1、August 2011 Translation by DIN-Sprachendienst.English price group 16No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS
2、 13.060.45!$tB,“1813109www.din.deDDIN EN ISO 5667-13Water quality Sampling Part 13: Guidance on sampling of sludges (ISO 5667-13:2011)English translation of DIN EN ISO 5667-13:2011-08Wasserbeschaffenheit Probenahme Teil 13: Anleitung zur Probenahme von Schlmmen (ISO 5667-13:2011)Englische bersetzung
3、 von DIN EN ISO 5667-13:2011-08Qualit de leau chantillonnage Partie 13: Lignes directrices pour lchantillonnage de boues (ISO 5667-13:2011)Traduction anglaise de DIN EN ISO 5667-13:2011-08SupersedesDIN EN ISO 5667-13:1998-02www.beuth.deDocument comprises pagesIn case of doubt, the German-language or
4、iginal shall be considered authoritative.3408.11 DIN EN ISO 5667-13:2011-08 2 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee ISO/TC 147 “Water quality” in collaboration with Technical Committee CEN/TC 308 “Characterization of sludges”
5、(Secretariat: AFNOR, France). The responsible German body involved in its preparation was the Normenausschuss Wasserwesen (Water Practice Standards Committee), Working Committee NA 119-01-03-04 UA Schlamm und Sedimente of NA 119-01-03 AA Wasseruntersuchung. ISO 5667 consists of the following parts,
6、under the general title Water quality Sampling: Part 1: Guidance on the design of sampling programmes and sampling techniques Part 3: Guidance on the preservation and handling of water samples Part 4: Guidance on sampling from lakes, natural and man-made Part 5: Guidance on sampling of drinking wate
7、r from treatment works and piped distribution systems Part 6: Guidance on sampling of rivers and streams Part 7: Guidance on sampling of water and steam in boiler plants Part 8: Guidance on the sampling of wet deposition Part 9: Guidance on sampling from marine waters Part 10: Guidance on sampling o
8、f waste waters Part 11: Guidance on sampling of groundwaters Part 12: Guidance on sampling of bottom sediments Part 13: Guidance on sampling of sludges Part 14: Guidance on quality assurance of environmental water sampling and handling Part 15: Guidance on the preservation and handling of sludge and
9、 sediment samples Part 16: Guidance on biotesting of samples Part 17: Guidance on sampling of bulk suspended solids Part 19: Guidance on sampling of marine sediments Part 20: Guidance on the use of sampling data for decision making Compliance with thresholds and classification systems Part 21: Guida
10、nce on sampling of drinking water distributed by tankers or means other than distribution pipes Part 22: Guidance on the design and installation of groundwater monitoring points Part 23: Guidance on passive sampling in surface waters DIN EN ISO 5667-13:2011-08 3 Designation of method S 1 “Guidance o
11、n sampling of sludges”: Method DIN EN ISO 5667-13 S 1 This standard has been published to implement the Water Framework Directive (WFD), Directive 2000/60/EC of the European Parliament and of the Council of 23 October 2000 establishing a framework for Community action in the field of water policy1).
