1、January 2008DEUTSCHE NORM English price group 10No part of this standard may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 83.140.10!$K_Q“1406046
2、www.din.deDDIN EN ISO 15013Plastics Extruded sheets of polypropylene (PP) Requirements and test methods (ISO 15013:2007)English version of DIN EN ISO 15013:2008-01Kunststoffe Extrudierte Tafeln aus Polypropylen (PP) Anforderungen und Prfung (ISO 15013:2007)Englische Fassung DIN EN ISO 15013:2008-01S
3、upersedesDIN EN ISO 15013:1999-05www.beuth.deDocument comprises 17 pagesDIN EN ISO 15013:2008-01 2 National foreword This standard has been prepared by Technical Committee ISO/TC 61 “Plastics” in collaboration with Technical Committee CEN/TC 249 “Plastics” (Secretariat: NBN, Belgium). The responsibl
4、e German body involved in its preparation was the Normenausschuss Kunststoffe (Plastics Standards Committee), Technical Committee NA 054-04-02 AA Halbzeuge aus Thermoplasten. The DIN Standards corresponding to the International Standards referred to in clause 2 of the EN are as follows: ISO 179-1 DI
5、N EN ISO 179-1 ISO 179-2 DIN EN ISO 179-2 ISO 291 DIN EN ISO 291 ISO 527-2 DIN EN ISO 527-2 ISO 1133 DIN EN ISO 1133 ISO 1873-1 DIN EN ISO 1873-1 ISO 2818 DIN EN ISO 2818 ISO 4577 DIN EN ISO 4577 ISO 11501 DIN EN ISO 11501 Amendments This standard differs from DIN EN ISO 15013:1999-05 as follows: a)
6、 In Table 2, the requirements regarding the melt mass-flow rate (MFR 230 C/2,16 kg) have been amended. b) Normative references have been updated. c) The standard has been editorially revised. Previous editions DIN 16971: 1982-01 DIN EN ISO 15013: 1999-05 National Annex NA (informative) Bibliography
7、DIN EN ISO 179-1, Plastics Determination of Charpy impact properties Part 1: Non-instrumented impact test DIN EN ISO 179-2, Plastics Determination of Charpy impact properties Part 2: Instrumented impact test DIN EN ISO 291, Plastics Standard atmospheres for conditioning and testing DIN EN ISO 15013:
8、2008-01 3 DIN EN ISO 527-1, Plastics Determination of tensile properties Part 1: General principles DIN EN ISO 527-2, Plastics Determination of tensile properties Part 2: Test conditions for moulding and extrusion plastics DIN EN ISO 1133, Plastics Determination of the melt mass-flow rate (MFR) and
9、the melt volume-flow rate (MVR) of thermoplastics DIN EN ISO 1873-1, Plastics Polypropylene (PP) moulding and extrusion materials Part 1: Designation system and basis for specifications DIN EN ISO 2818, Plastics Preparation of test specimens by machining DIN EN ISO 4577, Plastics Polypropylene and p
10、ropylene-copolymers Determination of thermal oxidative stability in air, oven method DIN EN ISO 11501, Plastics Film and sheeting Determination of dimensional change on heating DIN EN ISO 15013:2008-01 4 This page is intentionally blank EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN ISO 15013Octo
11、ber 2007ICS 83.140.10 Supersedes EN ISO 15013:1998 English VersionPlastics - Extruded sheets of polypropylene (PP) - Requirementsand test methods (ISO 15013:2007)Plastiques - Plaques extrudes en polypropylne (PP) -Exigences et mthodes dessai (ISO 15013:2007)Kunststoffe - Extrudierte Tafeln aus Polyp
12、ropylen (PP) -Anforderungen und Prfung (ISO 15013:2007)This European Standard was approved by CEN on 13 September 2007.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without a
13、ny alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made b
14、y translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Ger
15、many, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGMan
16、agement Centre: rue de Stassart, 36 B-1050 Brussels 2007 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN ISO 15013:2007: EContents Page 2 EN ISO 15013:2007 (E) Foreword 3 1 Scope . 4 2 Normative references . 4 3 Material 4 4 Requirem
17、ents 5 4.1 Appearance . 5 4.2 Dimensional tolerances . 5 4.3 Properties 6 5 Test methods 7 5.1 Test specimens . 7 5.2 Delivery condition 8 5.3 Appearance . 8 5.4 Dimensions . 8 5.5 Tensile stress at yield, y, and tensile strain at yield, y8 5.6 Modulus of elasticity in tension, Et. 8 5.7 Charpy impa
