1、BS EN ISO13500:2008ICS 75.180.10NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBRITISH STANDARDPetroleum and naturalgas industries Drilling fluid materials Specifications andtests July 2009corrigendumIncorporating+A1:2010National forewordThis British Standard is the UK impleme
2、ntation of EN ISO 13500:2008+A1:2010. It is identical to ISO 13500:2008, incorporating amendment 1:2010 and corrigendum July 2009. It supersedes BS EN ISO 13500:2008 which is withdrawn.The start and finish of text introduced or altered by amendment is indicated in the text by tags. Tags indicating c
3、hanges to ISO text carry the number of the ISO amendment. For example, text altered by ISO amendment 1 is indicated by !“.The UK participation in its preparation was entrusted to Technical Committee PSE/17/-/3, Drilling and completion fluids and well cements.A list of organizations represented on th
4、is committee can be obtained on request to its secretary. Hazard warning (clause 12 - Attapulgite)Attapulgite fibres bear similarities to asbestos fibres, which present a potential health risk. As a result, some countries and various operators have banned attapulgite from their drilling operations.
5、However, although the most commonly encountered forms of attapulgite are fibrous, some are granular. If attapulgite is to be used in drilling operations, then appropriate health and safety precautions should be employed for its handling, usage and disposal.This publication does not purport to includ
6、e all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot confer immunity from legal obligations. BS EN ISO 13500:2008+A1:2010This British Standard was published under the authority of the Standards Policy and Strategy
7、Committee on 28 February 2009 BSI 2011Amendments/corrigenda issued since publicationDate Comments 31 December 2009 Implementation of ISO corrigendum July 2009, calculation in C.2.3 replaced31 March 2011 Implementation of ISO amendment 1:2010 and its CEN endorsement A1:2010ISBN 978 0 580 69375 5EUROP
8、EAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN ISO 13500:2008+A1December 2010ICS 75.180.10 Supersedes EN ISO 13500:2006 English VersionPetroleum and natural gas industries - Drilling fluid materials -Specifications and tests (ISO 13500:2008)Industries du ptrole et du gaz naturel - Produits pourfluides
9、 de forage - Spcifications et essais (ISO13500:2008)Erdl- und Erdgasindustrie - Bohrsplungen -Spezifikationen und Prfungen (ISO 13500:2008)This European Standard was approved by CEN on 12 October 2008.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the condi
10、tions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three o
11、fficial versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria
12、, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE
13、FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: Avenue Marnix 17 B-1050 Brussels 2010 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN ISO 13500:2008: E3 Foreword This document (EN ISO
14、 13500:2008) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas indus
15、tries” the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2009, and conflicting national standards shall be withdrawn at the latest by May 2009. Attenti
16、on is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 13500:2006. According to the CEN/CENELEC Internal Regulations
17、, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands
18、, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 13500:2008 has been approved by CEN as a EN ISO 13500:2008 without any modification. Foreword to amendment A1This document (EN ISO 13500:2008/A1:2010) has be
19、en prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industrie
20、s” the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2011, and conflicting national standards shall be withdrawn at the latest by June 2011. Attention
21、 is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the
22、following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,
23、Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 13500:2008/A1:2010 has been approved by CEN as a EN ISO 13500:2008/A1:2010 without any modification. BS EN ISO 13500:2008+A1:2010EN ISO 13500:2008+A1:2010 (E)iiiContents Page Foreword iv Introdu
24、ction v 1 Scope . 1 2 Normative references . 1 3 Terms, definitions, symbols and abbreviations 1 4 Requirements 4 5 Calibration . 4 6 Packaged material 11 7 Barite 13 8 Haematite (hematite) 22 9 Bentonite . 30 10 Non-treated bentonite. 34 11 OCMA grade bentonite. 36 12 Attapulgite . 40 13 Sepiolite
25、. 43 14 Technical-grade low-viscosity CMC (CMC-LVT) 46 15 Technical-grade high-viscosity CMC (CMC-HVT) 50 16 Starch. 55 17 Low-viscosity polyanionic cellulose (PAC-LV) 59 18 High-viscosity polyanionic cellulose (PAC-HV) 66 19 Drilling-grade xanthan gum . 71 Annex A (informative) Mineral impurities i
26、n barite . 93Annex B (informative) Test precision. 94Annex C (informative) Examples of calculations 99Bibliography 103BS EN ISO 13500:2008+A1:2010EN ISO 13500:2008+A1:2010 (E) ISO 201120 Barite 4,1 . 82 iv Foreword ISO (the International Organization for Standardization) is a worldwide federation of
27、 national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. Int
28、ernational organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with t
29、he rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval
30、by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 13500 was prepared by Technical Committee I
31、SO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids, and well cements. This third edition cancels and replaces the second edition (ISO 13500:2006), subclauses 7.1.2/Table 2, 7.3.1, 8.5.2, 8.
