1、 FORD LABORATORY TEST METHOD BO 131-03 Date Action Revisions Rev. 7 2016 03 22 Revised Clarified sample air exposure conditions, see revisions M. Corley, FoE 2014 04 10 Revised See summary of revisions, added 80 C for China only D. Stark, NA 2007 06 07 Activated J.Williams FOE Controlled document at
2、 www.MATS Copyright 2016, Ford Global Technologies, LLC Page1 of 7 INTERIOR ODOR TEST Application This test method is used to determine the odor originating from interior trim materials/components/assemblies in the passenger or luggage compartment or from parts or ducting that convey air into the pa
3、ssenger compartment as dictated by the Material and/or Performance Specifications. Customer Clinics have indicated that the customer expects a new vehicle to have a neutral or new car smell. This test is designed to establish whether parts and materials used in a vehicle have an inappropriate or dis
4、turbing odor. Apparatus and Materials Required Mechanical Convection Ovens Capable of maintaining the specified test temperatures. 3-Litre Odorless Preserving Jar with Lid Dimensions of jar: approximately 250 mm high x 125 mm diameter; neck 100 mm diameter. The jar and any seals it may employ must b
5、e odorless. A suitable odorless material for the jar seals is polyethylene closed cell foam, 3 mm thick of 45 kg/m3 density. Suitable suppliers for jars of this type are: A Le Parfait French Glass Canning Jar with 100 mm Gasket and Lid-3 Liter French Flint and Ormco Ltd. Product Name/Code: Kiln300
6、0 Suitable supplier of material for making jar seals is: RS Components Ltd http:/uk.rs- Stock Number: 733 6696 UFP Technologies Stock Number: LD45 Plastazote Stainless Steel Wire Ring/Support Frame The above material is available from any reputable laboratory equipment supply house. Distilled or De
7、ionized Water 20 micro ohms/cm at 25 C maximum conductivity (ASTM D1125). Sample Preparation The area or weight and number of samples is determined using Table 1 below. The choice of variants A, B, C or D is based upon the area or weight content of each material used in the vehicle interior. FORD LA
8、BORATORY TEST METHOD BO 131-03 Copyright 2016, Ford Global Technologies, LLC Page 2 of 7 TABLE 1 Variant Application Specimen Weight/Size* A Clips, plugs, covers, foils and other small parts Sum of total, similar parts. Equal to or greater than 100 g or 100 cm2 B Armrests, ashtrays, door handles, sh
9、ift lever gaiters, sun visors, steering wheels, door/window seals and other medium size parts 1 each of 90 x 200 mm. If the component is less than 90 x 200 mm, test the actual part, i.e. door handles. For steering wheels, door/window seals or similar parts cut the component into a 200 mm length size
10、 C Seat Trim/roof covers, sound-deadeners, foils, foam materials, carpets, ducting and other large surface materials 3 each of 90 x 200 mm (in same jar) D* Sealers, adhesives, liquid applied sound deadeners and antiflutter mastics Panel dimensions: 200 x 100 x 0.8 mm Substrate: -Paint shop applied m
11、aterials-HDG with EC -Body shop applied materials-HDG substrate (cleaned and degreased) Materials dimensions: -Paint shop sealer-150 x 85 x 1 mm bead* -Body Shop sealer -100 x 6 mm bead* Curing conditions: FLTM BV 150-05 at minimum, nominal and maximum Age sample for 14-28 days after manufacture at
12、room temperature prior to bagging to allow for curing * Do not test components less than 100 g or 100 cm2. Surface area is determined as sum of areas exposed to car interior cabin. *Unless otherwise noted in the material specification. Note: For material testing, select variant per intended part app
13、lication. For materials used in several applications, test to the largest application variant. If the material thickness of a homogeneous material is more than 20 mm, then the sample is to be prepared for a 20 mm thickness. Sandwich materials must be tested in their compound state. FORD LABORATORY T
14、EST METHOD BO 131-03 Copyright 2016, Ford Global Technologies, LLC Page 3 of 7 Conditioning of Materials, Air Exposure and Test Conditions All test values indicated herein are based on material conditioned in a controlled atmosphere of 23 2 C and 50 5% relative humidity, for not less than 24 hours p
15、rior to testing, and tested under the same conditions unless otherwise specified. Parts should be exposed to the air for a period of time after manufacture and before testing. This helps ensure samples and parts are representative of behavior in vehicles. This period of time of air exposure is as fo
16、llows: Part is produced in China 7-14 days air exposure Part is produced anywhere but China 14-28 days air exposure The following points should be observed during the time of exposure to air: Temperature should not exceed 25 C Normal atmospheric pressures and humidities should be maintained Parts/Sa
