1、October 2010 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS
2、 59.080.01!$kUW“1725052www.din.deDDIN EN ISO 105-D01Textiles Tests for colour fastness Part D01: Colour fastness to dry cleaning using perchloroethylenesolvent (ISO 105-D01:2010)English translation of DIN EN ISO 105-D01:2010-10Textilien Farbechtheitsprfungen Teil D01: Bestimmung der Trockenreinigung
3、sechtheit mit Perchlorethylen-Lsemittel(ISO 105-D01:2010)Englische bersetzung von DIN EN ISO 105-D01:2010-10Textiles Essais de solidit des coloris Partie D01: Solidit des coloris au nettoyage sec au perchlorthylne(ISO 105-D01:2010)Traduction anglaise de DIN EN ISO 105-D01:2010-10SupersedesDIN EN ISO
4、 105-D01:1995-04www.beuth.deIn case of doubt, the German-language original shall be considered authoritative.Document comprises 12 pages10.10 DIN EN ISO 105-D01:2010-10 2 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee ISO/TC 38 “Textil
5、es” in collaboration with Technical Committee CEN/TC 248 “Textiles and textile products” (Secretariat: BSI, United Kingdom). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Working Committee NA 062-05-11 AA Farbe
6、chtheit von Textilien Deutsche Echtheitskommission DEK. The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 105-A01 DIN EN ISO 105-A01 ISO 105-A02 DIN EN 20105-A02 ISO 105-A03 DIN EN 20105-A03 ISO 105-A05 DIN EN ISO 105-A05 Amendments This
7、standard differs from DIN EN ISO 105-D01:1995-04 as follows: a) the title of the standard has been changed; b) in Clause 1 “Scope”, perchloroethylene has been specified as solvent; c) in Clause 2 “Normative references”, ISO 105-A05 has been added; d) the former clause relating to apparatus and reage
8、nts has been subdivided into two clauses; e) the description of the procedure (Clause 8) has been given in more detail; f) staining of the adjacent fabrics has been specified; g) the numerical grey scale rating for staining of the solvent has been deleted; h) Annex ZA has been deleted. Previous edit
9、ions DIN 54024: 1966-10, 1971-02, 1984-08 DIN EN ISO 105-D01: 1995-04 DIN EN ISO 105-D01:2010-10 3 National Annex NA (informative) Bibliography DIN EN ISO 105-A01, Textiles Tests for colour fastness Part A01: General principles of testing DIN EN 20105-A02, Textiles Tests for colour fastness Part A02
10、: Grey scale for assessing change in colour DIN EN 20105-A03, Textiles Tests for colour fastness Part A03: Grey scale for assessing staining DIN EN ISO 105-A05, Textiles Tests for colour fastness Part A05: Instrumental assessment of change in colour for determination of grey scale DIN EN ISO 105-D01
11、:2010-10 4 This page is intentionally blank EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 105-D01 May 2010 ICS 59.080.01 Supersedes EN ISO 105-D01:1995English Version Textiles - Tests for colour fastness - Part D01: Colour fastness Textiles - Essais de solidit des coloris - Partie D01: So
12、lidit des coloris au nettoyage sec au perchlorthylne (ISO 105-D01:2010) Textilien - Farbechtheitsprfungen - Teil D01: Bestimmung der Trockenreinigungsechtheit mit Perchlorethylen-Lsemittel (ISO 105-D01:2010) This European Standard was approved by CEN on 29 April 2010. CEN members are bound to comply
13、 with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Managemen
14、t Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the o
15、fficial versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,
16、Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN All rights of exploitation in any form and by any means reserved world
17、wide for CEN national Members. Ref. No. EN ISO 105-D01:2010: E(ISO 105-D01:2010) to dry cleaning using perchloroethylene solvent2 DIN EN ISO 105-D01:2010-10 EN ISO 105-D01:2010 (E) Contents Page Foreword3 1 Scope 4 2 Normative references 4 3 Principle5 4 Safety 5 5 Reagents and materials 5 6 Apparat
18、us .5 7 Test specimen6 8 Procedure .6 9 Test report 7 Bibliography8 3 Foreword This document (EN ISO 105-D01:2010) has been prepared by Technical Committee ISO/TC 38 “Textiles” in collaboration with Technical Committee CEN/TC 248 “Textiles and textile products” the secretariat of which is held by BS
19、I. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by November 2010, and conflicting national standards shall be withdrawn at the latest by November 2010. Attention is drawn to the possibility that s
