1、BS EN ISO10414-1:2008ICS 75.180.10NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBRITISH STANDARDPetroleum and naturalgas industries Fieldtesting of drillingfluidsPart 1: Water-based fluids (ISO10414-1:2008)This British Standardwas published under theauthority of the Standards
2、Policy and StrategyCommittee on 31 December2008 BSI 2008ISBN 978 0 580 56015 6Amendments/corrigenda issued since publicationDate CommentsBS EN ISO 10414-1:2008National forewordThis British Standard is the UK implementation of EN ISO10414-1:2008. It supersedes BS ISO 10414-1:2001 which is withdrawn.T
3、he UK participation in its preparation was entrusted to TechnicalCommittee PSE/17/-/3, Drilling and completion fluids and well cements.A list of organizations represented on this committee can be obtained onrequest to its secretary.This publication does not purport to include all the necessary provi
4、sionsof a contract. Users are responsible for its correct application.Compliance with a British Standard cannot confer immunityfrom legal obligations.EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN ISO 10414-1November 2008ICS 75.180.10English VersionPetroleum and natural gas industries - Field tes
5、ting of drillingfluids - Part 1: Water-based fluids (ISO 10414-1:2008)Industries du ptrole et du gaz naturel - Essais in situ desfluides de forage - Partie 1: Fluides aqueux (ISO 10414-1:2008)Erdl- und Erdgasindustrie - Feldprfung vonBohrflssigkeiten - Teil 1: Flssigkeiten auf Wasserbasis(ISO 10414-
6、1:2008)This European Standard was approved by CEN on 23 October 2008.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographica
7、l references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN mem
8、ber into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, La
9、tvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussel
10、s 2008 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN ISO 10414-1:2008: EBS EN ISO 10414-1:2008EN ISO 10414-1:2008 (E) 3 Foreword The text of ISO 10414-1:2008 has been prepared by Technical Committee ISO/TC 67 “Materials, equipment
11、and offshore structures for petroleum and natural gas industries” of the International Organization for Standardization (ISO) and has been taken over as EN ISO 10414-1:2008 by Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas ind
12、ustries” the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2009, and conflicting national standards shall be withdrawn at the latest by May 2009. Atten
13、tion is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of
14、the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slova
15、kia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 10414-1:2008 has been approved by CEN as a EN ISO 10414-1:2008 without any modification. BS EN ISO 10414-1:2008ISO 10414-1:2008(E) ISO 2008 All rights reserved iiiContents Page Foreword. v Introducti
16、on . vi 1 Scope . 1 2 Terms and definitions. 2 3 Symbols and abbreviated terms . 2 3.1 Symbols . 2 3.2 Abbreviations 6 4 Drilling fluid density (mud weight) 7 4.1 Principle. 7 4.2 Apparatus 7 4.3 Procedure 7 4.4 Calculation. 8 5 Alternative drilling fluid density method 9 5.1 Principle. 9 5.2 Appara
17、tus 10 5.3 Procedure 10 5.4 Calculation. 10 6 Viscosity and gel strength . 11 6.1 Principle. 11 6.2 Determination of viscosity using the Marsh funnel 11 6.3 Determination of viscosity and/or gel strength using a direct-indicating viscometer 11 7 Filtration. 14 7.1 Principle. 14 7.2 Low-temperature/l
18、ow-pressure test 14 7.3 High-temperature/high-pressure (HTHP) test 15 8 Water, oil and solids contents. 18 8.1 Principle. 18 8.2 Apparatus 18 8.3 Procedure 19 8.4 Calculation. 20 9 Sand content . 22 9.1 Principle. 22 9.2 Apparatus 22 9.3 Procedure 22 10 Methylene blue capacity 23 10.1 Principle. 23
19、10.2 Reagents and apparatus 23 10.3 Procedure 24 10.4 Calculation. 26 11 pH . 26 11.1 Principle. 26 11.2 Reagents and apparatus 27 11.3 Procedure for pH measurement 28 11.4 Care of electrode. 29 12 Alkalinity and lime content 29 12.1 Principle. 29 BS EN ISO 10414-1:2008ISO 10414-1:2008(E) iv ISO 200