17、mples should not be exposed to air in contaminated locations or locations with poor air quality Maximize the exposed area of the parts during air exposure (i.e. plaques should not be stacked but stored such that face and back sides are not in direct contact with other plaques) All parts or samples s
18、hould be wrapped/bagged for shipping and/or to limit the air exposure time as per the durations listed above. For wrapping/bagging one of the following should be used: heat sealed polyethylene (PE) bags clean plastic wrap foil (PE or PP) PE coated aluminum bags or aluminum foil Beginning and end dat
19、e of air exposure should be declared with the information supplied with the part. This is important for the test laboratory to know if air exposure has already occurred. Parts for testing must be labeled with the following information: Supplier Name Contact information Date of manufacture Beginning
20、and end date of air exposure Curing condition if applicable Program code if applicable Part number if applicable Part name if applicable Plant and location Shipping date Procedure 1. Clean the jars, lids (using laboratory washing machines) and seals (hand or machine wash) before each use. They must
21、be clean and odorless. 2. A blank test jar may be employed, as a control, to ensure that the jars are odorless and the water quality does not create an odor. 3. The jars containing the specimen(s) (or blank) should be conditioned and assessed per Table 2 below. FORD LABORATORY TEST METHOD BO 131-03
22、Copyright 2016, Ford Global Technologies, LLC Page 4 of 7 TABLE 2: Summary of Test Conditions Use a separate specimen and jar for each condition. Condition Temperature Test Time 1 23 2 C 24 h 1 h 2 40 2 C 24 h 1 h 3 65 2 C 2 h 10 min 4 (China Only)* 80 2 C 2 h 10 min *Applies to parts that are for t
23、he China market and regionally sourced only. Condition 1: Add 50 5 ml of distilled or deionized water to the jar(s). Take a stainless steel wire ring or support and suspend or stand the specimen(s) to be tested in the jar(s). The specimens are to be placed in the jar(s) in such a way to prevent dire
24、ct contact with the water and to avoid wetting the specimen(s). Close the jar(s) and allow the specimen(s) to condition for 24 h 1 hr at 23 2 C. Immediately evaluate the odor. Condition 2: Pre-heat an oven to 40 2 C. Add 50 5 ml of distilled or deionized water to the jar(s). Take a stainless steel w
25、ire ring or support and suspend or stand the specimen(s) to be tested in the jar(s). The specimen(s) are to be placed in the jar(s) in such a way to prevent direct contact with the water and to avoid wetting the specimen(s). Close the jar(s) and place in the pre-heated oven for 24 h 1 hr at 40 2 C.
26、Remove jar(s) from the pre-heated oven and immediately evaluate the odor. Return the jar(s) to the pre-heated oven at 40 2 C for 15 2 minutes between odor assessments. Condition 3: Pre-heat oven to 65 2 C. Take a stainless steel wire ring or support and suspend or stand the specimen(s) to be tested
27、in the jar(s). Close the jar(s) and place in the pre-heated oven for 2 h 10 min at 65 2 C. Remove the jar(s) from the pre-heated oven and immediately evaluate the odor. Three assessors (maximum) are permitted to evaluate the odor at one time. One minute, maximum total time, is allowed for the three
28、assessors to evaluate the odor prior to returning the jars to the pre-heated 65 2 C oven*. Return the jar(s) to the pre-heated oven at 65 2 C for 15 mintues (minimum) between odor assessments. FORD LABORATORY TEST METHOD BO 131-03 Copyright 2016, Ford Global Technologies, LLC Page 5 of 7 Condition 4
29、 for CHINA ONLY: Pre-heat oven to 80 2 C. Take a stainless steel wire ring or support and suspend or stand the specimen(s) to be tested in the jar(s). Close the jar(s) and place in the pre-heated oven for 2 h 10 min at 80 2 C. Remove the jar(s) from the 80 2 C pre-heated oven then transfer the jar(s
30、) to a second pre-heated oven at 65 2 C for 15 minutes (minimum). Remove the jar(s) from the 65 2 C pre-heated oven and immediately evaluate the odor. Three assessors (maximum) are permitted to evaluate the odor at one time. One minute, maximum total, is allowed for the three assessors to evaluate t
31、he odor prior to returning the jars to the pre-heated 80 2 C oven*. Between odor assessments return the jars to the 80 2 C pre-heated oven for 30 5minutes. Then place the jar(s) in the 65 2 C pre-heated oven for 15 minutes (minimum) prior to the evaluation. * No more than three assessors are allowed
32、 per group. 4. Evaluating the Odor: The assessors should be selected from staff who do not work in the production facility. Heavy smokers, users of strong perfumes, or people with sinus problems are not suitable. All assessors must be aware of any risk assessment documents and Toxicology reports of