18、ct strength of notched specimens, acn. 9 5.8 Melt mass-flow rate (MFR) . 9 5.9 Heat resistance . 9 5.10 Determination of shrinkage an heating 9 6 Designation . 10 6.1 Example for sheets 10 6.2 Example for sheets in rolled form 11 7 Marking 11 Annex A (normative) Requirements for rectangularity 12 DI
19、N EN ISO 15013:2008-01 Foreword 3 EN ISO 15013:2007 (E) This document (EN ISO 15013:2007) has been prepared by Technical Committee ISO/TC 61 “Plastics“ in collaboration with Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by NBN. This European Standard shall be given the s
20、tatus of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2008, and conflicting national standards shall be withdrawn at the latest by April 2008. This document supersedes EN ISO 15013:1998. According to the CEN/CENELEC Internal Regulations, t
21、he national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, N
22、orway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 15013:2007 has been approved by CEN as a EN ISO 15013:2007 without any modification. DIN EN ISO 15013:2008-01 1 Scope This International Standard specifies the
23、requirements and test methods for solid flat extruded sheets of polypropylene homopolymers (PP-H) and polypropylene copolymers (PP-B and PP-R) without fillers or reinforcing materials. This International Standard also applies to PP sheet in rolled form. It applies only to thicknesses of 0,5 mm to 40
24、 mm. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 179-1, Plastics D
25、etermination of Charpy impact properties Part 1: Non-instrumented impact test ISO 179-2, Plastics Determination of Charpy impact properties Part 1: Instrumented impact test ISO 291, Plastics Standard atmospheres for conditioning and testing ISO 527-2, Plastics Determination of tensile properties Par
26、t 2: Test conditions for moulding and extrusion plastics ISO 1133, Plastics Determination of the melt mass-flow rate (MFR) and the melt volume-flow rate (MVR) of thermoplastics ISO 1873-1, Plastics Polypropylene (PP) moulding and extrusion materials Part 1: Designation system and basis for specifica
27、tions ISO 2818, Plastics Preparation of test specimens by machining ISO 4577, Plastics Polypropylene and propylene-copolymers Determination of thermal oxidative stability in air Oven method ISO 11501, Plastics Film and sheeting Determination of dimensional change on heating 3 Material Sheets shall c
28、onsist of PP extrusion compounds as defined in ISO 1873-1, without fillers or reinforcing materials. The extrusion compounds can contain additives such as processing aids, stabilizers, flame retardants, impact modifiers and colorants. Compounds and additives of unknown identity shall not be used. NO
29、TE Legal conditions may necessitate a specific choice of extrusion material (see 4.3.3). 4 EN ISO 15013:2007 (E)DIN EN ISO 15013:2008-01 4 Requirements 4.1 Appearance Sheets shall be substantially free from bubbles, voids, cracks, visible impurities and other defects which would make them unfit for
30、the intended use. Surfaces shall be substantially smooth and free from sharp grooves, sink marks or damage. Colorants shall be homogeneously distributed throughout the material. Slight colour variations due to variations in the extrusion compound or processing conditions are admissible. The exact ex
31、tent of variations in any of the above shall be agreed between the interested parties. Sheets shall be examined in accordance with 5.3. 4.2 Dimensional tolerances 4.2.1 Thickness For any individual sheet, the thickness tolerance with reference to the nominal thickness shall be as given by h u (0,08
32、mm + 0,03 hn) (1) where h is the tolerance on the thickness, in millimetres; hnis the nominal thickness, in millimetres. Testing shall be in accordance with 5.4.1. 4.2.2 Length and width The nominal length, ln, and nominal width, bn, of sheets shall be as agreed between the interested parties. Unles
