1、June 2013 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 83
2、.180!%3u“2021682www.din.deDDIN EN 302-5Adhesives for load-bearing structures Test methods Part 5: Determination of maximum assembly time under referencedconditions;English version EN 302-5:2013,English translation of DIN EN 302-5:2013-06Klebstoffe fr tragende Holzbauteile Prfverfahren Teil 5: Bestim
3、mung der maximalen Wartezeit bei Referenzbedingungen;Englische Fassung EN 302-5:2013,Englische bersetzung von DIN EN 302-5:2013-06Adhsifs pour structures portantes en bois Mthodes dessai Partie 5: Dtermination du temps dassemblage maximal dans des conditions derfrence;Version anglaise EN 302-5:2013,
4、Traduction anglaise de DIN EN 302-5:2013-06SupersedesDIN V ENV 302-5:2002-03www.beuth.deDocument comprises 12 pagesIn case of doubt, the German-language original shall be considered authoritative.06.13DIN EN 302-5:2013-06 2 A comma is used as the decimal marker. National foreword This document (EN 3
5、02-5:2013) has been prepared by Technical Committee CEN/TC 193 “Adhesives” (Secretariat: AENOR, Spain). The responsible German body involved in its preparation was the Normenausschuss Holzwirtschaft und Mbel (Timber and Furniture Standards Committee), Working Committee NA 042-04-05 AA Spiegelausschu
6、ss zu CEN/TC 193/SC 1 Holzklebung. Amendments This standard differs from DIN V ENV 302-5:2002-03 as follows: a) the title of the standard has been modified; b) the rolling ball method given in DIN V ENV 302-5 has been exchanged by test pieces similar to EN 302-2. Previous editions DIN V ENV 302-5: 2
7、002-03 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 302-5 March 2013 ICS 83.180 Supersedes ENV 302-5:2001English Version Adhesives for load-bearing structures - Test methods - Part 5: Determination of maximum assembly time under referenced conditions Adhsifs pour structures portantes en bois
8、 - Mthodes dessai - Partie 5: Dtermination du temps dassemblage maximal dans des conditions de rfrence Klebstoffe fr tragende Holzbauteile - Prfverfahren - Teil 5: Bestimmung der maximalen Wartezeit bei Referenzbedingungen This European Standard was approved by CEN on 5 February 2013. CEN members ar
9、e bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to
10、the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Ce
11、ntre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithua
12、nia, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels
13、 2013 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 302-5:2013: EEN 302-5:2013 (E) 2 Contents Page Foreword 3 Introduction .4 1 Scope 6 2 Normative references 6 3 Terms and definitions .6 4 Principle 6 5 Apparatus .6 6 Procedure
14、.7 6.1 General 7 6.1.1 Selection of timber.7 6.1.2 Preparation of the bonded members .7 6.1.3 Glue spread level .7 6.2 Screening test 7 6.2.1 General 7 6.2.2 Adhesive application .7 6.2.3 Lay-up .7 6.2.4 Pressing time .8 6.2.5 Conditioning .8 6.2.6 Procedure and evaluation of the screening test 8 6.
