1、BS EN ISO5263-3:2004ICS 85.040NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBRITISH STANDARDPulps Laboratorywet disintegrationPart 3: Disintegration of mechanicalpulps at 85 C (ISO 5263-3:2004)Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 29/06/2009 07:41, Uncontroll
2、ed Copy, (c) BSIThis British Standardwas published under theauthority of the StandardsPolicy and StrategyCommittee on 30 April2009. BSI 2009ISBN 978 0 580 53926 8Amendments/corrigenda issued since publicationDate CommentsBS EN ISO 5263-3:2004National forewordThis British Standard was published by BS
3、I. It is the UK implementation of EN ISO 5263-3:2004. Together with BS EN ISO The UK participation in its preparation was entrusted to TechnicalCommittee PAI/11, Methods of test for paper, board and pulps.A list of organizations represented on this committee can be obtained onrequest to its secretar
4、y.This publication does not purport to include all the necessary provisionsof a contract. Users are responsible for its correct application.Compliance with a British Standard cannot confer immunityfrom legal obligations.5263-1:2004 and BS EN ISO 5263-2:2004 it supersedes BS EN ISO 5263:1997 which is
5、 withdrawn.Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 29/06/2009 07:41, Uncontrolled Copy, (c) BSIEUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN ISO 5263-3September 2004ICS 85.040 Supersedes EN ISO 5263:1997 English versionPulps - Laboratory wet disintegration - Part 3: Disintegration
6、 ofmechanical pulps at 85 degrees C (ISO 5263-3:2004)Ptes - Dsintgration humide en laboratoire - Partie 3:Dsintgration des ptes mcaniques 85 degrs C(ISO 5263-3:2004)This European Standard was approved by CEN on 2 August 2004.CEN members are bound to comply with the CEN/CENELEC Internal Regulations w
7、hich stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Stan
8、dard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standar
9、ds bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE
10、 FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2004 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN ISO 5263-3:2004: ELicensed Copy: Wang Bin, IS
11、O/EXCHANGE CHINA STANDARDS, 29/06/2009 07:41, Uncontrolled Copy, (c) BSIBS EN ISO 5263-3:2004ISO 5263-3:2004(E) ISO 2004 All rights reserved iiiContents Page Foreword iv 1 Scope 1 2 Normative references . 1 3 Definition 1 4 Apparatus. 2 5 Preparation of test portion. 2 6 Procedure. 3 7 Test report 4
12、 Annex A (normative) Construction of the Standard disintegrator 5 Annex B (normative) Checking the Standard disintegrator. 7 Annex C (normative) Circulation disintegrator . 8 Annex D (informative) The effect of latency in mechanical pulps. 9 Bibliography . 11 Licensed Copy: Wang Bin, ISO/EXCHANGE CH
13、INA STANDARDS, 29/06/2009 07:41, Uncontrolled Copy, (c) BSIBS EN ISO 5263-3:2004ISO 5263-3:2004(E) iv ISO 2004 All rights reservedForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing Intern
14、ational Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with
15、 ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical
16、 committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to
17、the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 5263-3 was prepared by Technical Committee ISO/TC 6, Paper, board and pulps, Subcommittee SC 5, Test methods and qualit
18、y specifications for pulps. This first edition cancels and partially replaces ISO 5263:1995 which has been technically revised. In the revision, ISO 5263 has been divided into three parts; Part 1 which is applicable to chemical pulps, Part 2 which is applicable to mechanical pulps without latency an
19、d Part 3 which is applicable to mechanical pulps exhibiting latency. In Part 3, an informative Annex has been inserted describing the effect of latency in mechanical pulps. ISO 5263 consists of the following parts, under the general title Pulps Laboratory wet disintegration: Part 1: Disintegration o
20、f chemical pulps Part 2: Disintegration of mechanical pulps at 20 C Part 3: Disintegration of mechanical pulps at W 85 C Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 29/06/2009 07:41, Uncontrolled Copy, (c) BSIBS EN ISO 5263-3:2004INTERNATIONAL STANDARD ISO 5263-3:2004(E) ISO 2004 All righ