33、s agreed differently, the length shall be in the direction of extrusion. For any individual sheet selected at random from any delivery, the tolerances on length and width shall be in accordance with Table 1. Testing shall be in accordance with 5.4.2. Table 1 Tolerances on length and width of sheet V
34、alues in millimetres Tolerances Nominal dimension DnLength Width Dnu 500 21+21+500 10 Maximum shrinkage in the direction of extrusion (%) 60 50 42 34 28 25 22 Not applicable 4.3.3 Physiological behaviour Relevant legislation concerning physiological behaviour shall be taken into consideration. 5 Tes
35、t methods 5.1 Test specimens 5.1.1 Preparation of test specimens Representative test specimens shall be cut longitudinally and transversely from locations evenly distributed over the length and width of the sheet. With sheets in roll form, a 2 m sample shall be cut from the end of the roll to prepar
36、e test specimens. The surfaces of the test specimens shall be free from damage and faults in order to avoid notch effects. Should any burrs be formed on the test specimens during preparation, these shall be eliminated without damaging the surfaces of the specimens. If required, the cut edges shall b
37、e finished with abrasive paper (grain size 220 or finer), the direction of abrasion being along the length of the test specimens. If it is necessary to machine the sheet to reduce it to the thickness required, one original surface shall be left intact. In particular, test specimens over 4,2 mm thick
38、 intended to be used in the tests described in 5.5 to 5.7 shall be machined down on one side to a thickness of 4,0 mm 0,2 mm in accordance with ISO 2818. 5.1.2 Conditioning All test specimens shall be conditioned for at least 16 h at standard temperature 23 as defined in ISO 291. Shorter conditionin
39、g times may be used by agreement between the interested parties when it can be shown that there is no significant difference in the results obtained. 5.1.3 Testing Testing shall be carried out at standard temperature 23 as defined in ISO 291, unless otherwise agreed between the interested parties or
40、 specified in the individual test standards. 7 EN ISO 15013:2007 (E) DIN EN ISO 15013:2008-01 5.2 Delivery condition Sheets shall be visually examined when delivered to ensure freedom from mechanical damage or other obvious defects. Sheets can be inspected by ultrasonic or X-ray methods where requir
41、ed. 5.3 Appearance Where possible, sheets shall be examined for visual defects by transmitted light using a suitable light source. Otherwise, sufficiently bright reflected light shall be used. Any defects thus identified shall be compared with the agreed specification (which may be either a written
42、specification or in the form of reference samples) and classified accordingly. 5.4 Dimensions 5.4.1 Thickness, h The thickness, h, shall be measured using suitable calibrated equipment meeting the specifications of Table 4. Table 4 Error limits of equipment Values in millimetres Nominal thickness, h
43、nError limit 0,50 u hn550 to 900) 1 000 4 ( 900 to 1 500) 1 000 5 ( 1 500 to 4 000) 1 000 6 u 550 1 220 3 ( 550 to 800) 1 220 4 ( 800 to 1 100) 1 220 5 ( 1 100 to 1 750) 1 220 6 ( 1 750 to 4 000) 1 220 7 u 550 1 500 3 ( 550 to 750) 1 500 4 ( 750 to 1 000) 1 500 5 ( 1 000 to 1 350) 1 500 6 ( 1 350 to
44、 1 850) 1 500 7 ( 1 850 to 3 000) 1 500 8 ( 3 000 to 4 000) 1 500 9 u 500 2 000 3 ( 500 to 700) 2 000 4 ( 700 to 900) 2 000 5 ( 900 to 1 150) 2 000 6 ( 1 150 to 1 450) 2 000 7 ( 1 450 to 1 800) 2 000 8 ( 1 800 to 2 300) 2 000 9 ( 2 300 to 3 000) 2 000 10 ( 3 000 to 4 000) 2 000 11 12 EN ISO 15013:20
45、07 (E)DIN EN ISO 15013:2008-01 Table A.1 (continued) Nominal sheet dimensions (length width) Maximum limit of deviation from rectangularity d1 d2 u 500 3 000 3 ( 500 to 700) 3 000 4 ( 700 to 850) 3 000 5 ( 850 to 1 050) 3 000 6 ( 1 050 to 1 250) 3 000 7 ( 1 250 to 1 500) 3 000 8 ( 1 500 to 1 700) 3 000 9 ( 1 700 to 2 000) 3 000 10 ( 2 000 to 2 300) 3 000 11 ( 2 300 to 2 700) 3 000 12 ( 2 700 to 3 100) 3 000 13 ( 3 100 to 3 700) 3 000 14 ( 3 700 to 4 000) 3 000 15 13 EN ISO 15013:2007 (E) DIN EN ISO 15013:2008-01
