1、July 2014 Translation by DIN-Sprachendienst.English price group 14No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 1
2、3.030.01!%2w“2158490www.din.deDDIN EN 16457Characterization of waste Framework for the preparation and application of a testing programme Objectives, planning and report;English version EN 16457:2014,English translation of DIN EN 16457:2014-07Charakterisierung von Abfllen Rahmenbedingungen fr die Vo
3、rbereitung und Anwendung einesUntersuchungsprogramms Ziele, Planung und Bericht;Englische Fassung EN 16457:2014,Englische bersetzung von DIN EN 16457:2014-07Caractrisation des dchets Procdure-cadre pour llaboration et la mise en oeuvre dun programme dessai Objectifs, planification et rapport;Version
4、 anglaise EN 16457:2014,Traduction anglaise de DIN EN 16457:2014-07www.beuth.deIn case of doubt, the German-language original shall be considered authoritative.Document comprises 28 pages 05.14 DIN EN 16457:2014-07 2 A comma is used as the decimal marker. National foreword This document (EN 16457:20
5、14) has been prepared by Technical Committee CEN/TC 292 “Characterization of waste” (Secretariat: NEN, Netherlands). The national standards bodies listed in the foreword are bound to adopt this European Standard in its entirety and without any modifications. The responsible German body involved in i
6、ts preparation was the Normenausschuss Wasserwesen (Water Practice Standards Committee), Working Committee NA 119-01-02-01 UA Probenahme of NA 119-01-02 AA Abfall- und Bodenuntersuchung. EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 16457 March 2014 ICS 13.030.01 English Version Characterizat
7、ion of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report Caractrisation des dchets - Procdure-cadre pour llaboration et la mise en oeuvre dun programme dessai -Objectifs, planification et rapport Charakterisierung von Abfllen - Rahmenbedin
8、gungen fr die Vorbereitung und Anwendung eines Untersuchungsprogramms - Ziele, Planung und Bericht This European Standard was approved by CEN on 20 December 2013. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standar
9、d the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English,
10、French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulga
11、ria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Tur
12、key and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2014 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members.
13、Ref. No. EN 16457:2014 EEN 16457:2014 (E) 2 Contents Page Foreword 3 Introduction .4 1 Scope 5 2 Normative references 5 3 Terms and definitions7 4 Defining a waste testing programme .9 4.1 Principles 9 4.2 Structure of a waste testing programme .10 4.3 Parameters to be tested for a waste 12 4.4 Resp
14、onsibilities and programme manager .13 4.5 Standards to be used 14 5 Carrying out a waste testing programme 15 6 Overall testing report .15 Annex A (normative) Matrix testing steps versus parameters specifying the standards to be used in a waste testing programme .17 Annex B (informative) A-deviatio
15、ns .25 Bibliography 26 DINEN 16457:2014-07EN 16457:2014(E)3 Foreword This document (EN 16457:2014) has been prepared by Technical Committee CEN/TC 292 “Characterization of waste”, the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either
16、 by publication of an identical text or by endorsement, at the latest by September 2014 and conflicting national standards shall be withdrawn at the latest by September 2014. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and
17、/or CENELEC shall not be held responsible for identifying any or all such patent rights. It is to be noted that for Germany an A-deviation applies (see Annex B). This document has been prepared by the ad hoc group “Testing programme” of CEN/TC 292. It has been decided by CEN/TC 292 to prepare the pr
18、esent document and to consider separately other issues supporting this document. This would finally result in a set of four documents on waste testing as listed in the Introduction. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are
19、 bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Por
20、tugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DINEN 16457:2014-07EN 16457:2014 (E) 4 Introduction This European Standard was elaborated as a help for those who have to organize and apply a waste testing programme. Often several parameters need to be d
21、etermined in a waste sample and for each parameter different testing steps of a different nature need to be coordinated and performed. This is done in accordance with dedicated standards developed by CEN/TC 292 (e.g. standards for the steps of sampling, extraction, leaching and analysis of eluates o
22、r extracts). In order to cope with these different parameters to be tested and with these different testing steps of different nature, the testing of a waste generally refers to different standards which should be used (and elaborated) in a coherent and coordinated way in a testing programme. This E
23、uropean Standard is designed for specifying such overall testing programmes. This European Standard may be used by different interested parties in waste testing: plant operators, testing institutes, accreditation bodies, etc. as well as by industries to address the waste testing part of their contra
24、cts and by regulators to address the waste testing part of their regulations. This European Standard can be used to: produce a standardized testing programme for use in regular or routine circumstances (elaboration of daughter/derived standards dedicated to well defined testing scenarios); incorpora
25、te the specific testing requirements of European and national legislation; design and develop a waste testing programme for use on a case by case basis. This European Standard provides requirements on the programme, objective, plan and report for the execution of a waste testing programme. This is d
26、one with the intent to ensure reliable and comparable results when using the reference methods that have been developed by CEN/TC 292 in accordance with the principles specified in this standard and in the supporting documents (listed below). As shown in Figures 2 and 3, for waste testing, the tests
