1、BS ISO 3054:2017Essential oil of lavandin Abrial(Lavandula angustifolia Mill.Lavandula latifolia Medik.),French typeBSI Standards PublicationWB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06BS ISO 3054:2017 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of ISO
2、 3054:2017. The UK participation in its preparation was entrusted to TechnicalCommittee AW/54, Essential oils.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users
3、 are responsible for its correctapplication. The British Standards Institution 2017. Published by BSI StandardsLimited 2017ISBN 978 0 580 89349 0ICS 71.100.60Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of the
4、Standards Policy and Strategy Committee on 28 February 2017.Amendments/Corrigenda issued since publicationDate Text affectedBS ISO 3054:2017 ISO 2017Essential oil of lavandin Abrial (Lavandula angustifolia Mill. Lavandula latifolia Medik.), French typeHuile essentielle de lavandin Abrial (Lavandula
5、angustifolia Mill. Lavandula latifolia Medik.), type FranceINTERNATIONAL STANDARDISO3054Fourth edition2017-02Reference numberISO 3054:2017(E)BS ISO 3054:2017ISO 3054:2017(E)ii ISO 2017 All rights reservedCOPYRIGHT PROTECTED DOCUMENT ISO 2017, Published in SwitzerlandAll rights reserved. Unless other
6、wise specified, no part of this publication may be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address b
7、elow or ISOs member body in the country of the requester.ISO copyright officeCh. de Blandonnet 8 CP 401CH-1214 Vernier, Geneva, SwitzerlandTel. +41 22 749 01 11Fax +41 22 749 09 47copyrightiso.orgwww.iso.orgBS ISO 3054:2017ISO 3054:2017(E)Foreword iv1 Scope . 12 Normative references 13 Terms and def
8、initions . 14 Requirements 25 Flashpoint 36 Sampling 37 Packaging, labelling and marking 3Annex A (informative) Typical chromatograms of the analysis by gas chromatography of the essential oil of lavandin Abrial (Lavandula angustifolia Mill. Lavandula latifolia Medik.), French type . 4Annex B (infor
9、mative) Flashpoint . 7Bibliography 8 ISO 2017 All rights reserved iiiContents PageBS ISO 3054:2017ISO 3054:2017(E)ForewordISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards
10、 is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take p
11、art in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In partic
12、ular the different approval criteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).Attention is drawn to the possibility that some of the elements of
13、this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the development of the document will be in the Introduction and/or on the ISO list of patent declarations received (see w
14、ww .iso .org/ patents).Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement.For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISOs adherence t
15、o the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following URL: www .iso .org/ iso/ foreword .html.This document was prepared by Technical Committee ISO/TC 54, Essential oils.This fourth edition cancels and replaces the third edition (ISO 3054:2001), w
16、hich has been technically revised.iv ISO 2017 All rights reservedBS ISO 3054:2017INTERNATIONAL STANDARD ISO 3054:2017(E)Essential oil of lavandin Abrial (Lavandula angustifolia Mill. Lavandula latifolia Medik.), French type1 ScopeThis document specifies certain characteristics of the essential oil o
17、f lavandin Abrial (Lavandula angustifolia Mill. Lavandula latifolia Medik.), principally produced in France, in order to facilitate assessment of its quality.NOTE This essential oil is also known commercially as oil of lavandin abrialis.2 Normative referencesThe following documents are referred to i