12、 The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 3534-2 E DIN ISO 3534-2 ISO 5667-1 DIN EN ISO 5667-1 ISO 5667-10 DIN 38402-11 ISO 5667-12 DIN 38414-11 ISO 5667-15 DIN EN ISO 5667-15 ISO 5667-16 DIN EN ISO 5667-16 ISO 10381-4 DIN ISO 10
13、381-4 ISO 10381-6 DIN ISO 10381-6 Expert assistance and specialized laboratories will be required to perform the analysis described in this standard. Existing safety regulations are to be taken into account. Depending on the objective of the analysis, a check shall be made on a case-by-case basis as
14、 to whether and to what extent additional conditions will have to be specified. German standard methods for the examination of water, waste water and sludge Standard methods published as DIN Standards are obtainable from Beuth Verlag GmbH, either individually or grouped in volumes. The standard meth
15、ods included in the loose-leaf publication entitled Deutsche Einheits-verfahren zur Wasser-, Abwasser- und Schlammuntersuchung will continue to be published jointly by Wiley-VCH Verlag and Beuth Verlag GmbH. All standard methods relevant to the Abwasserverordnung (Waste Water Regulation) (AbwV1) inc
16、luded in the new Regulation on 57, paragraph 1, number 1, of the Gesetz zur Ordnung des Wasserhaushaltes (German Water Management Act1) concerning Anforderungen an das Einleiten von Abwasser in Gewsser together with the Abwasserverordnung and the Gesetz zur Ordnung des Wasserhaushalts have been publ
17、ished by Beuth Verlag GmbH as a loose-leaf collection Analysenverfahren in der Abwasserverord-nung Rechtsvorschriften und Normen (Supplements). Standards or draft standards bearing the group title “German standard methods for the examination of water, waste water and sludge” are classified under the
18、 following categories (main titles): General information (group A) (DIN 38402) Sensory analysis (group B) (DIN 38403) Physical and physicochemical parameters (group C) (DIN 38404) Anions (group D) (DIN 38405) Cations (group E) (DIN 38406) Substance group analysis (group F) (DIN 38407) Gaseous consti
19、tuents (group G) (DIN 38408) Parameters characterizing effects and substances (group H) (DIN 38409) Biological-ecological methods of analysis (group M) (DIN 38410) Microbiological methods (group K) (DIN 38411) 1) Registered in the DITR database of DIN Software GmbH, obtainable from: Beuth Verlag Gmb
20、H, 10772 Berlin DIN EN ISO 5667-13:2011-08 4 Test methods using water organisms (group L) (DIN 38412) Individual constituents (group P) (DIN 38413) Sludge and sediments (group S) (DIN 38414) Bio-assays with microorganisms (group T) (DIN 38415) In addition to the methods described in the DIN 38402 to
21、 DIN 38415 series of standards, there are a number of European and International Standards available as DIN EN, DIN EN ISO and DIN ISO Standards, which also form part of the collection of German standard methods. Information on Parts of these series of standards that have already been published can
22、be obtained from the offices of the Normenausschuss Wasserwesen, telephone +49 30 2601-2448, or from Beuth Verlag GmbH, Burggrafenstr. 6, 10787 Berlin. Amendments This standard differs from DIN EN ISO 5667-13:1998-02 as follows: a) the title of the standard has been shortened; b) 13 further terms an
23、d definitions have been added; c) Clause 4 “Developing a sampling plan” has been added; d) Clause 5 “Sampling equipment and containers” has been revised and restructured; e) Clause 6 “Sampling procedure” has been extended to include a new Subclause 6.1.4.2 “Number of sub-samples”; f) new informative
24、 annexes have been added: Annex A “Support on the selection of equipment”; Annex D “Minimum number of samples in a composite sample Calculation example; g) the standard has been editorially revised. Previous editions DIN 38414-1: 1986-11 DIN EN ISO 5667-13: 1998-02 DIN EN ISO 5667-13:2011-0 5 Nation
25、al Annex NA (informative) Bibliography DIN 38402-11, German standard methods for the examination of water, waste water and sludge General information (group A) Part 11: Sampling of waste DIN 38414-11, German standard methods for the examination of water, waste water and sludge Sludge and sediments (
26、group S) Sampling of sediments (S 11) DIN EN ISO 5667-1, Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques DIN EN ISO 5667-15, Water quality Sampling Part 15: Guidance on the preservation and handling of sludge and sediment samples DIN EN ISO 5667-1
27、6, Water quality Sampling Part 16: Guidance on biotesting of samples DIN ISO 3534-2, Statistics Vocabulary and symbols Part 2: Applied statistics2)DIN ISO 10381-4, Soil quality Sampling Part 4: Guidance on the procedure for investigation of natural, near-natural and cultivated sites DIN ISO 10381-6,
28、 Soil quality Sampling Part 6: Guidance on the collection, handling and storage of soil under aerobic conditions for the assessment of microbiological processes, biomass and diversity in the laboratory 2) At draft stage 8DIN EN ISO 5667-13:2011-08 6 This page is intentionally blank EUROPEAN STANDARD
