1、Januar 2012DEUTSCHE NORM Normenausschuss Erdl- und Erdgasgewinnung (NG) im DINPreisgruppe 14DIN Deutsches Institut fr Normung e. V. Jede Art der Vervielfltigung, auch auszugsweise, nur mit Genehmigung des DIN Deutsches Institut fr Normung e. V., Berlin, gestattet.ICS 75.180.10!$xm“1857499www.din.deD
2、DIN EN ISO 13503-1Erdl- und Erdgasindustrie Komplettierungsflssigkeiten und Materialien Teil 1: Messung der Flieeigenschaften vonKomplettierungsflssigkeiten (ISO 13503-1:2011);Englische Fassung EN ISO 13503-1:2011Petroleum and natural gas industries Completion fluids and materials Part 1: Measuremen
3、t of viscous properties of completion fluids (ISO 13503-1:2011);English version EN ISO 13503-1:2011Industries du ptrole et du gaz naturel Fluides de compltion et matriaux Partie 1: Mesurage des proprits visqueuses des fluides de compltion(ISO 13503-1:2011);Version anglaise EN ISO 13503-1:2011Alleinv
4、erkauf der Normen durch Beuth Verlag GmbH, 10772 BerlinErsatz frDIN EN ISO 13503-1:2005-09www.beuth.deGesamtumfang 29 SeitenDIN EN ISO 13503-1:2012-01 2 Nationales Vorwort Dieses Dokument (EN ISO 13503-1:2011) wurde vom ISO/TC 67 Materials, equipment and offshore structures for petroleum, petrochemi
5、cal and natural gas industries“, Subkomitee SC 3 Drilling and completion fluids, and well cements“ in Zusammenarbeit mit dem Technischen Komitee CEN/TC 12 Materialien, Ausrstungen und Offshore-Bauwerke fr die Erdl-, petrochemische und Erdgasindustrie“ (Sekretariat: AFNOR, Frankreich) erarbeitet. Fr
6、Deutschland hat hieran der Arbeitskreis NA 109-00-01-03 AK Bohrsplung und Zemente - Spiegel-ausschuss zu ISO/TC 67/SC 3“ im Normenausschuss Erdl- und Erdgasgewinnung (NG) des DIN Deutsches Institut fr Normung e. V. mitgearbeitet. Diese europische Norm enthlt unter Bercksichtigung des DIN-Prsidialbes
7、chlusses 1/2004 nur die englische Originalfassung der ISO Norm. Diese Norm enthlt neben den gesetzlichen Einheiten auch die Einheiten F“, ft“, inch“, pound“, lbf“, psi“ und r/min“, die im Deutschen Normenwerk nicht zugelassen sind. Es wird ausdrcklich darauf hingewiesen, dass die Anwendung dieser Ei
8、nheiten im nationalen amtlichen und geschftlichen Verkehr aufgrund des Gesetzes ber Einheiten im Messwesen nicht zulssig ist. Umrechnung: Nicht-SI-Einheit SI-Einheit Umrechnung F C C = (5/9) (F-32) ft m 1 ft = 0,304 8 m in (inch) mm 1 inch = 25,4 mm lb (pound) kg 1 lb = 0,453 592 37 kg lbf N 1 lbf =
9、 4,448 222 N psi (psig) kPa 1 psi = 6,894 757 kPa r/min min11 r/min = 1 min1nderungen Gegenber DIN EN ISO 13503-1:2005-09 wurden folgende nderungen vorgenommen: a) neuer Abschnitt Introduction“; b) Streichung des alten Abschnitts 3 Abbreviated terms“; c) Erweiterung der Begriffsdefinitionen z.B.: zu
10、 Rotor“; d) Aktualisierung von Bild 1 Shear-history simulation diagram“; e) Neuer Abschnitt 7.2.2.1 c Torsion spring“; f) Aktualisierung von Bild 2 Geometry of a non-pressurized concentric-cylinder viscometer“; DIN EN ISO 13503-1:2012-01 3 g) Erweiterung des Abschnitts 7.2.2.2 Pressurized concentric
11、-cylinder viscometer“; h) nderung der Werte fr Viscometer speed“ in Tabelle 1; i) Aktualisierung von Bild 3 Geometry of a pressurized concentric-cylinder viscometer“; j) Wegfall des alten Abschnitts 9.5 Bingham plastic parameters for completion fluids“; k) Aktualisierung des Literaturverzeichnis. Fr
12、here Ausgaben DIN EN ISO 13503-1: 2005-09 DIN EN ISO 13503-1:2012-01 4 Nationaler Anhang NA (informativ) Begriffe Folgende Begriffe werden in der Norm verwendet: 2 Begriffe Fr die Anwendung dieses Dokuments gelten die folgenden Begriffe. 2.1 innerer Zylinder (bob) innerer Zylinder eines Koaxial-Zyli
13、nder-Rotationsviskosimeters 2.2 Komplettierungsflssigkeit viskosifizierte Behandlungsflssigkeit, die whrend der Komplettierung oder Aufwltigung eines Erdl- oder Erdgas-Frderbohrloches verwendet wird 2.3 Koaxial-Zylinder-Rotationsviskosimeter Rotationsviskosimeter, bestehend aus zueinander konzentris
14、ch angeordnetem inneren und ueren Zylinder 2.4 Elastizitt Vermgen eines Stoffes, nach einer Krafteinwirkung in seine Ausgangsform und seinen Ausgangszustand zurckzukehren 2.5 laminare Strmung Flieeigenschaft von Flssigkeiten bei der sich alle Schichten der Flssigkeit parallel zueinander bewegen ohne
