DIN EN ISO 15181-5-2008 Paints and varnishes - Determination of release rate of biocides from antifouling paints - Part 5 Calculation of the tolylfluanid and dichlofluanid release .pdf
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1、September 2008DEUTSCHE NORM English price group 12No part of this standard may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 87.040!$QtY“1468154w
2、ww.din.deDDIN EN ISO 15181-5Paints and varnishes Determination of release rate of biocides from antifouling paints Part 5: Calculation of the tolylfluanid and dichlofluanid release rate bydetermination of the concentration of dimethyltolylsulfamide (DMST)and dimethylphenylsulfamide (DMSA) in the ext
3、ract (ISO 15181-5:2008)English version of DIN EN ISO 15181-5:2008-09Beschichtungsstoffe Bestimmung der Auswaschrate von Bioziden aus Antifouling-Beschichtungen Teil 5: Berechung der Auswaschrate von Tolylfluanid und Dichlofluanid durch Bestimmungder Konzentration von Dimethyltolylsulfamid (DMST) und
4、 Dimethylphenylsulfamid (DMSA)im Extrakt (ISO 15181-5:2008)Englische Fassung DIN EN ISO 15181-5:2008-09www.beuth.deDocument comprises 23 pagesDIN EN ISO 15181-5:2008-09 2 National foreword This standard falls in the domain of Technical Committee CEN/TC 139 “Paints and varnishes” (Secretariat: DIN, G
5、ermany). It is identical with International Standard ISO 15181-5 which was prepared by ISO/TC 35/SC 9 “General test methods for paints and varnishes” (Secretariat: BSI, United Kingdom). The responsible German body involved in its preparation was the Normenausschuss Beschichtungsstoffe und Beschichtu
6、ngen (Coatings and Coating Materials Standards Committee), Technical Committee NA 002-00-07 AA Allgemeine Prfverfahren fr Beschichtungsstoffe und Beschichtungen. DIN EN ISO 15181 consists of the following parts, under the general title Paints and varnishes Determination of release rate of biocides f
7、rom antifouling paints: Part 1: General method for extraction of biocides Part 2: Determination of copper-ion concentration in the extract and calculation of the release rate Part 3: Calculation of the zinc ethylene-bis(dithiocarbamate) (zineb) release rate by determination of the concentration of e
8、thylenethiourea in the extract Part 4: Determination of pyridine-triphenylborane (PTPB) concentration in the extract and calculation of the release Part 5: Calculation of the tolylfluanid and dichlofluanid release rate by determination of the concentration of dimethyltolylsulfamide (DMST) and dimeth
9、ylphenylsulfamide (DMSA) in the extract The following part is under preparation: Part 6: Determination of tralopyril release rate by quantification of its degradation product 3-bromo-5-(4-chlorophenyl)-4-cyano-1H-pyrrole-2-carboxylic acid (BCCPCA) in the extract The DIN Standards corresponding to th
10、e International Standards referred to in the EN are as follows: ISO 3696 DIN ISO 3696 ISO 15181-1 DIN EN ISO 15181-1 National Annex NA (informative) Bibliography DIN ISO 3696, Water for analytical laboratory use Specification and test methods DIN EN ISO 15181-1, Paints and varnishes Determination of
11、 release rate of biocides from antifouling paints Part 1: General method for extraction of biocides EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN ISO 15181-5May 2008ICS 87.040English VersionPaints and varnishes - Determination of release rate of biocidesfrom antifouling paints - Part 5: Calculat
12、ion of the tolylfluanid anddichlofluanid release rate by determination of the concentrationof dimethyltolylsulfamide (DMST) and dimethylphenylsulfamide(DMSA) in the extract (ISO 15181-5:2008)Peintures et vernis - Dtermination du taux de lixiviationdes biocides contenus dans les peintures antisalissu
13、res -Partie 5: Calcul du taux de lixiviation du tolylfluanide et dudichlofluanide par dtermination de la concentration dudimthyl-tolylsulfamide (DMST) et du dimthyl-phnylsulfamide (DMSA) dans lextrait (ISO 15181-5:2008)Beschichtungsstoffe - Bestimmung der Auswaschrate vonBioziden aus Antifouling-Bes
14、chichtungen - Teil 5:Berechung der Auswaschrate von Tolylfluanid undDichlofluanid durch Bestimmung der Konzentration vonDimethyltolylsulfamid (DMST) und Dimethylphenylsulfamid(DMSA) im Extract (ISO 15181-5:2008)This European Standard was approved by CEN on 8 May 2008.CEN members are bound to comply
15、with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management C
16、entre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficia
17、l versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia
18、, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2008 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national
19、 Members.Ref. No. EN ISO 15181-5:2008: E2 DIN EN ISO 15181-5:2008-09EN ISO 15181-5:2008 (E)Contents Page Foreword3 Introduction .4 1 Scope 5 2 Normative references 5 3 Principle6 4 Supplementary information 6 5 Apparatus .6 6 Reagents and materials 7 7 Test samples 7 8 Preparation of calibration sta
20、ndards.8 9 Recovery and conversion check standards .9 10 Procedure 10 11 Calculation and expression of results 11 12 Validation of the method 15 13 Test report . 15 Annex A (normative) Supplementary information 17 Annex B (informative) Additional information on tolylfluanid, DMST, dichlofluanid and
21、DMSA. 18 Bibliography. 21 Foreword 3 EN ISO 15181-5:2008 (E)DIN EN ISO 15181-5:2008-09This document (EN ISO 15181-5:2008) has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes“ in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” the secretariat of which is
22、held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by November 2008, and conflicting national standards shall be withdrawn at the latest by November 2008. Attention is drawn to the possibil
23、ity that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are b
24、ound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden,
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