29、 NORME EUROPENNE EUROPISCHE NORM EN ISO 5667-13 May 2011 ICS 13.060.45; 13.060.30 Supersedes EN ISO 5667-13:1997English Version Water quality - Sampling - Part 13: Guidance on sampling of sludges (ISO 5667-13:2011) Qualit de leau - chantillonnage - Partie 13: Lignes directrices pour lchantillonnage
30、de boues (ISO 5667-13:2011) Wasserbeschaffenheit - Probenahme - Teil 13: Anleitung zur Probenahme von Schlmmen (ISO 5667-13:2011) This European Standard was approved by CEN on 30 April 2011. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for
31、giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three
32、official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodie
33、s of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United King
34、dom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 5667-13:2011: E
35、Contents Page Foreword3 Introduction .4 1 Scope 5 2 Normative references 5 3 Terms and definitions .6 4 Developing a sampling plan .7 4.1 Sampling objectives 7 4.2 Variability considerations .8 5 Sampling equipment and containers.8 5.1 General8 5.2 Sampling equipment .8 5.3 Containers and sample pre
36、servation.8 6 Sampling procedure 9 6.1 Sampling regime9 6.2 Replicate sampling 11 6.3 Methodology.12 6.4 Sample homogenization and sub-sampling for sludge cakes (quartering) 15 7 Sample storage 16 7.1 General16 7.2 Storage17 8 Safety 17 9 Labelling and reporting.17 Annex A (informative) Support on t
37、he selection of equipment 18 Annex B (informative) Vacuum sampling devices .22 Annex C (informative) Apparatus for sampling from pipes under pressure.24 Annex D (informative) Minimum number of samples in a composite sample Calculation example 26 Bibliography 28 DIN EN ISO 5667-13:2011-08 EN ISO 5667
38、-13:2011 (E) 2 Foreword This document (EN ISO 5667-13:2011) has been prepared by Technical Committee ISO/TC 147 “Water quality” in collaboration with Technical Committee CEN/TC 308 “Characterization of sludges” the secretariat of which is held by AFNOR. This European Standard shall be given the stat
39、us of a national standard, either by publication of an identical text or by endorsement, at the latest by November 2011, and conflicting national standards shall be withdrawn at the latest by November 2011. Attention is drawn to the possibility that some of the elements of this document may be the s
40、ubject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 5667-13:1997. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to imple
41、ment this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Swi
42、tzerland and the United Kingdom. Endorsement notice The text of ISO 5667-13:2011 has been approved by CEN as a EN ISO 5667-13:2011 without any modification. DIN EN ISO 5667-13:2011-08 EN ISO 5667-13:2011 (E) 3 Introduction This part of ISO 5667 should be read in conjunction with ISO 5667-1 and ISO 5
43、667-15. The general terminology used is in accordance with the various parts of ISO 6107. Sampling and the determination of the physical and chemical properties of sludges and related solids are normally carried out for a specific purpose. The sampling methods given are suitable for general use but
44、do not exclude modification in the light of any special factor known to the analyst receiving the samples or any operational reason dictating the need for sampling. Personnel taking samples should be fully aware of safety requirements before sampling occurs. The importance of using a valid sampling
45、technique cannot be overemphasized if the subsequent analysis is to be worthwhile. It is important that the personnel taking and analysing the sample be fully aware of its nature and the purpose for which the analysis is required before embarking on any work programme. Full cooperation with the labo
46、ratory analysing the samples ensures that the most effective application of the sampling occasion can be made. For example, the use of method-specific sample preservation techniques assists in the accurate determination of results. This part of ISO 5667 is applicable to sampling motivated by differe
47、nt objectives, some of which are to: a) provide data for the operation of activated sludge plants; b) provide data for the operation of sludge treatment facilities; c) determine the concentration of pollutants in wastewater sludges for disposal to landfill; d) test whether prescribed substance limit
48、s are contravened when sludge is used in agriculture; e) provide information on process control in potable and wastewater treatment, including: 1) addition or withdrawal of solids, 2) addition or withdrawal of liquid; f) provide information for legally enforceable aspects of the disposal of sewage a
49、nd waterworks sludges; g) facilitate special investigations into the performance of new equipment and processes; h) optimize costs, e.g. for the transport of sludges for treatment or disposal. When designing a sludge sampling programme, it is essential that the objectives of the study be kept in mind, so that the information gained corresponds to that required. In addition, the data should not be distorted by the use of inappropriate techniques, e.g. inadequate s
