1、BSI Standards PublicationPD CEN/TR 16557:2013Automotive fuels HighFAME diesel fuel blends (B11 B30) Background tothe parameters required andtheir respective limits anddeterminationPD CEN/TR 16557:2013 PUBLISHED DOCUMENTNational forewordThis Published Document is the UK implementation of CEN/TR16557:
2、2013.The UK participation in its preparation was entrusted to TechnicalCommittee PTI/2, Liquid Fuels.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users are resp
3、onsible for its correctapplication. The British Standards Institution 2013. Published by BSI StandardsLimited 2013ISBN 978 0 580 81349 8ICS 75.160.20Compliance with a British Standard cannot confer immunity fromlegal obligations.This Published Document was published under the authority of theStandar
4、ds Policy and Strategy Committee on 30 September 2013.Amendments issued since publicationDate Text affectedPD CEN/TR 16557:2013TECHNICAL REPORT RAPPORT TECHNIQUE TECHNISCHER BERICHT CEN/TR 16557 September 2013 ICS 75.160.20 English Version Automotive fuels - High FAME diesel fuel blends (B11 - B30)
5、- Background to the parameters required and their respective limits and determination Carburants pour automobiles - Mlanges de carburants diesel ayant une teneur en EMAG leve (B11 - B30) - Contexte de llaboration des caractristiques requises, de leurs dterminations et de leurs limites respectives Kr
6、aftstoffe fr Kraftfahrzeuge - Dieselkraftstoffmischungen mit hohem FAME-Anteil (B10 - B30) - Hintergrund zu den geforderten Parametern und deren jeweiligen Grenzwerten und Bestimmungen This Technical Report was approved by CEN on 15 June 2013. It has been drawn up by the Technical Committee CEN/TC 1
7、9. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Pol
8、and, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2013 CEN All rights of exploitation
9、 in any form and by any means reserved worldwide for CEN national Members. Ref. No. CEN/TR 16557:2013: EPD CEN/TR 16557:2013CEN/TR 16557:2013 (E) 2 Contents Page Foreword . 3 1 Scope 4 2 Normative references 4 3 Background of the High FAME diesel blends (B11 - B30) taskforce work 5 4 Record of the w
10、ork to date . 6 4.1 Context . 6 4.2 The Task Force 6 4.3 Planning 8 5 The feasibility study 9 5.1 Background 9 5.2 Parameters to be included 10 5.3 Considerations on the parameters 11 5.4 Dyes and markers 18 5.5 Additives . 18 5.6 Sampling . 18 5.7 Pump marking 18 5.8 Parameters considered and not i
11、ncluded in the draft specification 19 6 Conclusions . 21 7 Acknowledgement . 21 Bibliography 22 PD CEN/TR 16557:2013CEN/TR 16557:2013 (E) 3 Foreword This document (CEN/TR 16557:2013) has been prepared by Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of petr
12、oleum, synthetic and biological origin”, the secretariat of which is held by NEN. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. PD C
13、EN/TR 16557:2013CEN/TR 16557:2013 (E)PD CEN/TR 16557:2013CEN/TR 16557:2013 (E) 2 Contents Page Foreword . 3 1 Scope 4 2 Normative references 4 3 Background of the High FAME diesel blends (B11 - B30) taskforce work 5 4 Record of the work to date . 6 4.1 Context . 6 4.2 The Task Force 6 4.3 Planning 8
14、 5 The feasibility study 9 5.1 Background 9 5.2 Parameters to be included 10 5.3 Considerations on the parameters 11 5.4 Dyes and markers 18 5.5 Additives . 18 5.6 Sampling . 18 5.7 Pump marking 18 5.8 Parameters considered and not included in the draft specification 19 6 Conclusions . 21 7 Acknowle
15、dgement . 21 Bibliography 22 PD CEN/TR 16557:2013CEN/TR 16557:2013 (E) 3 Foreword This document (CEN/TR 16557:2013) has been prepared by Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin”, the secretariat of which i
16、s held by NEN. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. PD CEN/TR 16557:2013CEN/TR 16557:2013 (E)PD CEN/TR 16557:2013CEN/TR 165
17、57:2013 (E) 4 1 Scope This Technical Report provides background information to the deliberations within CEN that led to establish a specification for blending from more than 10 % (V/V) up to 30 % (V/V) of fatty acid methyl ester (FAME) in diesel fuel to be used in captive fleet application for desig
18、nated vehicles. It gives guidance and explanations to the producers, blenders, marketers and users of high FAME diesel blends (B11 to B30). The sole designation “Bxx” refers to a FAME-diesel blend where “xx” is the specific FAME content in volume percentage. The connotation “Byy fuel” is used in thi