20、ome of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 105-D01:1995. According to the CEN/CENELEC Internal Regulations, the national standards organizati
21、ons of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal
22、, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 105-D01:2010 has been approved by CEN as a EN ISO 105-D01:2010 without any modification. DIN EN ISO 105-D01:2010-10 EN ISO 105-D01:2010 (E) 1 Scope This part of ISO 105 specifies a me
23、thod for determining the resistance of the colour of textiles of all kinds and in all forms to drycleaning using perchloroethylene solvent. This method is neither suitable for the evaluation of the durability of textile finishes, nor is it intended for use in evaluating the resistance of colours to
24、spot and stain removal procedures used by the drycleaner. This test covers colour fastness to drycleaning only; commercial drycleaning practice normally involves other operations, such as water spotting, solvent spotting and steam pressing, etc., for which other standard test methods are available i
25、f the full response to drycleaning of a textile is to be assessed. The presence of absorbed water in drycleaning solvent, or the presence of a detergent and water in a drycleaning solvent, are known to alter the colour fastness properties of some materials. This test requires the assessment of the m
26、aterial under test in a dry state, using solvent alone, within containers that do not contain water. Fastness to drycleaning, without further qualification in this part of ISO 105, means fastness to drycleaning in perchloroethylene. However, if required, other solvents that are used for textile clea
27、ning can be used. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 105-
28、A01:2010, Textiles Tests for colour fastness Part A01: General principles of testing ISO 105-A02, Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour ISO 105-A03, Textiles Tests for colour fastness Part A03: Grey scale for assessing staining ISO 105-A04, Textiles T
29、ests for colour fastness Part A04: Method for the instrumental assessment of the degree of staining of adjacent fabrics ISO 105-A05, Textiles Tests for colour fastness Part A05: Instrumental assessment of change in colour for determination of grey scale rating ISO 105-F01, Textiles Tests for colour
30、fastness Part F01: Specification for wool adjacent fabric ISO 105-F02, Textiles Tests for colour fastness Part F02: Specification for cotton and viscose adjacent fabric ISO 105-F03, Textiles Tests for colour fastness Part F03: Specification for polyamide adjacent fabric 4DIN EN ISO 105-D01:2010-10 E
31、N ISO 105-D01:2010 (E) ISO 105-F04, Textiles Tests for colour fastness Part F04: Specification for polyester adjacent fabric ISO 105-F05, Textiles Tests for colour fastness Part F05: Specification for acrylic adjacent fabric ISO 105-F06, Textiles Tests for colour fastness Part F06: Specification for
32、 silk adjacent fabric ISO 105-F07, Textiles Tests for colour fastness Part F07: Specification for secondary acetate adjacent fabric ISO 105-F10, Textiles Tests for colour fastness Part F10: Specification for adjacent fabric: Multifibre 3 Principle A specimen of the textile in contact with a specifie
33、d adjacent fabric or fabrics in a cotton fabric bag, together with non-corrodible steel discs, is agitated in perchloroethylene (see Clause 1), then squeezed or centrifuged, and dried in hot air. The change in colour of the specimen and the staining of the adjacent fabric or fabrics are assessed wit
34、h reference to the original specimen, either with grey scales or instrumentally. 4 Safety Perchloroethylene and other solvents may be injurious to human health. It is therefore important to follow guidelines for the safe use of solvents. It is recommended that testing be carried out in a well-ventil
35、ated area and that containers of solvent opened only within the confines of a fume cabinet or hood. It is also recommended that protective gloves and goggles worn, and that skin contact with solvents and inhalation of solvent fumes avoided. Guidelines for the safe disposal of solvents should be rigo
