1、BRITISH STANDARD BS EN ISO 10426-3:2004 Incorporating Amendment No. 1 to BS ISO 10426-3:2003 (renumbers the BS ISO as BS EN ISO 10426-3:2004) Petroleum and natural gas industries Cements and materials for well cementing Part 3: Testing of deepwater well cement formulations The European Standard EN I
2、SO 10426-3:2004 has the status of a British Standard ICS 75.020; 91.100.10 BS EN ISO 10426-3:2004 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 10 September 2003 BSI 10 January 2005 ISBN 0 580 42595 9 National foreword This British Standard
3、 is the official English language version of EN ISO 10426-3:2004. It is identical with ISO 10426-3:2003. The UK participation in its preparation was entrusted by Technical Committee PSE/17, Materials and equipment for petroleum, petrochemical and natural gas industries, to Subcommittee PSE/17/-/3, D
4、rilling and completion fluids and well cements, which has the responsibility to: A list of organizations represented on this subcommittee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to in this doc
5、ument may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract
6、. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for c
7、hange, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page, pages ii to v, a blank
8、 page, pages 1 to 13, the annex ZA page, an inside back cover and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. Date Comments 15502 10 January 2005 Implementation of the European StandardEUR
9、OPEANSTANDARD NORMEEUROPENNE EUROPISCHENORM ENISO104263 October2004 ICS91.100.10;75.020 Englishversion PetroleumandnaturalgasindustriesCementsandmaterials forwellcementingPart3:Testingofdeepwaterwellcement formulations(ISO104263:2003) IndustriesduptroleetdugaznaturelCimentset matriauxpourlacimentati
10、ondespuitsPartie3:Essais deformulationsdecimentpourpuitseneauprofonde(ISO 104263:2003) ErdlundErdgasindustrieZementeundMaterialenfr dieZementationvonTiefbohrungenTeil3:Prfungvon UnterwasserBohrlochzement(ISO104263:2003) ThisEuropeanStandardwasapprovedbyCENon30September2004. CENmembersareboundtocompl
11、ywiththeCEN/CENELECInternalRegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithoutanyalteration.Uptodatelistsandbibliographicalreferencesconcernings uchnational standardsmaybeobtainedonapplicationtotheCentralSecretariatortoanyCENmember. ThisEuropeanSt
12、andardexistsinthreeofficialversions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCENmemberintoitsownlanguageandnotifiedtotheCentralSecretariathasthesamestatusast heofficial versions. CENmembersarethenationalstandardsbodiesofAustria,Belgium,Cyprus,Czech
13、Republic,Denmark,Estonia,Finland,France, Germany,Greece,Hungary,Iceland,Ireland,Italy,Latvia,Lithuania,Luxembourg,Malta,Netherlands,Norway,Poland,Portugal, Slovakia, Slovenia,Spain,Sweden,SwitzerlandandUnitedKingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPENDENORMALISATION EUROPISCHESKOMITEEF
14、RNORMUNG ManagementCentre:ruedeStassart,36B1050Brussels 2004CEN Allrightsofexploitationinanyformandbyanymeansreserved worldwideforCENnationalMembers. Ref.No.ENISO104263:2004:EEN SIO 014-623:)E( 4002 2 Foreword The text of ISO 10426-3:2003 has been prepared by Technical Committee ISO/TC 67 “Materials
15、, equipment and offshore structures for petroleum and natural gas industries“ of the International Organization for Standardization (ISO) and has been taken over as EN ISO 10426- 3:2004 by Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum and natural gas indus
16、tries“ the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2005, and conflicting national standards shall be withdrawn at the latest by April 2005. Acc
17、ording to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithu
18、ania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Endorsement notice The text of ISO 10426-3:2003 has been approved by CEN as EN ISO 10426-3:2004 without any modifications. NOTE Normative references to International Sta
19、ndards are listed in annex ZA (normative). ENISO104263:2004 Reference number ISO 10426-3:2003(E)INTERNATIONAL STANDARD ISO 10426-3 First edition 2003-08-15 Petroleum and natural gas industries Cements and materials for well cementing Part 3: Testing of deepwater well cement formulations Industries d
20、u ptrole et du gaz naturel Ciments et matriaux pour la cimentation des puits Partie 3: Essais de formulations de ciment pour puits en eau profonde 3002:362401OSISBENISO104263:2004ISO 10426-3:2003(E) DPlcsid Fremia ihTs PDF file mya ctnoian emdebt dedyfepcaes. In ccacnadrow eitA hebods licnesilop gni
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23、sne oeru taht teh file is siutlbae fosu re yb ISO memdob rebeis. In tlnu ehikletneve y ttah lborp aem lertait gno it is f,dnuo plsaee ifnrom ttneC ehlar Secterirata ta teh serddaig sleb nevwo. ISO 3002 All irthgs erse.devr lnUeto sswrehise specified, on trap fo this lbupictaion maeb y cudorperro de
24、tuilizi den yna form ro na ybm ynae,s lecetrinoc ro mceinahcla, incliduntohp gcoiypodna gn micrfoilm, wittuoh repmissii now nritign from ietI rehSa Ot tsserdda eh ebolw or ISOs memreb i ydobn the cnuotfo yr ttseuqer ehe.r ISO cirypothg fofice saCe tsopale 65 eneG 1121-HC 02 av leT. 4 + 10 947 22 1 1
25、1 xaF0 947 22 14 + 9 74 E-mial coirypthgis.o gro We bwww.is.o groii ISO 3002 Allr ihgtsser edevrBS3002:362401OSIENISO104263:2004 iiiContents Page Foreword iv Introduction v 1 Scope 1 2 Normative references . 1 3 Terms and definitions. 1 4 Sampling 1 5 Preparation of slurry. 2 5.1 Preparation of conv
26、entional cement slurry 2 5.2 Preparation of speciality cement slurries. 2 6 Strength tests for deepwater well cements 2 6.1 General information 2 6.2 Sampling methods 2 6.3 Preparation of slurry. 2 6.4 Non-destructive sonic testing . 3 6.5 Destructive testing 4 6.6 Strength determination. 6 7 Thicke
