1、 DEUTSCHE NORMMrz 2010DIN EN ISO 13503-2 ICS 75.180.99 Ersatz fr DIN EN ISO 13503-2:2007-02 Erdl- und Erdgasindustrie Komplettierungsflssigkeiten und -materialien Teil 2: Messung der Eigenschaften von Sttzmaterialien zum Einsatz bei hydraulischen Fraktionierungs- und in Kiespackungsvorgngen (ISO 135
2、03-2:2006 + Amd 1:2009); Englische Fassung EN ISO 13503-2:2006 + A1:2009 Petroleum and natural gas industries Completion fluids and materials Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations (ISO 13503-2:2006 + Amd 1:2009); English version EN
3、ISO 13503-2:2006 + A1:2009 Industries du ptrole et du gaz naturel Fluides de compltion et matriaux Partie 2: Mesurage des proprits des matriaux de soutnement utiliss dans les oprations de fracturation hydraulique et de remplissage de gravier (ISO 13503-2:2006 + Amd 1:2009); Version anglaise EN ISO 1
4、3503-2:2006 + A1:2009 Gesamtumfang 42 SeitenNormenausschuss Erdl- und Erdgasgewinnung (NG) im DIN DIN Deutsches Institut fr Normung e.V. .Jede Art der Vervielfltigung, auch auszugsweise, nur mit Genehmigung des DIN Deutsches Institut fr Normung e.V. , Berlin gestattet. Alleinverkauf der Normen durch
5、 Beuth Verlag GmbH, 10772 Berlin Preisgruppe 17 www.din.de www.beuth.de !$?“1562857B55EB1B3E14C22109E918E8EA43EDB30F09DCEB7EF8AD9NormCD - Stand 2010-04 DIN EN ISO 13503-2:2010-03 Nationales Vorwort Dieses Dokument (EN ISO 13503-2:2006 + A1:2009) wurde vom Technischen Komitee ISO/TC 67 Materials, equ
6、ipment and offshore structures for petroleum, petrochemical and natural gas industries“ in Zusammenarbeit mit dem Technischen Komitee CEN/TC 12 Materialien, Ausrstungen und Offshore-Bauwerke fr die Erdl-, petrochemische und Erdgasindustrie“ erarbeitet, dessen Sekretariat von AFNOR (Frankreich) gehal
7、ten wird. Fr Deutschland hat hieran der Arbeitskreis NA 109-00-01 AK 3 Bohrsplung und Zemente“ im Normenausschuss Erdl- und Erdgasgewinnung (NG) mitgearbeitet. Dieses Dokument enthlt die nderung 1, angenommen von CEN am 2009-10-07. Der Beginn und das Ende von neuem oder gendertem Text werden durch d
8、ie Markierungen angezeigt. Dieses Dokument enthlt unter Bercksichtigung des DIN-Prsidialbeschlusses 1/2004 nur die englische Originalfassung der ISO Norm. Dieses Dokument enthlt neben den gesetzlichen Einheiten auch die Einheiten F“, ft“, gal“, inch“, lb/gal“, psi“, die im Deutschen Normenwerk nicht
9、 zugelassen sind. Es wird ausdrcklich darauf hingewiesen, dass die Anwendung dieser Einheiten im nationalen amtlichen und geschftlichen Verkehr aufgrund des Gesetzes ber Einheiten im Messwesen nicht zulssig ist. Umrechnung: Nicht-SI-Einheit SI-Einheit Umrechnung F C (5/9) (F-32) ft M 1 ft = 0,304 8
10、m gal (galone) l 1 gal = 3,785 l in (inch) mm 1 inch = 25,4 mm lb/gal kg/m31 lb/gal = 0,118 kg/dm3psi (psig) kPa 1 psi = 6,894 757 kPa nderungen Gegenber DIN EN ISO 13503-2:2007-02 wurden folgende nderungen vorgenommen: a) Abschnitt 1 Anwendungsbereich“ letzter Satz ersetzt; b) Abschnitt 2 Normative
11、 Verweisungen“ Datum fr ASTM E11 ergnzt; c) neuer Anhang B hinzugefgt. Frhere Ausgaben DIN EN ISO 13503-2: 2007-02 2 !“ B55EB1B3E14C22109E918E8EA43EDB30F09DCEB7EF8AD9NormCD - Stand 2010-04 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 13503-2 November 2006 +A1 November 2009 ICS 75.100 Eng
12、lish Version Petroleum and natural gas industries Completion fluids and materials Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations (ISO 13503-2:2006 + Amd 1:2009) Industries du ptrole et du gaz naturel Fluides de compltion et matriaux Partie 2
13、 Mesurage des proprits des matriaux de soutnement utiliss dans les oprations de fracturation hydraulique et de remplissage de gravier (ISO 13503-2:2006 + Amd 1:2009) Erdl- und Erdgasindustrie Komplettierungsflssigkeiten und -materialien Teil 2: Messung der Eigenschaften von Sttzmaterialien zum Eins