21、ts reserved 1Pulps Laboratory wet disintegration Part 3: Disintegration of mechanical pulps at W 85 C 1 Scope This part of ISO 5263 specifies an apparatus and the procedures for the laboratory wet disintegration of mechanical pulps that exhibit latency. This apparatus and procedure are required for
22、preparation of the test portion in a number of other International Standards dealing with pulps. ISO 5263-3 is applicable to all kind of mechanical pulps (i.e. mechanical, semi-chemical and chemi-mechanical pulps) exhibiting latency. Mechanical pulps not exhibiting latency shall be disintegrated acc
23、ording to ISO 5263-2. The procedure specified in ISO 5263-2 should be used to disintegrate all mechanical pulps to be measured for brightness. NOTE Brightness is not significantly altered by the presence of latency; however, hot disintegration of mechanical pulps can lead to significant loss of brig
24、htness. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 638, Pulps Det
25、ermination of dry matter content ISO 4119, Pulps Determination of stock concentration ISO 14487, Pulps Standard water for physical testing 3 Definition For the purposes of this part of ISO 5263, the following definitions apply. 3.1 disintegration of mechanical pulp mechanical treatment in water so t
26、hat interlaced fibres, which were free in the pulp stock, are again separated from one another without appreciably changing their structural properties 3.2 latency condition of a mechanical pulp in which some of its properties are inhibited and require disintegration of the pulp at elevated temperat
27、ure to be developed Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 29/06/2009 07:41, Uncontrolled Copy, (c) BSIBS EN ISO 5263-3:2004ISO 5263-3:2004(E) 2 ISO 2004 All rights reservedNOTE 1 Latency is due to the distorted form of the fibres, acquired in mechanical processing, especially at hig
28、h consistency, and subsequently preserved upon cooling at high consistency. It is assumed that its preservation is caused by the hardening of the lignin. NOTE 2 The degree of latency in a pulp is generally related to the consistency and energy applied during the mechanical processing. 3.3 latency re
29、moval procedure using a combination of mechanical treatment, i.e. disintegration, and heat treatment using a temperature exceeding the softening temperature of lignin NOTE In this part of ISO 5263, the temperature for latency removal is stated to be not less than 85 C. 4 Apparatus Ordinary laborator
30、y apparatus and the following: 4.1 Disintegrator with heat supply or hot-water supply capable of maintaining a temperature of W 85 C in the suspension during the entire disintegration procedure. Use either the Standard disintegrator (4.1.1) or the Circulation disintegrator (4.1.2). Since the two typ
31、es of disintegrator do not treat the fibres in the same way (see 6), the disintegrator used must be reported. 4.1.1 Standard disintegrator, constructed as described in Annex A. For latency removal, the Standard disintegrator shall be equipped with an electrically heated container or shall have a sup
32、ply of hot water, capable of keeping the temperature of the fibre-water suspension at the temperature stated in 4.1. NOTE 1 The procedure for checking the Standard disintegrator is given in Annex B. NOTE 2 For safety reasons, it is not recommended to use a Standard disintegrator intended for disinte
33、gration at 20 C and an electric hot plate for boiling water. 4.1.2 Circulation disintegrator, of Domtar type, constructed as described in Annex C. The disintegrator shall have a supply of water of a temperature of between 90 C and 95 C. There must be a means of running the pump for short intervals o
34、f time. To prevent damage to the pump, the pump must not run dry for more than 3 s. 4.2 Balance, capable of weighing with an accuracy of 0,2 g. 4.3 Standard water, for physical testing, as specified in ISO 14487. 5 Preparation of test portion If the pulp is wet or air-dry, determine the dry matter c
35、ontent in accordance with ISO 638. If the pulp is in slush form, determine the dry matter content in accordance with ISO 4119. If the concentration of a slush pulp sample is less than 1,5 % by mass, thicken it to the appropriate volume, carefully avoiding the loss of fines. This is most easily done
