DIN EN 13615 Berichtigung 1-2003 Corrigenda to DIN EN 13615 2002-04 German version EN 13615 2001 AC 2002《DIN EN 13615-2002技术勘误》.pdf

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1、Mai 2003Berichtigungen zu DIN EN 13615:2002-04Deutsche Fassung EN 13615:2001/AC:2002Berichtigung 1zuDIN EN 13615Es wird empfohlen, auf der betroffenen Normeinen Hinweis auf diese Berichtigung zu machen.ICS 77.040.30; 77.150.60Corrigenda to DIN EN 13615:2002-04;German version EN 13615:2001/AC:2002Cor

2、rigenda DIN EN 13615:2002-04;Version allemande EN 13615:2001/AC:2002InDIN EN 13615Verfahren fr die Analyse von Zinn in Masseln Bestimmung des Gehaltes an Verunreini-gungselementen in Zinn der Reinheitsgrade 99,90 % und 99,85 % durch Atomspektrometrie;Deutsche Fassung EN 13615:2001ist der letzte wie

3、folgt lautende Absatz von 7.2 zu streichen:Fr die Bestimmung von Antimon in smtlichen Proben und Kupfer in den Proben Nr 1, 2, 3 und 6 wer-den 10 ml der Lsungen in einen 100-ml-Messkolben gegeben und bis zur Marke mit verdnnter Salz-sure (4.4) aufgefllt.Die berichtigte Fassung von 7.2 ist nachfolgen

4、d aufgefhrt.7.2 Vorbereitung der KalibrierlsungenFr die Bestimmung der Verunreinigungen werden jeweils (1,0 0,1) g hochreines Zinn (4.14) gewogenund in jedes von sieben 250-ml-Becherglsern gegeben. 20 ml des Suregemisches (4.8) werden zu-gegeben und der Inhalt bis zum Auflsen erhitzt. Die Lsung wird

5、 abgekhlt und in einen 100-ml-Messkolben gegeben und die in Tabelle 1 angegebenen Mengen der Metall-Stammlsungen werdenzugegeben.Anschlieend wird bis zur Marke mit verdnnter Salzsure (4.4) aufgefllt.Fortsetzung Seite 2Normenausschuss Nichteisenmetalle (FNNE) im DIN Deutsches Institut fr Normung e. V

6、 DIN Deutsches Institut fr Normung e.V. .Jede Art der Vervielfltigung, auch auszugsweise, Ref. Nr. DIN EN 13615:2002-04/Ber 1:2003-05nur mit Genehmigung des DIN Deutsches Institut fr Normung e. V., Berlin, gestattet.Alleinverkauf der Normen durch Beuth Verlag GmbH, 10772 Berlin DIN EN 13615 Ber 1:2

7、003-052Tabelle 1 Volumina der zur Vorbereitung der Kalibrierlsungen zu verwendenden Metall-StammlsungenMetall-StammlsungmlKolbenNrSb4.13.2Cu4.13.4Pb4.13.6Bi4.13.8Cd4.13.10Zn4.13.12Fe4.13.14As4.13.16Al4.13.18Ag4.13.21Ni4.13.23In4.13.251 0,0 0,0 0,0 0,0 0,0 0,0 0,0 0,0 0,0 0,0 0,0 0,02 0,5 0,5 0,5 0,5 0,5 0,5 1,0 1,0 1,0 1,0 1,0 1,03 1,0 1,0 1,0 1,0 1,0 1,0 2,0 2,0 2,0 2,0 2,0 2,04 2,0 2,0 2,0 2,0 2,0 2,0 4,0 3,0 3,0 3,0 3,0 3,05 3,0 3,0 3,0 4,0 3,0 3,0 6,0 4,0 4,0 4,0 4,0 4,06 4,0 4,0 4,0 6,0 4,0 4,0 8,0 5,0 5,0 5,0 5,0 5,07 5,0 5,0 5,0 8,0 5,0 5,0 10,0 6,0 6,0 6,0 6,0 6,0

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