15、3 Final test .8 6.3.1 General 8 6.3.2 Pressing time .8 6.3.3 Conditioning .8 6.4 Delamination test procedures 9 6.4.1 Preparation of the test pieces 9 6.4.2 Testing for delamination .9 6.5 Measurement and evaluation of delamination 9 7 Expression of results 9 8 Requirement 10 8.1 Screening test . 10
16、 8.2 Final test 10 9 Test report . 10 DIN EN 302-5:2013-06 EN 302-5:2013 (E) 3 Foreword This document (EN 302-5:2013) has been prepared by Technical Committee CEN/TC 193 “Adhesives”, the secretariat of which is held by AENOR. This European Standard shall be given the status of a national standard, e
17、ither by publication of an identical text or by endorsement, at the latest by September 2013 and conflicting national standards shall be withdrawn at the latest by September 2013. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CE
18、N and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes ENV 302-5:2001. The following modifications have been made: The principle for the determination of maximum assembly time has been totally altered; The rolling ball method has been e
19、xchanged by test pieces similar to EN 3022. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former
20、 Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 302-5:2013-06 EN 302-5:2013 (E) 4 In
21、troduction This document is one of a series dealing with adhesives for use with timber structures, and is published in support of EN 1995, Eurocode 5: Design of timber structures. The series consists of three classification and performance requirements for adhesives for load-bearing timber structure
22、s; phenolic and aminoplastic adhesives (EN 301), one component polyurethane adhesive (EN 15425) and emulsion polymerized isocyanate adhesive (prEN 16254) and all together eleven test methods (EN 302 Parts 1 to 7 and EN 15416 Parts 2 to 5). These European Standards have the following titles: EN 301,
23、Adhesives, phenolic and aminoplastic, for load-bearing timber structures Classification and performance requirements EN 15425, Adhesives One component polyurethane for load bearing timber structures Classification and performance requirements prEN 16254, Adhesives Emulsion polymerized isocyanate (EP
24、I) for load-bearing timber structures Classification and performance requirements EN 302, Adhesives for load-bearing timber structures Test methods Part 1: Determination of longitudinal tensile shear strength Part 2: Determination of resistance to delamination Part 3: Determination of the effect of
25、acid damage to wood fibres by temperature and humidity cycling on the transverse tensile strength Part 4: Determination of the effects of wood shrinkage on the shear strength Part 5: Determination of maximum assembly time under referenced conditions Part 6: Determination of the minimum pressing time
26、 under referenced conditions Part 7: Determination of the working life under referenced conditions EN 15416, Adhesives for load bearing timber structures other than phenolic and aminoplastic Test methods Part 2: Static load test of multiple bondline specimens in compression shear Part 3: Creep defor
27、mation test at cyclic climate conditions with specimens loaded in bending shear Part 4: Determination of open assembly time for one component polyurethane adhesives Part 5: Determination of conventional pressing time Safety statement Persons using this document should be familiar with the normal lab
28、oratory practice, if applicable. This document cannot address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any regulatory conditions. DIN EN 302-5:2013-06 EN 302-5:
29、2013 (E) 5 Environmental statement It is understood that some of the material permitted in this standard can have a negative environmental impact. As technological advantages lead to better alternatives for these materials, they will be eliminated from this standard to the greatest extent possible.
30、At the end of the test, it is recommended that the user of the standard take care to carry out an appropriate disposal of the wastes, according to local regulations. DIN EN 302-5:2013-06 EN 302-5:2013 (E) 6 1 Scope This European Standard specifies a laboratory method of determining the maximum assem
31、bly time at two spread rate levels in standard atmosphere 20/65. This European Standard is intended for obtaining a reliable base of comparison of the maximum assembly time between adhesives at referenced conditions. 2 Normative references The following documents, in whole or in part, are normativel
32、y referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 301, Adhesives, phenolic and aminoplastic, for load-bearing timb
33、er structures Classification and performance requirements EN 302-2:2013, Adhesives for load-bearing timber structures Test methods Part 2: Determination of resistance to delamination EN 923:2005+A1:2008, Adhesives Terms and definitions 3 Terms and definitions For the purposes of this document, the t