36、by sedimentation of the suspension and removing a part of the water phase or by dewatering through a filter paper on a Bchner funnel. Use standard water (4.3) for disintegrating pulps to be used in tests where drainability properties are of importance. In all cases, use water of the same quality as
37、required in the procedure for which the pulp is disintegrated. Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 29/06/2009 07:41, Uncontrolled Copy, (c) BSIBS EN ISO 5263-3:2004ISO 5263-3:2004(E) ISO 2004 All rights reserved 3For the Standard disintegrator (4.1.1), take a test portion correspo
38、nding to a mass of (50 5) g of oven-dry pulp. For the Circulation disintegrator (4.1.2), take a test portion corresponding to a mass of (56 1) g of oven-dry pulp. If the sample is in sheet-form, do not cut the sheets and avoid taking cut edges. If the dry matter comprises 20 % or more of the sample,
39、 soak the test portion in 1 l to 1,5 l of water (standard water or other) at (20 5) C for at least the minimum soaking time specified in Table 1. If the pulp is in the form of sheets or slabs, after soaking tear the sample into pieces of dimensions approximately 25 mm 25 mm. Soaking for a time longe
40、r than the minimum specified, for example overnight, has been found not to have any significant effect on the results. The soaking time shall, however, never be longer than 24 h for any pulp grade. NOTE Flash-dried mechanical pulp needs to be soaked for a minimum of 10 min. Table 1 Recommended soaki
41、ng time for mechanical pulps Dry matter content of the pulp, % by mass Minimum soaking time 60 4 hWhere necessary for climatic reasons, a temperature of between 25 C and 30 C may be used, provided that this is stated in the test report. 6 Procedure 6.1 Disintegration and latency removal WARNING Sinc
42、e the hot-disintegration procedure involves the treatment of the test portion at a temperature exceeding 85 C, cautions must be taken to prevent scalding. Information regarding the effect of latency in mechanical pulps (or in pulps having a high lignin content) is given in Annex D. 6.2 Standard disi
43、ntegrator Transfer the test portion, after preparing as described in Clause 5, into the container of the Standard disintegrator (4.1.1). Add water of the same quality as used in Clause 5 to give a total volume of (2 500 25) ml. Use the heater to heat the mixture to W 85 C. Set the revolution counter
44、 to zero. Switch the motor on and allow the propeller to make 30 000 revolutions. Stop the propeller and check visually that the pulp is completely disintegrated, for instance by diluting a small portion from the disintegrator with water in a glass cylinder and inspecting it under transmitted light.
45、 If it is not completely disintegrated, continue the disintegration until complete separation of fibres is achieved and/or the fibre bundles and fragments are separated to the extent expected in the pulp at the time of manufacture. At the end of the disintegration, the temperature shall not be less
46、than 85 C. If for any reason a different pulp charge or a different number of revolutions is used, this shall be stated in the test report. Immediately after disintegration, dilute the pulp suspension using cold water of the same quality as used in Clause 5, to a concentration not less than 3 g/l. I
47、f necessary, cool the suspension to approximately 20 C. Licensed Copy: Wang Bin, ISO/EXCHANGE CHINA STANDARDS, 29/06/2009 07:41, Uncontrolled Copy, (c) BSIBS EN ISO 5263-3:2004ISO 5263-3:2004(E) 4 ISO 2004 All rights reserved6.3 Circulation disintegrator To heat the Circulation disintegrator (4.1.2)
48、, fill the disintegrator container with water at a temperature between 90 C and 95 C to within 4 cm of the top of the container. Close the lid tightly. Start the recirculation pump and allow it to operate for (2,0 0,1) min. After the pump has stopped, open the drain of the container slightly and mea
49、sure the temperature of the water leaving the container. Drain the water completely and repeat this cycle until this temperature exceeds 90 C. NOTE This preliminary step with hot water is done to heat the container, piping and pump. Immediately add water, of the same quality as used in Clause 5, at a temperature between 90 C and 95 C until the container is approximately half-full. Transfer the test portion, after preparing as described in Clause 5, to the Circulation-disintegrator container a