14、atz bei hydraulischen Fraktionierungs- und in Kiespackungsvorgngen (ISO 13503-2:2006 + Amd 1:2009) This European Standard was approved by CEN on 22 September 2006, includes amendment A1 approved by CEN on 7 October 2009. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which
15、 stipulate the conditions for inclusion of this amendment into the relevant national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. This amendment ex
16、ists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are the national standards
17、 bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom
18、 EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2009 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 13503-2:2006 + A1:
19、2009: EB55EB1B3E14C22109E918E8EA43EDB30F09DCEB7EF8AD9NormCD - Stand 2010-04 EN ISO 13503-2:2006 + A1:2009 (E) Contents Page Foreword4 !Foreword 5 Introduction .6 1 Scope 7 2 Normative references 7 3 Abbreviations.7 4 Standard proppant sampling procedure .7 4.1 General7 4.2 Particle segregation 8 4.3
20、 Equipment 8 4.4 Number of required samples Bulk.11 4.4.1 Proppants for hydraulic fracturing 11 4.4.2 Gravel-packing media .11 4.5 Sampling Bulk material .12 4.6 Sampling Bagged material .12 4.6.1 Bags up to 50 kg (110 lb) 12 4.6.2 Totes/bulk bags/super sacks weighing up to 2 000 kg (4 400 lb) .12 5
21、 Sample handling and storage.12 5.1 Sample reduction.12 5.2 Sample splitting .12 5.3 Sample and record retention and storage 12 6 Sieve analysis 13 6.1 Purpose.13 6.2 Description .13 6.3 Equipment and materials 13 6.4 Procedure .13 6.5 Calculation of the mean diameter, median diameter and standard d
22、eviation.14 6.5.1 General14 6.5.2 Mean diameter14 6.5.3 Median diameter.15 6.6 Sieve calibration 16 6.6.1 Purpose.16 6.6.2 Description .16 6.6.3 Procedure .17 6.6.4 Preparing calibration samples .18 7 Proppant sphericity and roundness 18 7.1 Purpose.18 7.2 Description .19 7.3 Apparatus capability .1
23、9 7.4 Procedure .19 7.5 Alternate method for determining average sphericity and roundness20 7.5.1 Use of photomicrographs .20 7.5.2 Procedure .20 7.5.3 Suggested magnification for photomicrographs .202 DIN EN ISO 13503-2:2010-03 B55EB1B3E14C22109E918E8EA43EDB30F09DCEB7EF8AD9NormCD - Stand 2010-04 EN
24、 ISO 13503-2:2006 + A1:2009 (E) Page 8 Acid solubility 20 8.1 Purpose 20 8.2 Description.21 8.3 Equipment and materials21 8.4 Procedure.21 8.4.1 General .21 8.4.2 Preparation of 12:3 HCI:HF solution22 8.4.3 Solubility test .22 9 Turbidity test23 9.1 Purpose 23 9.2 Description.23 9.3 Equipment and ma
25、terials23 9.4 Equipment calibration.23 9.5 Procedure.23 10 Procedures for determining proppant bulk density, apparent density and absolute density 24 10.1 Purpose 24 10.2 Description.24 10.3 Bulk density .24 10.3.1 Equipment and materials24 10.3.2 Calibration of cylinder.26 10.3.3 Procedure.26 10.4
26、Apparent density .27 10.4.1 Equipment and materials27 10.4.2 Procedure.27 10.5 Absolute density28 10.5.1 Description.28 10.5.2 Equipment 28 10.5.3 Procedures.29 11 Proppant crush-resistance test .29 11.1 Purpose 29 11.2 Description.29 11.3 Equipment and materials29 11.4 Sample preparation .30 11.5 C
27、rush-resistance procedure 31 12 Loss on ignition of resin-coated proppant .32 12.1 Objective.32 12.2 Apparatus and materials.33 12.3 Loss-on-ignition procedure for whole-grain proppant33 Annex A (informative) Formazin solution preparation35 A.1 Preparation of a formazin polymer solution for calibrat
28、ion35 A.2 Equipment Calibration 35 Annex B (informative) Proppant specifications.36 B.1 Fracturing proppant sizes 36 B.2 Gravel packing sizes.37 B.3 Sphericity and roundness 37 B.4 Acid solubility 38 B.5 Maximum proppant turbidity38 B.6 Maximum crush material 38 B.6.1 General .38 B.6.2 Gravel packin