34、erms and definitions given in EN 923:2005+A1:2008 and the following apply. 3.1 assembly time time interval under specified conditions from spread of adhesive on the lamellae until the cramping pressure is applied 3.2 maximum assembly time time interval after which an adhesive coat loses its bonding
35、ability 4 Principle Delamination test pieces similar to EN 302-2 are produced with different assembly times for individual bond lines by using 5 mm spacers in the corners. A delamination test is performed to evaluate the maximum assembly time at which the highest allowed delamination value is exceed
36、ed. 5 Apparatus 5.1 Autoclave or similar pressure vessel, as described in EN 302-2. 5.2 Vacuum pump or similar device, as described in EN 302-2. 5.3 Pump or similar device, as described in EN 302-2. 5.4 Air-circulating oven(s) or chamber(s), as described in EN 302-2. DIN EN 302-5:2013-06 EN 302-5:20
37、13 (E) 7 5.5 Balance, as described in EN 302-2. 5.6 Wood chisel and hammer,or similar devices capable of opening the glue lines. 5.7 Spacers, made of wood or hard plastic with a thickness of 5 mm. 6 Procedure 6.1 General NOTE This test method has two stages: screening test (6.2) and final test (6.3)
38、. 6.1.1 Selection of timber Make laminated members out of flat-sawn, straight-grained Norway spruce (Picea abies L.), free of reaction wood, with a density of (450 25) kg/m at 12 % moisture content. Preferably, knot-free wood should be used, but allowances are made for boards with knots up to a maxi
39、mum of 15 mm in diameter, but splay (spike) knot is not allowed. Condition the timber in the standard climate (20 2) C and a relative humidity of (65 5) %) for at least 7 days prior to bonding, ensuring that the timber has a moisture content of (12 1) %. 6.1.2 Preparation of the bonded members For e
40、ach laminated member, prepare six lamellae (150 5) mm wide, (30 1) mm thick and approximately 500 mm long. The desired thickness is achieved by planing 38 mm thick lamellae. Bond the lamellae within 8 h of planing. Within each laminated member assembly, ensure that the six lamellae present the same
41、growth ring orientation. The assembly is produced in climate (20 1) C and (65 2) % relative humidity. A strict climate control is very important as small changes in air temperature and relative humidity will highly influence the drying tendency of the applied adhesive and thus influence the maximum
42、assembly time. The circulation of air should be as low as possible. 6.1.3 Glue spread level The assembly time is determined with two levels of glue spread: 250 g/m and 400 g/m. 6.2 Screening test 6.2.1 General For each level of glue spread (6.1.3) make one laminated member of six lamellae giving fiv
43、e glue lines with different assembly time for each glue line. 6.2.2 Adhesive application Apply the adhesive on one side of the lamellae in accordance with the adhesive manufacturers recommendation, as a glue mix or as separate spread of adhesive and hardener by using a ribbon spreader. 6.2.3 Lay-up
44、Start to apply the adhesive on the top surface of the lamellae number 2. After 2 min open assembly time, place 5 mm thick spacers in each corner and cover the glue line by placing lamellae number 1 on top of lamellae number 2. DIN EN 302-5:2013-06 EN 302-5:2013 (E) 8 Then continue to apply the adhes
45、ive on the top surface of lamellae number 3. After 2 min open assembly time, add 5 mm spacers in each corner and cover the glue line with the assembly consisting of lamellae number 1 and number 2. Continue the same procedure with lamellae number 4, 5 and 6. If the expected assembly time is 30 min th
46、en use 5 min intervals between the glue lines; for expected assembly time 30 min to 60 min, use 10 min intervals; and for expected assembly time 60 min, use 15 min intervals. EXAMPLE If the expected assembly time is 50 min, then start with 30 min assembly time and continue with 40 min, 50 min, 60 mi
47、n and end with 70 min assembly time. 6.2.4 Pressing time After the elapsed time of the assembly times, remove the spacers from the corners and press the laminated member at (20 2) C and (65 5) % relative humidity with a pressure of 0,6 N/mm. The pressing time shall be as recommended by the adhesive
48、manufacturer. 6.2.5 Conditioning After bonding and pressing, but before cutting and testing, condition the assembly for 7 days at (20 2) C and (65 5) % relative humidity. A longer or shorter conditioning time may be used if recommended by the adhesive manufacturer. 6.2.6 Procedure and evaluation of
49、the screening test Prepare the test pieces and follow the test procedure as described in 6.4. If the first screening test does not give a clear indication of the maximum assembly time, all glue lines pass the requirement (delamination less than 4 %). If none of the glue lines pass the requirement or the time intervals for the assembly time between glue lines is too long or too short, then make a second screening test with more appropriate time settings. When the screeni