15、 sich zu vermischen 2.6 nicht vernetzte Flssigkeit lineare, polymerviskosifizierte Lsung oder jede andere Flssigkeit, die keine bedeutende, zum Weienberg-Effekt (bob climbing“) fhrende Elastizitt aufweist 2.7 Rheologie Lehre vom Deformations- und Flieverhalten der Stoffe 2.8 uerer Zylinder Lufer uer
16、er, sich drehender Zylinder eines Koaxial-Zylinder-Rotationsviskosimeters 2.9 Schergeschichte Folge von Schergeschwindigkeiten und Temperaturen, die vor und whrend Messungen auf Flssigkeiten angewendet wurden DIN EN ISO 13503-1:2012-01 5 2.10 Schergeschichtssimulator Gert zum Simulieren von Scherges
17、chichte in einer Flssigkeit 2.11 Schergeschwindigkeit Geschwindigkeit, mit der ein Teilchen einer Flssigkeit an einem anderen vorbei gleitet, geteilt durch den Abstand dieser Teilchen 2.12 Scherspannung zum Aufrechterhalten des Flieens einer Flssigkeit notwendige Kraft 2.13 viskoelastische Flssigkei
18、t vernetzte Polymerlsung oder andere Flssigkeit mit bedeutender zum Weienberg-Effekt (bob climbing“) fhrender Elastizitt 2.14 Viskositt Ma fr die innere Reibung einer Flssigkeit, deren Flieen durch uere Krafteinwirkung initiiert wurde DIN EN ISO 13503-1:2012-01 6 Leerseite EUROPEAN STANDARD NORME EU
19、ROPENNE EUROPISCHE NORM EN ISO 13503-1 November 2011 ICS 75.100 Supersedes EN ISO 13503-1:2005 English Version Petroleum and natural gas industries - Completion fluids and materials - Part 1: Measurement of viscous properties of completion fluids (ISO 13503-1:2011) Industries du ptrole et du gaz nat
20、urel - Fluides de compltion et matriaux - Partie 1: Mesurage des proprits visqueuses des fluides de compltion (ISO 13503-1:2011) Erdl- und Erdgasindustrie - Komplettierungsflssigkeiten und Materialien - Teil 1: Messung der Flieeigenschaften von Komplettierungsflssigkeiten (ISO 13503-1:2011) This Eur
21、opean Standard was approved by CEN on 31 October 2011. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
22、concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN membe
23、r into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
24、Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marn
25、ix 17, B-1000 Brussels 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 13503-1:2011: E EN ISO 13503-1:2011 (E) 2 Contents Page Foreword 3 Introduction .4 1 Scope 5 2 Terms and definitions .5 3 Measurement and precision .6
26、4 Fluid preparation6 5 Fluid preparation using shear-history simulation (optional) 6 5.1 General 6 5.2 Requirements for proper shear-history simulation 7 5.3 Conditions for sample delivery 8 5.4 Conditions for standard shear-history simulation .8 5.5 Operational considerations 8 6 Instrument calibra
27、tion .8 7 Measurement procedures .8 7.1 General 8 7.2 Non-crosslinked fluids (see 2.6) .8 7.2.1 General 8 7.2.2 Apparatus .9 7.3 Crosslinked polymer and surfactant fluids 14 7.3.1 General . 14 7.3.2 Apparatus 14 8 Calculation procedures 15 8.1 General concepts 15 8.2 Brief review of geometry-indepen
28、dent rheology versus nominal rheology . 16 8.3 Limitations/problems that can produce erroneous results 17 8.4 Calculation method for concentric-cylinder viscometers 17 8.4.1 General . 17 8.4.2 Calculation of shear stress from torque values 17 8.4.3 Nominal shear rate from angular velocity 18 8.4.4 C
29、onsistency index calculation 18 8.4.5 Fluid consistency index calculation . 19 8.5 Calculations for optional shear-history simulation . 19 8.5.1 Flow rate and tubing length requirement . 19 8.5.2 Minimum radius of curvature 20 9 Test report . 20 Bibliography . 23 DIN EN ISO 13503-1:2012-01 EN ISO 13
30、503-1:2011 (E) 3 Foreword This document (EN ISO 13503-1:2011) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offsho
31、re structures for petroleum, petrochemical and natural gas industries” the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2012, and conflicting national
32、 standards shall be withdrawn at the latest by May 2012. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN I
33、SO 13503-1:2005. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary,
34、 Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 13503-1:2011 has been approved by CEN as a EN ISO 13503-1:2011 without any modific
35、ation. DIN EN ISO 13503-1:2012-01 EN ISO 13503-1:2011 (E) 4 Introduction For the purposes of this part of ISO 13503, completion fluids are defined as viscosified treating fluids used during the completion or workover of a petroleum- or natural-gas-producing well. The objective of this part of ISO 13
