standards bodies of Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normal
18、isation Europisches Komitee fr Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1995 All rights of reproduction and communication in any form and by any means reserved in all countries to CEN and its members. Ref. No. EN ISO 105-X01:1995 EEN ISO 105-X01:1995 BSI 11-1999 2 Foreword Th
19、e text of the International Standard from ISO/TC 38, Textiles, of the International Organization for Standardization (ISO) has been taken over as a European Standard by the Technical Committee CEN/TC 248, Textiles and textile products. This European Standard shall be given the status of a national s
20、tandard, either by publication of an identical text or by endorsement, at the latest by May1996, and conflicting national standards shall be withdrawn at the latest by May 1996. According to CEN/CENELEC Internal Regulations, the following countries are bound to implement this European Standard: Aust
21、ria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. NOTENormative references to International Standards are listed in Annex ZA (normative).EN ISO 105-X01:1995 BSI 11-1999 3 1 S
22、cope This part of ISO 105 specifies a method for determining the resistance of the colour of textiles in all forms to the manufacturing operation designed to remove vegetable impurities by a treatment with aluminium chloride at high temperatures. The method is mainly applicable to wool and textiles
23、containing wool, particularly those containing also acetate or polyamide fibres. 2 Normative references The following standards contain provisions which, through reference in this text, constitute provisions of this part of ISO 105. At the time of publication, the editions indicated were valid. All
24、standards are subject to revision, and parties to agreements based on this part of ISO 105 are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 10
25、5-A01:1989, Textiles Tests for colour fastness Part A01: General principles of testing. ISO 105-A02:1993, Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour. 3 Principle A specimen impregnated with aluminium chloride solution is dried, baked, rinsed and neutralize
26、d. The changes in colour after rinsing, neutralizing and drying are assessed with the grey scale. 4 Apparatus and materials 4.1 Oven, for drying specimens in air 60 C 2 C and baking in air at 115 C 2 C. 4.2 Aluminium chloride solution ( 1,037 g/ml), containing 51,4 g of AlCl 3 .6H 2 O per litre. 4.3
27、 Ammonium hydroxide solution, containing 2 ml of 20 % NH 4 OH per litre. 4.4 Test control: A dyeing of Cl Mordant Red 3 (Colour Index, 3rd Edition) treated with potassium dichromate. The test control is prepared by entering a well wetted-out pattern of wool cloth at 40 C into a dye-bath containing 1
28、% Cl Mordant Red 3 (Colour Index, 3rd Edition), 10 % sodium sulfate decahydrate (Na 2 SO 4 .10H 2 O) and 3 % acetic acid(300 g/l), all percentages being calculated on the mass of the pattern, at a liquor ratio of 40 : 1. The dye-bath is raised to the boil in 30 min and boiled for a further 30 min. I
29、f necessary, the dye-bath is exhausted by careful addition of 1% to3% acetic acid (300 g/l) or 1% sulfuric acid( 1,84 g/ml), well diluted with water. The bath is boiled for a further 15 min after addition of the acid. The dye-bath is cooled down by addition of cold water, and 0,5 % potassium dichrom
30、ate dissolved in water is added. The dye-bath is raised to the boil again and boiled for 30 min. The pattern is then removed, rinsed in cold, running tap-water and dried. 4.5 Grey scale for assessing change in colour, complying with ISO 105-A02. 5 Test specimen 5.1 If the textile to be tested is fab
31、ric, use a specimen measuring 40 mm 100 mm. 5.2 If the textile to be tested is yarn, knit it into fabric and use a specimen measuring40mm 100mm, or make a wick of parallel lengths 100 mm long and about 5 mm in diameter, tied near both ends. 5.3 If the textile to be tested is loose fibre, comb and co
32、mpress enough of it to form a sheet measuring40mm 100 mm. 6 Procedure 6.1 Carry out the operations described below in 6.2 to 6.5 with the test specimen and the test-control specimen in parallel, in separate baths. 6.2 Immerse the specimen in the aluminium chloride solution (4.2) for 15 min at room t
33、emperature (at a liquor ratio of 20 : 1). Squeeze it to leave in 80 % of its own mass of solution. 6.3 Dry the specimen by hanging it in an oven for30min, or longer if necessary, at 60 C 2 C. Then bake it by heating for 15 min at 115 C 2 C. 6.4 Rinse the specimen for 5 min in cold, running tap-water
34、 and then divide it into two equal parts. Dry one half by hanging it in air at a temperature not exceeding 60 C. 6.5 Agitate the other half for 30 min at room temperature in the ammonium hydroxide solution(4.3) (liquor ratio 40 : 1). Then rinse it for5min in cold, running tap-water and dry it by han
35、ging it in air at a temperature not exceeding60 C.EN ISO 105-X01:1995 4 BSI 11-1999 6.6 Assess the effect on the unneutralized test-control specimen with the grey scale. If the change in colour is not equal to the rating “4-5 yellower” on the appropriate scale, the test has not been carried out corr
36、ectly, and the operations described in 6.1 to 6.5 inclusive shall be repeated with a fresh test specimen and a fresh test-control specimen. 6.7 Assess the change in colour of each half of the test specimen with the grey scale. 7 Test report The test report shall include the following particulars: a)
37、 the number and date of publication of this part of ISO 105 (i.e. ISO 105-X01:1993); b) all details necessary for the identification of the sample tested; c) the numerical ratings for change in colour for both the rinsed and the neutralized portions of the test specimen.EN ISO 105-X01:1995 BSI 11-19
38、99 5 Annex ZA (normative) Normative references to international publications with their relevant European publications This European Standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate places in the text and
39、 the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication referred to applies. Pu
40、blication Year Title EN Year ISO 105-A01 1994 Textiles Tests for colour fastness PartA01:General principles of testing EN ISO 105-A01 1994 ISO 105-A03 1993 Textiles Tests for colour fastness PartA03:Grey scale for assessing staining EN 20105-A03 19946 blankBSEN ISO 105-X01:1996 BSI 11-1999 List of r
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