1、CAN/CGSB-3.524-2011Biodiesel (B100) for Blending in Middle Distillate FuelsICS 75.160.20National Standard of CanadaCopyright Canadian General Standards Board Provided by IHS under license with CGSBNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-The CANADIAN GENERAL
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20、opyright Canadian General Standards Board Provided by IHS under license with CGSBNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-NATIONAL STANDARD OF CANADA CAN/CGSB-3.524-2011BIODIESEL (B100) FOR BLENDING IN MIDDLE DISTILLATE FUELSCETTE NORME NATIONALE DU CANADA E
21、ST DISPONIBLE EN VERSIONSFRANAISE ET ANGLAISE.NATIONAL STANDARD OF CANADA CAN/CGSB-3.14-2006Prepared by the Approved by the Canadian General Standards Board Standards Council of CanadaPublished December 2011 by the Canadian General Standards Board Gatineau, Canada K1A 1G6 HER MAJESTY THE QUEEN IN RI
22、GHT OF CANADA, as represented by the Minister of Public Works and Government Services, the Minister responsible for the Canadian General Standards Board (2011). No part of this publication may be reproduced in any form without the prior permission of the publisher.Copyright Canadian General Standard
23、s Board Provided by IHS under license with CGSBNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-CANADIAN GENERAL STANDARDS BOARDCOMMITTEE ON MIDDLE DISTILLATE FUELS(Voting membership at date of approval)ChairmanMitchell, K. Shell Canada Ltd. (Producer)General Intere
24、st CategoryHersant, G. Oleotek Inc.Jaaskelainen, H. ConsultantJacula, T. Maxxam Analytics Inc.Lee, S.W. Natural Resources CanadaPickard, A.L. ConsultantSquires, B. Oti Canada GroupTharby, R.D. Tharby Technology, ConsultantsVidian-Jones, C. Certispec Services Inc.Webster, G. Advanced Engine Technolog
25、y Ltd.Wispinski, D. Alberta Innovates Technology FuturesYuen, W. Saskatchewan Research CouncilProducer CategoryBoulton, L. Husky EnergyCampbell, S. Canadian Bioenergy Corp.Cosentino, J. Afton Chemical Corp.Fenwick, S Archer Daniels Midland Co.Hiscock, R North AtlanticJobin, J.L. Ultramar Ltd.Kenney,
26、 B. Suncor Energy Inc.Lund, C. Imperial Oil Ltd.Malynowsky, E. Innospec Inc.Millard, P GE Water and Process TechnologiesMozdzen, E. Lubrizol Canada Ltd.Norton, K. Biox Corp.Paszti, M. Rothsay Payne, J.P. Infineum Canada Ltd.Porter, S. Canadian Renewable Fuels AssociationRobichaud, S. Irving Oil Ltd.
27、Winters, P. Baker PetroliteRegulator CategoryArchambault, R. Government of QuebecParsons, R. Government of ManitobaRensing, M.J. Government of British ColumbiaCopyright Canadian General Standards Board Provided by IHS under license with CGSBNot for ResaleNo reproduction or networking permitted witho
28、ut license from IHS-,-,-CAN/CGSB-3.524 -2011User CategoryBryksaw, G. General Motors of Canada Ltd.Dickout, S. National DefenceEveleigh, S. Government of Northwest TerritoriesKhan, S. Ministry of Transportation, OntarioLaskowski, S. Canadian Trucking AllianceLeclerc, K. Socit de Transport de MontralL
29、emieux, J. Public Works and Government Services CanadaMcKinstry, R. The Railway Association of CanadaSt-Laurent, A. Canadian Coast GuardStumborg, M. Agriculture and Agri-Food CanadaWhite, D. Government of NunavutSecretary (Non-voting)Jimenez, J. Canadian General Standards BoardAcknowledgment is made
30、 for the translation of this National Standard of Canada by the Translation Bureau of Public Works and Government Services Canada.Copyright Canadian General Standards Board Provided by IHS under license with CGSBNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-1CAN/
31、CGSB-3.524-2011CANADIAN GENERAL STANDARDS BOARDBIODIESEL (B100) FOR BLENDING IN MIDDLE DISTILLATE FUELS1. SCOPE1.1 This standard applies to one grade of biodiesel that is intended for use as a blending component in middle distillate fuels. 1.1.1 Biodiesel meeting this standard is not intended for us
32、e as a fuel in its neat form.1.2 The testing and evaluation of a product against this standard may require the use of materials and/or equipment that could be hazardous. This document does not purport to address all the safety aspects associated with its use. Anyone using this standard has the respo
33、nsibility to consult the appropriate authorities and to establish appropriate health and safety practices in conjunction with any applicable regulatory requirements prior to its use.2. REFERENCED PUBLICATIONS2.1 The following publications are referenced in this standard:2.1.1 Canadian General Standa