36、503 is to provide a standard procedure for measuring the viscous properties of single-phase, non-particulate-laden completion fluids. These fluids are viscosified brines, gravel-pack carrier fluids, and fracturing fluids. These fluids can be either crosslinked or non-crosslinked (aqueous, hydrocarbo
37、n- or acid-based). An optional shear-history simulation procedure is provided for fluids that are potentially shear-sensitive. This procedure is designed to simulate the shearing effects experienced by a fluid in surface apparatus and during the time it is being conveyed down the wellbore. Shear-his
38、tory simulation is most often used during the development of new fracturing fluids to characterize their sensitivity to shear. These standard procedures were compiled on the basis of several years of comparative testing, debate, discussion, and continued research by the industry. This standard proce
39、dure is largely based on API RP 13M, first edition, July 2004. In this part of ISO 13503, where practical, US Customary units (USC) are included in parentheses for convenience. DIN EN ISO 13503-1:2012-01 EN ISO 13503-1:2011 (E) 5 1 Scope This part of ISO 13503 provides consistent methodology for det
40、ermining the viscosity of completion fluids used in the petroleum and natural gas industries. For certain cases, methods are also provided to determine the rheological properties of a fluid. 2 Terms and definitions For the purposes of this document, the following terms and definitions apply. 2.1 bob
41、 inner cylinder of a concentric-cylinder viscometer 2.2 completion fluid viscosified treating fluid used during the completion or workover of a petroleum- or natural-gas-producing well 2.3 concentric-cylinder viscometer rotational viscometer that consists of a concentric-cylindrical bob and a cylind
42、rical rotor 2.4 elasticity capability of a material to regain its original shape and condition upon removal of an acting stress 2.5 laminar flow flow property of fluids in which all layers of the fluid move parallel to each other and no material is transferred between layers 2.6 non-crosslinked flui
43、d linear, polymer-viscosified solution or any fluid that does not exhibit significant elasticity leading to the Weissenberg effect (bob climbing) 2.7 rheology science of the deformation and flow of matter 2.8 rotor outer rotating cylinder of a concentric-cylinder viscometer 2.9 shear history sequenc
44、e of shear rates and temperatures applied to fluids prior to and during measurements 2.10 shear-history simulator apparatus used to simulate shear history in a fluid 2.11 shear rate rate at which one particle of fluid is sliding by another particle divided by the distance between those particles 2.1
45、2 shear stress force required to sustain fluid flow DIN EN ISO 13503-1:2012-01 EN ISO 13503-1:2011 (E) 6 2.13 viscoelastic fluid crosslinked polymer solution or other fluid that exhibits significant elasticity, leading to the Weissenberg effect (bob climbing) 2.14 viscosity measure of the internal f
46、riction of a fluid when caused to flow by an external force 3 Measurement and precision Temperatures shall be measured to an accuracy of 1 C (2 F); pH shall be measured to an accuracy of 0,1 units. All other quantitative measurements shall be made to an accuracy of 2 %, unless specified otherwise. 4
47、 Fluid preparation Certain aspects of sample preparation and handling can affect the viscosity or rheological properties of a fluid. During all procedures, steps shall be taken to minimize entraining air into the fluid. The procedure used to prepare the fluid sample shall be documented, including th
48、e following information: a) description and/or composition of the base fluid; preparation of the fluid shall be described, starting with the fluid source, such as deionized water, tap water, completion brines, produced water, seawater or type of oil; b) identification of mixing apparatus, container
49、volume, and total volume of fluid prepared; c) identification of each fluid component and amount added; d) the order and method of addition of each component; e) mixing speeds, with time at each speed; f) ageing or holding time prior to measurements, if required; g) temperature; h) pH (for aqueous fluids); i) all other aspects of the fluid preparation which are known to affect the outcome of the viscosity measurement, such as filtrati