27、 to be performed consist (see also the supporting documents listed below) of two main works: the sampling in the field and the analysis-quantification in the laboratory. The needed coordination and interface is the responsibility of the programme manager (see 4.4). It is also the responsibility of t
28、he programme manager to design the testing programme, to authorize the testing report and to submit it to the customer. This European Standard includes one normative annex and one informative annex which are part of this standard. This European Standard is intended to become a part of a set of docum
29、ents consisting of the present document: EN 16457, Characterization of waste Framework for the preparation and application of a testing programme Objective, planning and report and of three supporting documents providing important information: CEN/TS (WI 00292082), Characterization of waste Framewor
30、k for the preparation and application of a testing programme Application of EN ISO/IEC 17025 (in preparation) CEN/TS (WI 00292085), Characterization of waste Framework for the preparation and application of a testing programme Guidelines for the elaboration of standardised testing methods (in prepar
31、ation) CEN/TR (WI 00292084), Characterization of waste Framework for the preparation and application of a testing programme General information on content tests and leaching tests (in preparation) DIN EN 16457:2014-07 EN 16457:2014 (E) 5 1 Scope This European Standard specifies requirements for a wa
32、ste testing programme regarding mainly objectives, planning and report with the intent to ensure reliable and comparable results when using the reference methods that have been developed and/or adopted by CEN/TC 292. The planning and report aspects of this European Standard are applicable to any was
33、te testing programme dedicated to the determination of one or several parameters. They are also applicable to all testing steps for each parameter from sampling up to reporting whether these steps are taking place in the field (e.g. sampling) or in the laboratory (e.g. analysis-quantification). This
34、 European Standard does not address aspects of safety for activities in the field and inside laboratory. NOTE The term planning a testing programme is used here with the general meaning of organizing a testing programme and being in accordance with the terms testing plan, sampling plan, laboratory p
35、lan used in the present European Standard. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of t
36、he referenced document (including any amendments) applies.1)EN 12457-1, Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 1: One stage batch test at a liquid to solid ratio of 2 l/kg for materials with high solid content and with parti
37、cle size below 4 mm (without or with size reduction) EN 12457-2, Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 2: One stage batch test at a liquid to solid ratio of 10 l/kg for materials with particle size below 4 mm (without or wi
38、th size reduction) EN 12457-3, Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 3: Two stage batch test at a liquid to solid ratio of 2 l/kg and 8 l/kg for materials with high solid content and with particle size below 4 mm (without o
39、r with size reduction) EN 12457-4, Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 4: One stage batch test at a liquid to solid ratio of 10 l/kg for materials with particle size below 10 mm (without or with size reduction) EN 13137,
40、Characterization of waste - Determination of total organic carbon (TOC) in waste, sludges and sediments EN 13656, Characterization of waste - Microwave assisted digestion with hydrofluoric (HF), nitric (HNO3) and hydrochloric (HCl) acid mixture for subsequent determination of elements EN 13657, Char
41、acterization of waste - Digestion for subsequent determination of aqua regia soluble portion of elements EN 14039, Characterization of waste - Determination of hydrocarbon content in the range of C10 to C40 by gas chromatography EN 14345, Characterization of waste - Determination of hydrocarbon cont
42、ent by gravimetry 1) Useful information may be found in several CEN/TRs as mentioned in Annex A. The use of CEN/TRs is not mandatory and other sources of information may be used provided that the requirements of the basic EN or CEN/TS are fulfilled. The list of such CEN/TR is given in the Bibliograp
43、hy, references 5 to 15. DINEN 16457:2014-07EN 16457:2014 (E) 6 EN 14346, Characterization of waste - Calculation of dry matter by determination of dry residue or water content CEN/TS 14405, Characterization of waste - Leaching behaviour tests - Up-flow percolation test (under specified conditions) p
44、rEN 14429, Characterisation of waste - Leaching behaviour test - Influence of pH on leaching with initial acid/base addition EN 14582, Characterization of waste - Halogen and sulfur content - Oxygen combustion in closed systems and determination methods EN 14735, Characterization of waste - Preparat
45、ion of waste samples for ecotoxicity tests EN 14899, Characterization of waste - Sampling of waste materials - Framework for the preparation and application of a Sampling Plan prEN 14997, Characterisation of waste - Leaching behaviour test - Influence of pH on leaching with continuous pH control EN
46、15002, Characterization of waste - Preparation of test portions from the laboratory sample EN 15169, Characterization of waste - Determination of loss on ignition in waste, sludge and sediments EN 15192, Characterisation of waste and soil - Determination of Chromium(VI) in solid material by alkaline
47、 digestion and ion chromatography with spectrophotometric detection EN 15308, Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by using capillary gas chromatography with electron capture or mass spectrometric detection EN 15309, Characterization of
48、 waste and soil - Determination of elemental composition by X-ray fluorescence EN 15216, Characterization of waste - Determination of total dissolved solids (TDS) in water and eluates CEN/TS 15364, Characterization of waste - Leaching behaviour tests - Acid and base neutralization capacity test EN 15527, Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS) CEN/TS 15862, Characterisation of waste - Compliance leach