27、ning-time tests for deepwater well cements. 7 7.1 General. 7 7.2 Sampling 7 7.3 Preparation of slurry. 7 7.4 Apparatus. 7 7.5 Test procedures 7 8 Static or stirred fluid-loss test . 8 8.1 Apparatus. 8 8.2 Sampling 8 8.3 Preparation of slurry. 8 8.4 Conditioning procedures . 8 9 Deepwater well-simula
28、tion free fluid and slurry stability tests 9 9.1 General. 9 9.2 Sampling 9 9.3 Slurry preparation . 9 9.4 Test procedure 9 10 Determination of rheological properties and gel strength using a rotational viscometer 10 10.1 General. 10 10.2 Sampling 10 10.3 Preparation of slurry. 10 10.4 Apparatus. 10
29、10.5 Procedure. 10 11 Compatibility of wellbore fluids. 11 11.1 General. 11 11.2 Preparation of test fluids 11 11.3 Property determination. 11 Bibliography . 13 3002:362401OSISBENISO104263:2004iv Foreword ISO (the International Organization for Standardization) is a worldwide federation of national
30、standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International
31、 organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules g
32、iven in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at leas
33、t 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 10426-3 was prepared by Technical Committee ISO/TC 67
34、, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids, and well cements. ISO 10426 consists of the following parts, under the general title Petroleum and natural gas industries Cements and materials f
35、or well cementing: Part 1: Specification Part 2: Testing of well cements Part 3: Testing of deepwater well cement formulations Part 4: Preparation and testing of foamed cement slurries at atmospheric pressure The following part is under preparation: Part 5: Determination of shrinkage and expansion o
36、f well cement formulations at atmospheric pressure BSISO104263:2003ENISO104263:2004 vIntroduction The test methods contained in this part of ISO 10426, though generally based on ISO 10426-2, take into account the specialized sampling/testing requirements and unique downhole temperature profiles foun
37、d in deepwater wells. ISO 10426-2 contains no applicable well simulation schedules for deepwater cementing operations. In a deepwater cementing environment, a number of factors impact the thermal history of the cement slurry. These factors include: water depth, mud-line temperature, geothermal gradi
38、ent, the presence or absence of a drilling riser, drilling fluid temperature, ocean current velocity, presence of thermoclines (layers of ocean water separated by temperature), ambient sea-surface temperature, cement mix-water temperature, bulk cement temperature, cement mixing rate, cement heat of
39、hydration, displacement rate, prior circulating and static event history, drill pipe size and mass, casing size and mass, and hole size. Given the number of variables impacting the thermal history of a cement formulation during placement and curing, and the interdependence of many of those variables
40、, the user is directed to employ numerical heat- transfer simulation or actual field measurement to determine the test temperature and the temperature/pressure schedule for the test methods contained in this part of ISO 10426. In this way, the testing of the cement formulation can reflect as closely
41、 as possible the actual temperature profile found during field cementing operations. Numerical modelling may be used to determine the relative magnitude of the input variables so that “most likely” and “less likely” scenarios of temperature history can be assessed. The values of some input variables
42、 may not be known precisely and a range of possible values should be employed. Physical laboratory testing can then be conducted at “most likely” conditions, with some additional testing at “less likely” conditions to determine the sensitivity to well conditions. Sound engineering judgement can then
43、 be applied to assess the risks. These procedures serve not only for the testing of well cements under deepwater well conditions, but may also be used in those circumstances where low seafloor temperatures are found at shallow water depths. Well cements that can be used in deepwater well cementing c
44、an include those of ISO Classes A, C, G or H (as given in ISO 10426-1 1 ), high-alumina cement, appropriate foamed cements, various types of ductile cement compositions, etc. In each deepwater well cementing operation, the cement chosen needs to be fit for purpose. In this part of ISO 10426, where p
45、ractical, United States customary (USC) units are included in parentheses for information. 3002:362401OSISBENISO104263:20043002:362401OSISBENISO104263:2004INTENRATIONAL TSANDADR IS-62401 O3:(3002E)1Petroleum and natural gas industries Cements and materials for well cementing Part 3: Testing of deepw
46、ater well cement formulations 1 Scope This part of ISO 10426 provides procedures for testing well cements and cement blends for use in the petroleum and natural gas industries in a deepwater environment. 2 Normative references The following referenced documents are indispensable for the application
47、of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 10426-2:2003, Petroleum and natural gas industries Cements and materials for well cementing Part 2: Testing of well ce
48、ments ASTM C 109, Standard test method for compressive strength of hydraulic cement mortars 3 Terms and definitions For the purposes of this part of ISO 10426, the terms and definitions given in ISO 10426-2 apply. 4 Sampling Samples of the neat cement or cement blend, solid and liquid additives, and mixing water are required to test a slurry in accordance with this part of ISO 10426. Accordingly, the best available sampling technology should be e