33、all submitted components, which should be readily available, if requested. Acceptance tests shall be made by a minimum of five assessors. If the rating of individual tests differs by more than two points, three additional assessors shall be used to retest the sample. The test must be conducted in an
34、 environment free from drafts and contaminant odors. The lid should be removed and the assessors nose should be positioned about 5 cm over the edge of the jar. The air from the jar should be wafted towards the assessors nose. The assessor should slowly inhale through the nose. The lid should not be
35、off the jar longer than 5 seconds. Record the appropriate rating (refer to “Rating Scale“). If the assessor gives a rating which would be classed as a failure, a description of the odor must be included in the report. The person conducting the Odor Test should not allow the assessors to view any pre
36、vious ratings or comments in any way. 5. Repeat Step 4 for each assessor and each sample. 6. The odor rating is indicated by the arithmetic mean of all the assessors individual ratings, the value being rounded up to the nearest half point. To ensure that odor differentiation can be established by th
37、e assessors, all conditions being tested shall be conducted in the same time frame. For all the variants and conditions, the odor evaluation uses the rating of 1 to 6, with half-point ratings, as follows: FORD LABORATORY TEST METHOD BO 131-03 Copyright 2016, Ford Global Technologies, LLC Page 6 of 7
38、 Rating Scale Rating 1 not perceptible Rating 1.5 slightly perceptible Rating 2 perceptible, not disturbing Rating 2.5 clearly perceptible but not disturbing Rating 3 very perceptible but not disturbing Rating 3.5 intense enough to be slightly disturbing Rating 4 disturbing Rating 4.5 intense and di
39、sturbing Rating 5 strongly disturbing Rating 5.5 very intense, disturbing Rating 6 extremely disturbing The definition of a disturbing odor is one that would be considered inappropriate for a new car smell. The smell of a component/ material is defined as disturbing, not when it is more concentrated
40、, but rather when it transitions from one acceptable odor to another unacceptable odor upon conditioning. The concentrated odor of hot plastic, hot rubber, hot leather, etc. would not qualify as a disturbing odor. A disturbing odor or inappropriate smell is also one that is identifiable as smells th
41、at are not normally associated with the interior of a new car, (i.e. sour milk, fish, perfume, burnt, musky, asphalt, rotten meat). The assessors should be encouraged to use the half point ratings to improve differentiation between samples. 7. The test report shall include: A reference to this stand
42、ard. All necessary details for identifying the test samples. Material variant classification (A, B, C or D) from Table 1. Test condition(s) (1, 2, 3, and/or 4) from Table 2. Identification of assessor by name or number. Individual and average odor rating. Samples defined as unacceptable should inclu
43、de an odor description. Special characteristics of the test samples and their condition, beginning and end dates of air exposure Date of manufacture of the samples and the date of the test. Any significant details of the manufacturing process (i.e. curing times) Example of the test result designatio
44、n: Designation Test Method Test Variant Test Condition Rating Odor Test FLTM BO131-03 B 2 3 average (2, 2.5, 2.5, 3, 3, 3) Odor Test FLTM BO131-03 C 3 4 average (3, 3, 4, 4, 5) Fish like smell Chemicals, materials, parts, and equipment referenced in this document must be used and handled properly. E
45、ach party is responsible for determining proper use and handling in its facilities. FORD LABORATORY TEST METHOD BO 131-03 Copyright 2016, Ford Global Technologies, LLC Page 7 of 7 Summary of Revisions 2016/03/22 Sources for odor testing jars Section “Conditioning of Materials and Test Conditions” ad
46、ded more statement to clarify that samples should be exposed to air for a defined period of time after manufacture and before testing. 2014/04/10 Added Condition 4 (80 C) for the China market only. Condition 4 will be re-evaluated in 6 - 12 months Added 7-14 day conditioning period for the China mar
47、ket only. Updated equipment supplier information Added test size note for Variant A Changed number of assessors from 3-5 to a minimum of five, changed assessment to be a mean instead of average Add descriptions for the half point scale Editorial changes for clarification 2013/10/25 Editorial Correct
48、ed odor average for first odor example 2013/04/15 Modified the test temperature for Condition 3 from 80 C to 65 C 2012/05/01 Added North America source for jar seal 2011/12/22 Updated application paragraph Variant A allowed usage of actual part if less than 30 g Deleted statement that if part size is weights less than 30 g multiple parts should be tested together to achieve 30 g minimum. Added option to use blank jar as a reference Added optional pre-heating for condition 3