19、s document for a fuel with a defined range of FAME allowed and having “yy” volume percentage of FAME content as the maximum of that range. NOTE For the purposes of this document, the term “% (m/m)” and “% (V/V)” are used to represent the mass fraction, , and the volume fraction, , respectively. 2 No
20、rmative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendment
21、s) applies. EN 116:1997, Diesel and domestic heating fuels - Determination of cold filter plugging point EN 590, Automotive fuels Diesel Requirements and test methods EN 12662:2008, Liquid petroleum products - Determination of contamination in middle distillates EN 14078:2009, Liquid petroleum produ
22、cts - Determination of fatty acid methyl ester (FAME) content in middle distillates - Infrared spectrometry method EN 14214, Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods EN 15195:2007, Liquid petroleum
23、products - Determination of ignition delay and derived cetane number (DCN) of middle distillate fuels by combustion in a constant volume chamber EN 15751:2009, Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxi
24、dation method EN 16091:2011, Liquid petroleum products - Middle distillates and fatty acid methyl ester (FAME) fuels and blends - Determination of oxidation stability by rapid small scale oxidation method EN 16329:2013, Diesel and domestic heating fuels - Determination of cold filter plugging point
25、- Linear cooling bath method EN ISO 2719:2002, Determination of flash point - Pensky-Martens closed cup method (ISO 2719:2002) EN ISO 3104:1996, Petroleum products - Transparent and opaque liquids - Determination of kinematic viscosity and calculation of dynamic viscosity (ISO 3104:1994) EN ISO 3170
26、, Petroleum liquids - Manual sampling (ISO 3170) EN ISO 3171, Petroleum liquids - Automatic pipeline sampling (ISO 3171) PD CEN/TR 16557:2013CEN/TR 16557:2013 (E) 5 EN ISO 3405:2011, Petroleum products - Determination of distillation characteristics at atmospheric pressure (ISO 3405:2011) EN ISO 367
27、5:1998, Crude petroleum and liquid petroleum products - Laboratory determination of density - Hydrometer method (ISO 3675:1998) EN ISO 5165:1998, Petroleum products - Determination of the ignition quality of diesel fuels - Cetane engine method (ISO 5165:1998) EN ISO 6245:2002, Petroleum products - D
28、etermination of ash (ISO 6245:2001) EN ISO 12185:1996, Crude petroleum and petroleum products - Determination of density - Oscillating U-tube method (ISO 12185:1996) EN ISO 12937:2000, Petroleum products - Determination of water - Coulometric Karl Fischer titration method (ISO 12937:2000) EN ISO 208
29、46:2011, Petroleum products - Determination of sulfur content of automotive fuels - Ultraviolet fluorescence method (ISO 20846:2011) EN ISO 20884:2011, Petroleum products - Determination of sulfur content of automotive fuels - Wavelength-dispersive X-ray fluorescence spectrometry (ISO 20884:2011) 3
30、Background of the High FAME diesel blends (B11 - B30) taskforce work At the 2009 plenary meeting, CEN/TC 19 decided to register the following preliminary work item as described in its active programme of work: Automotive fuels High FAME diesel blends (B10 - B30) Requirements and test methods, under
31、responsibility of WG 24, with the scope to finalise its feasibility study in time to allow WG 24 to report to TC19 in order to make a final decision on activation at 2011 plenary meeting at the latest on the basis of existing related national standards and to consider and solve the comments as prese
32、nted by SUTN during the PWI ballot. An automatic link has been established between the diesel fuel and FAME standards (EN 590 and EN 14214 respectively) and the High FAME diesel blends standard so that modifications to one will be coherent with the other. Captive fleets are in general considered as
33、a group of vehicles that possess specific supply logistics, their own dedicated facilities for storage and distribution and adequate maintenance of the vehicles. As the definitions are widespread around Europe and the group does not wish to contradict specific legal situations in some countries, the
34、 technical definition of captive fleets is left to the national standardization bodies and will be required. The provisional scope would thus read: “This European Standard specifies requirements and test methods for marketed and delivered high FAME (B30) fuel for use in diesel engine vehicles design