18、n the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO/TS 210, Essential oils General rule
19、s for packaging, conditioning and storageISO/TS 211, Essential oils General rules for labelling and marking of containersISO 212, Essential oils SamplingISO 279, Essential oils Determination of relative density at 20 C Reference methodISO 280, Essential oils Determination of refractive indexISO 592,
20、 Essential oils Determination of optical rotationISO 875, Essential oils Evaluation of miscibility in ethanolISO 1242, Essential oils Determination of acid valueISO 11024 (all parts), Essential oils General guidance on chromatographic profiles3 Terms and definitionsFor the purposes of this document,
21、 the following terms and definitions apply.ISO and IEC maintain terminological databases for use in standardization at the following addresses: IEC Electropedia: available at h t t p :/ www .electropedia .org/ ISO Online browsing platform: available at h t t p :/ www .iso .org/ obp3.1essential oil o
22、f lavandin Abrialessential oil obtained by steam distillation of the freshly cut flowering tops of a particular clone of lavandin (Lavandula angustifolia Mill. Lavandula latifolia Medik.), of the Lamiaceae family, principally produced in FranceNote 1 to entry: For information on CAS number, see ISO/
23、TR 21092. ISO 2017 All rights reserved 1BS ISO 3054:2017ISO 3054:2017(E)4 Requirements4.1 Essential oil of lavandin Abrial shall meet the requirements given in Table 1.Table 1 Requirements for the essential oil of lavandin AbrialCharacteristics Requirements Test methodAppearance Clear mobile liquid
24、Colour Pale yellow Odour Characteristic, resembling lavender, with a slight camphoraceous noteRelative density at 20 C, d20200,887 to 0,897 ISO 279Refractive index at 20 C 1,460 0 to 1,466 0 ISO 280Optical rotation Between -5 and -1,5 ISO 592Miscibility in ethanol 80 % (volume fraction), at 20 CIt s
25、hall not be necessary to use more than 4 volumes of ethanol 70 % (vol-ume fraction) to obtain a clear solu-tion with 1 volume of essential oil.Sometimes, opalescence can arise on continuing the addition of ethanol.ISO 875Acid value Maximum: 1,0 ISO 12424.2 Carry out the analysis of the essential oil
26、 by gas chromatography. Determine the chromatographic profile in accordance with ISO 11024 (all parts). Identify in the chromatogram obtained, the representative and characteristic components shown in Table 2. The proportions of these components, indicated by the integrator, shall be as shown in Tab
27、le 2. This constitutes the chromatographic profile of the essential oil.Table 2 Chromatographic profileComponentMinimum Maximum% %1,8-Cineole 6,0 12,5Limonene 0,5 1,5(Z)-Ocimene 1,4 3,0(E)-Ocimene 2,5 6,0Camphor 7,0 11,0Linalool 28,0 38,0Linalyl acetate 19,0 29,0-Caryophyllene 1,5 2,5Terpinen-4-ol 0
28、,3 1,2Borneol 1,5 3,5Lavandulol 0,4 1,2Lavandulyl acetate 1,0 2,0Myrcene 0,4 0,9-Terpineol 0,3 1,2Hexyl butyrate 0,2 0,5NOTE The chromatographic profile is normative, contrary to typical chromatograms given for information in Annex A.2 ISO 2017 All rights reservedBS ISO 3054:2017ISO 3054:2017(E)5 Fl
29、ashpointInformation on the flashpoint is given in Annex B.6 SamplingSampling shall be performed in accordance with ISO 212.Minimum volume of test sample: 25 ml.NOTE This volume is sufficient to carry out all the tests specified in this document at least once.7 Packaging, labelling and markingThese i
30、tems shall be in accordance with ISO/TS 210 and ISO/TS 211. ISO 2017 All rights reserved 3BS ISO 3054:2017ISO 3054:2017(E)Annex A (informative) Typical chromatograms of the analysis by gas chromatography of the essential oil of lavandin Abrial (Lavandula angustifolia Mill. Lavandula latifolia Medik.