32、6.5, 8.13.4, 10.2.5, 11.4, 14.4.3, and 15.4.3 of which have been technically revised. Clause 17 on low-viscosity polyanionic cellulose, Clause 18 on high-viscosity polyanionic cellulose, and Clause 19 on drilling-grade xanthan gum have been added. BS EN ISO 13500:2008+A1:2010EN ISO 13500:2008+A1:201
33、0 (E) ISO 2011vIntroduction This International Standard covers materials that are in common usage in petroleum and natural-gas drilling fluids. These materials are used in bulk quantities, can be purchased from multiple sources and are available as commodity products. No single-source or limited-sou
34、rce products are included, nor are speciality products. International Standards are published to facilitate communication between purchasers and manufacturers, to provide interchangeability between similar equipment and materials purchased from different manufacturers and/or at different times and t
35、o provide an adequate level of safety when the equipment or materials are utilized in the manner and for the purposes intended. This International Standard provides minimum requirements and is not intended to inhibit anyone from purchasing or producing materials to other standards. This Internationa
36、l Standard is substantially based on API Spec 13A, 16th Edition, February 1, 2004. The purpose of this International Standard is to provide product specifications for barite, haematite, bentonite, nontreated bentonite, Oil Companies Materials Association (OCMA) grade bentonite, attapulgite, sepiolit
37、e, technical-grade low-viscosity carboxymethylcellulose (CMC-LVT), technical-grade high-viscosity carboxymethylcellulose (CMC-HVT), starch, low-viscosity polyanionic cellulose, high-viscosity polyanionic cellulose and drilling-grade Xanthomaonas campestris. The intent of the document is to incorpora
38、te all International Standards for drilling fluid materials into an ISO-formatted document. A survey of the industry found that only the American Petroleum Institute (API) issued testing procedures and specification standards for these materials. Reference to OCMA materials has been included in API
39、work, as the OCMA and subsequent holding committees were declared defunct, and all specifications were submitted to API in 1983. Annex A (informative) lists the mineral impurities in barite, Annex B (informative) provides the test precision and Annex C (informative) details examples of calculations.
40、 BS EN ISO 13500:2008+A1:2010EN ISO 13500:2008+A1:2010 (E) ISO 2011INTERNATIONAL STANDARD 1Petroleum and natural gas industries Drilling fluid materials Specifications and tests 1 Scope This International Standard covers physical properties and test procedures for materials manufactured for use in o
41、il- and gas-well drilling fluids. The materials covered are barite, haematite, bentonite, nontreated bentonite, OCMA-grade bentonite, attapulgite, sepiolite, technical-grade low-viscosity carboxymethylcellulose (CMC-LVT), technical-grade high-viscosity carboxymethylcellulose (CMC-HVT), starch, low-v
42、iscosity polyanionic cellulose (PAC-LV), high-viscosity polyanionic cellulose (PAC-HV) and drilling-grade Xanthomonas campestris (Xanthan gum). This International Standard is intended for the use of manufacturers of named products. 2 Normative references The following referenced documents are indisp
43、ensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 6780, Flat pallets for intercontinental materials handling Principal dimensions and tolera
44、nces ISO 10414-1:2008, Petroleum and natural gas industries Field testing of drilling fluids Part 1: Water-based fluids ASTM D422, Standard Test Method for Particle-Size Analysis of Soils ASTM E11, Standard Specification for Wire Cloth and Sieves for Testing Purposes ASTM E161, Standard Specificatio
45、n for Precision Electroformed Sieves ASTM E77, Standard Test Method for Inspection and Verification of Thermometers ASTM E177, Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods NIST (NBS) Monograph 150, Liquid-In-Glass Thermometry 3 Terms, definitions, symbols and abbrev
46、iations 3.1 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1.1 ACS reagent grade chemicals that meet purity standards as specified by the American Chemical Society (ACS) BS EN ISO 13500:2008+A1:2010EN ISO 13500:2008+A1:2010 (E) ISO 20112 3.1.2 f
47、lash side side containing residue (“flash”) from stamping, or the side with concave indentation 3.2 Symbols and abbreviations ACS American Chemical Society API American Petroleum Institute APME Association of Plastic Manufacturers in Europe ASTM American Society for Testing and Materials EDTA Ethyle
48、nediaminetetraacetic acid CAS Chemical Abstracts Service CMC-HVT Carboxymethylcellulose High-viscosity, technical-grade CMC-LVT Carboxymethylcellulose Low-viscosity, technical-grade OCMA Oil Companies Materials Association NBS National Bureau of Standards NIST National Institute of Standards and Tec
49、hnology TC to contain TD to deliver Bchydrometer correction curve intercept b yield point/plastic viscosity ratio D1equivalent particle diameter immediately greater than 6 m, determined in Equation (9) D2equivalent particle diameter immediately less than 6 m, determined in Equation (9) Deequivalent spherical diameter, expressed in micrometres Cccalibration correction Cm40 times the EDTA volume, expressed in millilitres KSsample constant L effective depth, expressed in centimetres log(20/) correction for temperature variance Mchydrometer correctio