35、ed or subsequently adapted to run on high FAME (B30) fuel. High FAME (B30) fuel is a mixture of more than 10 % (V/V) up to 30 % (V/V) fatty acid methyl esters (commonly known as FAME) complying to EN 14214 and automotive diesel fuel complying to EN 590. For maintenance and control reasons it is to b
36、e used in captive fleets that are intended to have an appropriate fuel management.” The group agreed that the national captive fleet description requirement needed to be required in a point in the text. PD CEN/TR 16557:2013CEN/TR 16557:2013 (E)PD CEN/TR 16557:2013CEN/TR 16557:2013 (E) 4 1 Scope This
37、 Technical Report provides background information to the deliberations within CEN that led to establish a specification for blending from more than 10 % (V/V) up to 30 % (V/V) of fatty acid methyl ester (FAME) in diesel fuel to be used in captive fleet application for designated vehicles. It gives g
38、uidance and explanations to the producers, blenders, marketers and users of high FAME diesel blends (B11 to B30). The sole designation “Bxx” refers to a FAME-diesel blend where “xx” is the specific FAME content in volume percentage. The connotation “Byy fuel” is used in this document for a fuel with
39、 a defined range of FAME allowed and having “yy” volume percentage of FAME content as the maximum of that range. NOTE For the purposes of this document, the term “% (m/m)” and “% (V/V)” are used to represent the mass fraction, , and the volume fraction, , respectively. 2 Normative references The fol
40、lowing documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 116:1997, D
41、iesel and domestic heating fuels - Determination of cold filter plugging point EN 590, Automotive fuels Diesel Requirements and test methods EN 12662:2008, Liquid petroleum products - Determination of contamination in middle distillates EN 14078:2009, Liquid petroleum products - Determination of fat
42、ty acid methyl ester (FAME) content in middle distillates - Infrared spectrometry method EN 14214, Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requirements and test methods EN 15195:2007, Liquid petroleum products - Determination o
43、f ignition delay and derived cetane number (DCN) of middle distillate fuels by combustion in a constant volume chamber EN 15751:2009, Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation method EN 16091:201
44、1, Liquid petroleum products - Middle distillates and fatty acid methyl ester (FAME) fuels and blends - Determination of oxidation stability by rapid small scale oxidation method EN 16329:2013, Diesel and domestic heating fuels - Determination of cold filter plugging point - Linear cooling bath meth
45、od EN ISO 2719:2002, Determination of flash point - Pensky-Martens closed cup method (ISO 2719:2002) EN ISO 3104:1996, Petroleum products - Transparent and opaque liquids - Determination of kinematic viscosity and calculation of dynamic viscosity (ISO 3104:1994) EN ISO 3170, Petroleum liquids - Manu
46、al sampling (ISO 3170) EN ISO 3171, Petroleum liquids - Automatic pipeline sampling (ISO 3171) PD CEN/TR 16557:2013CEN/TR 16557:2013 (E) 5 EN ISO 3405:2011, Petroleum products - Determination of distillation characteristics at atmospheric pressure (ISO 3405:2011) EN ISO 3675:1998, Crude petroleum an
47、d liquid petroleum products - Laboratory determination of density - Hydrometer method (ISO 3675:1998) EN ISO 5165:1998, Petroleum products - Determination of the ignition quality of diesel fuels - Cetane engine method (ISO 5165:1998) EN ISO 6245:2002, Petroleum products - Determination of ash (ISO 6
48、245:2001) EN ISO 12185:1996, Crude petroleum and petroleum products - Determination of density - Oscillating U-tube method (ISO 12185:1996) EN ISO 12937:2000, Petroleum products - Determination of water - Coulometric Karl Fischer titration method (ISO 12937:2000) EN ISO 20846:2011, Petroleum product
49、s - Determination of sulfur content of automotive fuels - Ultraviolet fluorescence method (ISO 20846:2011) EN ISO 20884:2011, Petroleum products - Determination of sulfur content of automotive fuels - Wavelength-dispersive X-ray fluorescence spectrometry (ISO 20884:2011) 3 Background of the High FAME diesel blends (B11 - B30) taskforce work At the 2009 plenary meeting, CEN/TC 19 decided to register the following preliminary work item as described in its active programme of work: Automotive fuels High FAME diesel blends (B10 - B30) Requirements and te