34、rds Board (CGSB)CAN/CGSB-3.0 Methods of Testing Petroleum and Associated Products:No. 28.8 Visual Haze Rating of Distillate Fuel Oils CAN/CGSB-3.2 Heating Fuel Oil CAN/CGSB-3.520 Automotive Low-Sulphur Diesel Fuel Containing Low Levels of Biodiesel Esters (B1-B5)CAN/CGSB-3.522 Diesel Fuel Containing
35、 Biodiesel (B6-B20).2.1.2 ASTM InternationalAnnual Book of ASTM Standards (Appendix B).2.1.3 European Committee for Standardization (CEN)EN 14107 Fat and oil derivatives. Fatty acid methyl esters (FAME). Determination of phosphorous content by inductively coupled plasma (ICP) emission spectrometryEN
36、 14110 Fat and oil derivatives. Fatty acid methyl esters (FAME). Determination of methanol contentEN 14112 Fat and oil derivatives. Fatty acid methyl esters (FAME). Determination of oxidation stability (accelerated oxidation test)EN 14538 Fat and oil derivatives. Fatty acid methyl ester (FAME). Dete
37、rmination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)EN 15751 Automotive fuels. Fatty acid methyl ester (FAME) fuel and blends with diesel fuel. Determination of oxidation stability by accelerated oxidation method.2.2 See Appendix C for
38、 regulations that apply to biodiesel.Copyright Canadian General Standards Board Provided by IHS under license with CGSBNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-2 CAN/CGSB-3.524-20112.3 A dated reference in this standard is to the issue specified. An undated
39、reference in this standard is to the latest issue, unless otherwise specified by the authority applying this standard. The sources are given in the Notes section.3. DEFINITIONSThe following definitions apply in this standard:3.1 Biodiesel Mono-alkyl esters of long-chain fatty acids derived from rene
40、wable sources. In its neat form, biodiesel is commonly designated as B100. In the context of this standard the biodiesel is intended as a blending component in a finished diesel fuel or heating oil.3.2 Diesel Fuel A middle distillate fuel composed of hydrocarbons and naturally occurring, petroleum-d
41、erived, non-hydrocarbons, boiling in the range of 130400C, intended for use as a fuel in traditional compression-ignition engines.3.3 Heating Fuel Oil A distillate fuel oil intended for use in liquid-fuel-burning equipment for the generation of heat for domestic and industrial purposes.3.4 Middle Di
42、stillate Fuel A fuel boiling in the range of 130400C composed of hydrocarbons, including naturally occurring, petroleum-derived, non-hydrocarbons. 4. GENERAL REQUIREMENTS4.1 The biodiesel specified shall be long chain alkyl esters and may contain additives designed to improve its properties or perfo
43、rmance.4.2 The biodiesel shall be a stable, homogeneous liquid free from foreign matter likely to clog filters or nozzles or to damage equipment. Haze may be assessed using CAN/CGSB-3.0 No. 28.8 or ASTM D4176, Procedure 2. 4.3 There shall be no intentional addition of used lubricating oils, extraneo
44、us fluids, unconverted triglycerides (such as raw vegetable oils, animal fats, fish oils or used cooking oils), which are not suitable components for use in biodiesel. 5. DETAILED REQUIREMENTSNote: The precision statement of some of the quoted test methods in this standard may not be fully applicabl
45、e.5.1 The biodiesel meeting this standard may contain up to 0.5% by volume middle distillate. Metered volumes shall be reported.5.2 The biodiesel shall comply with the specified limiting values. The specified limiting values shall not be changed. This precludes any allowances for test method precisi
46、on and adding or subtracting digits.5.2.1 For purposes of determining conformance with the specified limiting values, an observed value or a calculated value shall be rounded off to the nearest unit in the last right-hand digit used in expressing the specified limiting value, in accordance with the
47、rounding-off method of ASTM E29. There is one exception (par. 5.5).5.2.2 Where test values differ between two parties, a resolution shall be in accordance with ASTM D3244 in order to determine conformance with the specified limiting values, with the criticality of the limits set at P = 0.5.5.3 Test
48、methods other than those referenced in this standard may be used only if they have been validated in accordance with ASTM D3764 or D6708. These are referred to as validated test methods. 5.3.1 Differences in precision, sensitivity and bias between test methods referenced in the standard and the vali
49、dated test methods shall be noted. Copyright Canadian General Standards Board Provided by IHS under license with CGSBNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-CAN/CGSB-3.524-2011 35.3.2 Validated test methods shall only be used within the bounds of the data covered in their validation.5.3.3 In the e