31、), French type4 ISO 2017 All rights reservedBS ISO 3054:2017ISO 3054:2017(E)Peak identification Operating conditionsColumn: capillary; length 50 m; internal diameter 0,2 mmStationary phase: polydimethyl siloxaneFilm thickness: 0,25 mOven temperature: temperature programming from 65 C to 230 C at a r
32、ate of 2 C/minInjector temperature: 230 CDetector temperature: 250 CDetector: flame ionization typeCarrier gas: hydrogenVolume injected: 0,2 lCarrier gas flow rate: 1,1 ml/minSplit ratio: 1/1001 -Pinene 12 Camphor2 Camphene 13 Borneol3 -Pinene 14 Lavandulol4 Myrcene 15 Terpinen-4-ol5 Hexyl acetate 1
33、6 -Terpineol6 1,8-Cineole + -Phellandrene 17 Hexyl butyrate7 Limonene 18 Linalyl acetate8 (Z)-Ocimene 19 Lavandulyl acetate9 (E)-Ocimene 20 -Caryophyllene10 Linalool11 1-Octen-3-yl acetateFigure A.1 Typical chromatogram taken on an apolar column ISO 2017 All rights reserved 5BS ISO 3054:2017ISO 3054
34、:2017(E)Peak identification Operating conditions1 -Pinene + -Thujene 15 Linalool Column: capillary; length 50 m; internal diameter 0,32 mmStationary phase: carbowax 20MaFilm thickness: 0,25 mOven temperature: temperature programming from 65 C to 230 C at a rate of 2 C/minInjector temperature: 230 CD
35、etector temperature: 250 CDetector: flame ionization typeCarrier gas: hydrogenVolume injected: 0,2 lCarrier gas flow rate: 1,1 ml/minSplit ratio: 1/100a Carbowax 20M is an example of a suitable product available commercially. This information is given for the convenience of users of this document an
36、d does not constitute an endorsement by ISO of this product.2 Camphene 16 Linalyl acetate3 -Pinene 17 Caryophyllene4 Myrcene 18 Terpinen-4-ol5 Limonene 19 Lavandulyl acetate6 1,8-Cineole + -Phellandrene 20 Lavandulol (co-eluted)7 (Z)-Ocimene 21 Borneol + -Terpineol8 (E)-Ocimene9 Hexyl acetate10 Terp
37、inolene11 1-Octen-3-yl acetate12 Hexyl butyrate13 1-Octen-3-ol14 CamphorFigure A.2 Typical chromatogram taken on a polar column6 ISO 2017 All rights reservedBS ISO 3054:2017ISO 3054:2017(E)Annex B (informative) FlashpointB.1 General informationFor safety reasons, transport companies, insurance compa
38、nies, and people in charge of safety services require information on the flash points of essential oils, which in most cases are flammable products.A comparative study on the relevant methods of analysis (see ISO/TR 11018) concluded that it was difficult to recommend a single apparatus for standardi
39、zation purposes, given that: there is a wide variation in the chemical composition of essential oils; the volume of the sample needed in certain requirements would be too costly for high priced essential oils; as there are several different types of equipment which can be used for the determination,
40、 users cannot be expected to use one specified type only.Consequently, it was decided to give a mean value for the flashpoint annexed to each International Standard, for information, in order to meet the requirements of the interested parties.The equipment with which this value was obtained has to b
41、e specified.For further information, see ISO/TR 11018.B.2 Flashpoint of the essential oil of lavandin Abrial, French typeThe mean values are +74 C (see NOTE 1) or +77 C (see NOTE 2).NOTE 1 Obtained with “Setaflash”1)equipment.NOTE 2 Obtained with “Luchaire”1)equipment.1) Equipment available commerci
42、ally. This information is given for the convenience of users of this document and does not constitute an endorsement by ISO of this product. ISO 2017 All rights reserved 7BS ISO 3054:2017ISO 3054:2017(E)Bibliography1 ISO 3218, Essential oils Principles of nomenclature2 ISO/TR 11018, Essential oils G
43、eneral guidance on the determination of flashpoint3 ISO/TR 21092, Essential oils Characterization8 ISO 2017 All rights reservedBS ISO 3054:2017BS ISO 3054:2017ISO 3054:2017(E) ISO 2017 All rights reservedICS 71.100.60Price based on 8 pagesThis page deliberately left blankBSI is the national body res
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