20、8 All rights reserved12.2 Reagents and apparatus 30 12.3 Procedure Phenolphthalein and methyl orange filtrate alkalinities 30 12.4 Procedure Phenolphthalein drilling fluid alkalinity 31 12.5 Calculation of ion concentrations from Pfand Mf31 12.6 Estimation of lime content . 31 13 Chloride ion conten
21、t . 32 13.1 Principle . 32 13.2 Reagents and apparatus 32 13.3 Procedure. 32 13.4 Calculation. 32 14 Total hardness as calcium . 33 14.1 Principle . 33 14.2 Reagents and apparatus 33 14.3 Procedure. 34 14.4 Calculation. 35 Annex A (informative) Chemical analysis of water-based drilling fluids 36 Ann
22、ex B (informative) Shear strength measurement using shearometer tube . 52 Annex C (informative) Resistivity 54 Annex D (informative) Removal of air or gas prior to testing 56 Annex E (informative) Drill pipe corrosion ring coupon. 57 Annex F (informative) Sampling, inspection and rejection 61 Annex
23、G (informative) Rig-site sampling . 63 Annex H (informative) Calibration and verification of glassware, thermometers, viscometers, retort-kit cup and drilling fluid balances 66 Annex I (normative) High-temperature/high-pressure filtration testing of water-based drilling fluids using the permeability
24、-plugging apparatus and cells equipped with set-screw-secured end caps 71 Annex J (normative) High-temperature/high-pressure filtration testing of water-based drilling fluids using the permeability-plugging apparatus and cells equipped with threaded end caps 81 Annex K (informative) Water-based dril
25、ling fluids report form 90 Bibliography . 91 BS EN ISO 10414-1:2008ISO 10414-1:2008(E) ISO 2008 All rights reserved vForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Stand
26、ards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also ta
27、ke part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees i
28、s to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibili
29、ty that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 10414-1 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and
30、 natural gas industries, Subcommittee SC 3, Drilling and completion fluids, and well cements. This second edition cancels and replaces the first edition (ISO 10414-1:2001), to which Annexes I, J and K have been added and other minor changes made to the sentence structure, grammar and other non-techn
31、ical editing. ISO 10414 consists of the following parts, under the general title Petroleum and natural gas industries Field testing of drilling fluids: Part 1: Water-based fluids Part 2: Oil-based fluids BS EN ISO 10414-1:2008ISO 10414-1:2008(E) vi ISO 2008 All rights reservedIntroduction This part
32、of ISO 10414 is based on API RP 13B-1, third edition, December 20032and ISO 10414 (all parts)6. Annexes A to H and K of this part of ISO 10414 are for information only. Annexes I and J are normative. In this part of ISO 10414, where practical, U.S. Customary (USC) units are included in brackets for
33、information. BS EN ISO 10414-1:2008INTERNATIONAL STANDARD ISO 10414-1:2008(E) ISO 2008 All rights reserved 1Petroleum and natural gas industries Field testing of drilling fluids Part 1: Water-based fluids DANGER As with any laboratory procedure requiring the use of potentially hazardous chemicals, t
34、he user is expected to have proper knowledge and to have received training in the use and disposal of these chemicals. The user is responsible for compliance with all applicable local, regional and national requirements for worker and local health, safety and environmental liability. 1 Scope This pa
35、rt of ISO 10414 provides standard procedures for determining the following characteristics of water-based drilling fluids: a) drilling fluid density (mud weight); b) viscosity and gel strength; c) filtration; d) water, oil and solids contents; e) sand content; f) methylene blue capacity; g) pH; h) a
36、lkalinity and lime content; i) chloride content; j) total hardness as calcium. Annexes A through K provide additional test methods which may be used for chemical analysis for calcium, magnesium, calcium sulfate, sulfide, carbonate and potassium; determination of shear strength; determination of resi