29、g proppants 38 B.6.3 Fracturing proppants 39 Bibliography40 3 DIN EN ISO 13503-2:2010-03 B55EB1B3E14C22109E918E8EA43EDB30F09DCEB7EF8AD9NormCD - Stand 2010-04 EN ISO 13503-2:2006 + A1:2009 (E) Foreword This document (EN ISO 13503-2:2006) has been prepared by Technical Committee ISO/TC 67 Materials, e
30、quipment and offshore structures for petroleum and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries“, the secretariat of which is held by AFNOR. This European Standard shal
31、l be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2007, and conflicting national standards shall be withdrawn at the latest by May 2007. According to the CEN/CENELEC Internal Regulations, the national standards organizati
32、ons of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia
33、 Slovenia, Spain, Sweden, Switzerland and United Kingdom. Endorsement notice The text of ISO 13503-2:2006 has been approved by CEN as EN ISO 13503-2:2006 without any modifications. 4 DIN EN ISO 13503-2:2010-03 B55EB1B3E14C22109E918E8EA43EDB30F09DCEB7EF8AD9NormCD - Stand 2010-04 EN ISO 13503-2:2006
34、 A1:2009 (E) !Foreword This document (EN ISO 13503-2:2006/A1:2009) has been prepared by Technical Committee ISO/TC 67 Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 Materials, equipment and of
35、fshore structures for petroleum, petrochemical and natural gas industries” the secretariat of which is held by AFNOR. This Amendment to the European Standard EN ISO 13503:2006 shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the lates
36、t by May 2010, and conflicting national standards shall be withdrawn at the latest by May 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such paten
37、t rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Irelan
38、d, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 13503-2:2006/Amd 1:2009 has been approved by CEN as a EN ISO 13503-2:2006/A1:2009 without any modi
39、fication.“ 5 DIN EN ISO 13503-2:2010-03 B55EB1B3E14C22109E918E8EA43EDB30F09DCEB7EF8AD9NormCD - Stand 2010-04 EN ISO 13503-2:2006 + A1:2009 (E) 6 Introduction This part of ISO 13503 is a compilation and modification of API RP 56 1, API RP 58 2and API RP 60 3. The procedures have been developed to imp
40、rove the quality of proppants delivered to the well site. They are for use in evaluating certain physical properties used in hydraulic fracturing and gravel-packing operations. These tests should enable users to compare the physical characteristics of various proppants tested under the described con
41、ditions and to select materials useful for hydraulic fracturing and gravel-packing operations. The procedures presented in this part of ISO 13503 are not intended to inhibit the development of new technology, material improvements or improved operational procedures. Qualified engineering analysis an
42、d judgment are required for their application to a specific situation. In this part of ISO 13503, where practical, US Customary (USC) units are included in brackets for information. Annex A of this part of ISO 13503 is for information only. DIN EN ISO 13503-2:2010-03 B55EB1B3E14C22109E918E8EA43EDB30
43、F09DCEB7EF8AD9NormCD - Stand 2010-04 EN ISO 13503-2:2006 + A1:2009 (E) 1 Scope This part of ISO 13503 provides standard testing procedures for evaluating proppants used in hydraulic fracturing and gravel-packing operations. NOTE “Proppants” mentioned henceforth in this part of ISO 13503 refer to san
44、d, ceramic media, resin-coated proppants, gravel-packing media and other materials used for hydraulic fracturing and gravel-packing operations. The objective of this part of ISO 13503 is to provide a consistent methodology for testing performed on hydraulic fracturing and/or gravel-packing proppants
45、 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ASTM E11, Standard Specification for Wire Cloth and Sieves for Testing Purposes 3 Abbreviations API American Petrole