36、rously followed. 5 Reagents and materials 5.1 Perchloroethylene (otherwise known as tetrachloroethene or tetrachloroethylene) solvent, a general-purpose reagent shall be used, which shall be stored over anhydrous sodium carbonate to neutralize any hydrochloric acid formed. 5.2 Adjacent fabrics, in a
37、ccordance with ISO 105-A01. Either 5.2.1 Multifibre adjacent fabric, Type DW or Type TV, complying with ISO 105-F10. Or 5.2.2 Two single-fibre adjacent fabrics, complying with the relevant parts: ISO 105-F01 to ISO 105-F07. One of the two adjacent fabrics shall be made of the textile to be tested or
38、 that predominating in the case of blends, and the second fabric shall be made of the fibre indicated second in order of predominance, or as otherwise specified. 5.2.3 Non-dyeable fabric (for example polypropylene), if required. 5.3 Cotton twill cloth, bleached, undyed, free of finishes, of mass per
39、 unit area (270 70) g/m2. 5.4 Non-corrodible (stainless) steel discs, (30 2) mm diameter (3 0,5) mm height, smooth and free from rough edges, of mass (20 2) g. 5.5 Grey scale for assessing change in colour, in accordance with ISO 105-A02. 5.6 Grey scale for assessing staining, in accordance with ISO
40、 105-A03. 5DIN EN ISO 105-D01:2010-10 EN ISO 105-D01:2010 (E) 6 Apparatus 6.1 Suitable mechanical device, consisting of a water bath and containing a rotating shaft which supports, radially, stainless steel containers with a diameter of (75 5) mm and a height of (125 10) mm, of capacity (550 50) ml,
41、 the bottom of the containers being (45 10) mm from the centre of the shaft. The containers shall be closed using solvent-resistant gaskets. 6.1.1 The shaft/container assembly is rotated at a frequency of (40 2) min1. The temperature of the water bath is thermostatically controlled to maintain the t
42、est solvent at (30 2) C. 6.1.2 Other mechanical devices may be used for the tests, provided that it can be demonstrated that the results are identical with those obtained by the apparatus described in 6.1. 6.2 Fume cabinet or hood, with sufficient attributes to confine solvent vapour and thereby pro
43、tect human health. 6.3 Spectrophotometer or colorimeter for assessing change in colour and staining, complying with ISO 105-A04 and ISO 105-A05. 7 Test specimen 7.1 If the textile to be tested is fabric, follow the procedure in either 7.1.1 or 7.1.2. 7.1.1 Attach a specimen of (100 2) mm (40 2) mm t
44、o a piece of the multifibre adjacent fabric (5.2.1), also measuring (100 2) mm (40 2) mm, by sewing along one of the shorter edges, with the multifibre adjacent fabric next to the face side of the specimen. 7.1.2 Attach a specimen of (100 2) mm (40 2) mm between the two single-fibre adjacent fabrics
45、 (5.2.2), also measuring (100 2) mm (40 2) mm, by sewing along one of the shorter edges. 7.2 Yarn may be knitted into fabric form and tested as prepared in 7.1. Where yarn or loose fibre is to be tested, take a mass of the yarn or loose fibre approximately equal to one-half of the combined mass of t
46、he adjacent fabrics, and position it as described in either 7.2.1 or 7.2.2. 7.2.1 Place it between a (100 2) mm (40 2) mm piece of the multifibre adjacent fabric (5.2.1) and a (100 2) mm (40 2) mm piece of the non-dyeable fabric (5.2.3) and sew them along all four sides (see ISO 105-A01:2010: 10.3,
47、Preparation of composite specimens). 7.2.2 Place it between a (100 2) mm (40 2) mm piece of each of the two specified single-fibre fabrics (5.2.2) and sew along all four sides. 8 Procedure 8.1 Prepare the mechanical device (6.1) by allowing the water bath (see 6.1) to attain its working temperature
48、of (30 2) C. 8.2 Prepare a bag with inside dimensions of 100 mm 100 mm using the undyed cotton twill cloth (5.3) by sewing together two squares of this cloth around three sides. Place the composite specimen and 12 steel discs (5.4) inside the bag. Close the bag by any convenient means. 8.3 Remove th
49、e steel containers (see 6.1) from the mechanical device. Ensure that the interior of each container, including its lid and sealing gasket, are dry. This should be achieved by wiping each containers components with a dry cotton cloth. 8.4 Place the bag containing the composite specimen and the steel discs in the container. 6DIN EN ISO 105-D01:2010-10 EN ISO 105-D01:2010 (E) 8.5 Within the confines of the fume cabin