37、stivity; removal of air; drill-pipe corrosion monitoring; sampling, inspection and rejection; BS EN ISO 10414-1:2008ISO 10414-1:2008(E) 2 ISO 2008 All rights reserved rig-site sampling; calibration and verification of glassware, thermometers, viscometers, retort-kit cup and drilling-fluid balances;
38、permeability-plugging testing at high temperature and high pressure for two types of equipment; example of a report form for water-based drilling fluid. 2 Terms and definitions For the purposes of this document, the following terms and definitions apply. 2.1 ACS reagent grade chemical meeting the pu
39、rity standards specified by the American Chemical Society (ACS) 2.2 darcy permeability of a porous medium, where one darcy is the flow of a single-phase fluid of 1 cP viscosity that completely fills the voids of the porous medium, flowing through the medium under conditions of viscous flow at a rate
40、 of 1 mls1cm2cross-sectional area and under a pressure or equivalent hydraulic gradient of 1 atmcm1 NOTE 1 cP = 1 mPas. 2.3 quarter verb mix and divide into four specimens to ensure homogeneity of specimens 2.4 spurt loss volume of fluid that passes through the filtration medium before a filter cake
41、 is formed 2.5 tube sampling sampling method consisting of the withdrawal of powdered sample from bag or bulk via a cylindrical device pushed into the sample, locked shut and withdrawn 3 Symbols and abbreviated terms 3.1 Symbols NOTE Subscript “A” to symbol denotes metric units. Subscript “B” to sym
42、bol denotes U.S. customary units. AAarea, in square centimetres ABarea, in square inches cb,Aconcentration of weighting material, in kilograms per cubic metre cb,Bconcentration of weighting material, in pounds per barrel cCa,Aconcentration of calcium ion, in milligrams per litre cCa,Bconcentration o
43、f calcium ion, in parts per million by mass (USC) BS EN ISO 10414-1:2008ISO 10414-1:2008(E) ISO 2008 All rights reserved 3cCa+Mg,Aconcentration of calcium and magnesium ion (total hardness), in milligrams per litre cCa+Mg,Bconcentration of calcium and magnesium ion (total hardness), in parts per mil
44、lion (USC) cCaSO4,Aconcentration of calcium sulfate, in milligrams per litre cCaSO4,Bconcentration of calcium sulfate, in parts per million by mass (USC) cCO2+CO3+HCO3,Aconcentration of total soluble carbonates, in milligrams per litre cCO2+CO3+HCO3,Bconcentration of total soluble carbonates, in par
45、ts per million by mass (USC) cCl,Aconcentration of chloride ion, in milligrams per litre cCl,Bconcentration of chloride ion, in parts per million by mass (USC) cex-CaSO4,Aconcentration of excess, undissolved calcium sulfate, in milligrams per litre cex-CaSO4,Bconcentration of excess, undissolved cal
46、cium sulfate, in parts per million by mass (USC) cf,KCl,Aconcentration of potassium chloride in filtrate, in milligrams per litre cf,KCl,Bconcentration of potassium chloride in filtrate, in parts per million by mass (USC) cK,Aconcentration of potassium ion, in milligrams per litre cK,Bconcentration
47、of potassium ion, in parts per million by mass (USC) cKCl,Aconcentration of potassium chloride, in milligrams per litre cKCl,Bconcentration of potassium chloride, in parts per million by mass (USC) clg,Aconcentration of low-gravity solids, in kilograms per cubic metre clg,Bconcentration of low-gravi
48、ty solids, in pounds per barrel clime,Alime content of the drilling fluid, in kilograms per cubic metre clime,Blime content of the drilling fluid, in pounds per barrel cNaCl,A concentration of sodium chloride, in milligrams per litre cNaCl,Bconcentration of sodium chloride, in parts per million by m
49、ass (USC) cS,Aconcentration of sulphide ion, in milligrams per litre cS,Bconcentration of sulphide ion, in parts per million by mass (USC) cSS,Asuspended solids concentration, in kilograms per cubic metre cSS,B suspended solids concentration in pounds per barrel cMBTmethylene blue capacity cththermometer correction to be added to the working thermometer reading D outer diameter EBE,Abentonite equivalent, expressed in kilograms per cubic metre BS EN ISO 10414-1:2008ISO 10414-1:2008(E) 4 ISO 2008 All r
