1、 ENGINEERING MATERIAL SPECIFICATIONDate Action Revisions Rev. 12011 10 05 Revised Editorial changes to 3.1.2 2011 09 07 Activated Replaces WSS-M4D582-A2 A. Pan and Global Materials TeamControlled document at www.MATS Copyright 2011, Ford Global Technologies, LLC Page 1 of 6 POLYBUTYLENE TEREPHTHALAT
2、E (PBT), POLYETHYLENE WRS-M4D582-B2 TEREPHTHALATE (PET), HEAT STABILIZED, 50% GLASS FIBER REINFORCED MOLDING COMPOUND, 18% PCR CONTENT 1. SCOPE The material defined by this specification is a heat stabilized 50% glass fiber reinforced injection molding compound based on a blend of polybutylene and p
3、olyethylene terephthalate compound containing 18% recycled content. 2. APPLICATION This specification was released originally for material used for fixed mirror brackets. 3. REQUIREMENTS 3.1 STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Material suppliers and part producers must conform to the Comp
4、anys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.1.1 Many 4D resin specifications prior to 2011, identified certain requirements with the symbol (s), which indicated that the mean and +/- 3 sigma values were to be reported. The specification minimum, maximum or range was estab
5、lished using 3 sigma data. For 2011 and beyond, refer to Table 1 for number of samples required for each test to establish specification limits. 3.1.2 Material approved to WRS-M4D582-B2 must contain 18% Post Consumer Recycled (PCR) content as defined by WRS-M99P42-A1. The remaining portion of the ma
6、terial can come from virgin sources. 3.1.3 The use of regrind is permitted, for economic and environmental reasons, with compliance as indicated in WSS-M99P1111-A. 3.2 SAMPLE PREPARATION Unless otherwise specified all tests shall be carried out on injection molded, one-end gated test specimens. The
7、test specimens A and D shall be molded using molding conditions defined in ISO 7792-2. No annealing is allowed. See Tables 1 and 2 for the number of samples required. Specimens shall be as follows: ENGINEERING MATERIAL SPECIFICATIONWRS-M4D582-B2 Copyright 2011, Ford Global Technologies, LLC Page 2 o
8、f 6 Specimen A 150 minimum x 10 x 4.0 +/- 0.2 mm (ISO 527-2, Specimen Type 1A) Specimen B 355 x 100 x 1.0 +/- 0.1 mm (ISO 3795) Specimen C 145 x 60 x 3.2 +/- 0.2 mm Specimen D Center of Specimen A, 80 x 10 x 4.0 +/- 0.2 mm Specimen E 100 mm diameter x 3.2 mm Specimen F 80 mm diameter x 3.2 mm Specim
9、en G 90 mm x 200 mm Specimen H 50 +/- 1 mm diameter x 3.2 +/- 0.2 mm Specimen I 100 mm x 150 mm, min 3.3 MATERIAL PROPERTIES 3.3.1 Filler Content 48 - 52 % (ISO 3451/2, glass fiber, test temperature 850 +/-25 C, test portion 2 to 2.5 g) 3.3.2 Melt Temperature 215 - 225 C (ISO 11357, 10 C/min heating
10、 rate) 3.3.3 Density 1.71 - 1.77 g/cm3(ISO 1183, Method A) 3.3.4 Tensile Strength at Break 130 MPa min (ISO 527-1 At 23 +/- 2 C 8.9 kJ/m23.4.4.2 Impact Strength, Notched Izod; At -40 +/- 2 C 8.4 kJ/m23.4.5 Melt Volume Rate 36 cm3/10 minutes 4.2 MATERIAL IDENTIFICATION FOR RECYCLING PURPOSES PBT+PET-
11、GF50 (ISO 1043/ 11469) 5. SUMMARY OF REVISIONS 2011 10 05 Editorial changes to 3.1.2ENGINEERING MATERIAL SPECIFICATIONWRS-M4D582-B2 Copyright 2011, Ford Global Technologies, LLC Page 6 of 6 Table 1: Minimum Sample Size Initial Approval New Manufacturing Location for Previously Approved Material Para
12、. Test Minimum Lots Specimens per Lot Total Test Specimens Lots Specimens per lot Total Test Specimens 3.1 WSS-M99P1111-A 3.3.1 Filler Content* 3 1 3 1 1 1 3.3.2 Melt Temperature* 3 1 3 1 1 1 3.3.3 Density 1 3 3 3.3.4 Tensile Strength at Break* 3 5 15 1 5 5 3.3.5 Tensile Modulus 1 10 10 3.3.6 Flexur
13、al Modulus* 3 10 30 1 10 10 3.3.7 Impact Strength Notched Charpy (per condition)* 3 10 30 1 10 10 3.3.8 Heat Deflection Temperature* 3 2 6 1 2 2 3.3.9 Heat Aged Properties 3.3.9.1 Tensile Strength at Break Change 1 5 5 3.3.9.2 Impact Strength, Notched Charpy Change 1 10 10 3.3.10 Flammability 1 5 5
14、3.4.1 Coefficient of Linear Thermal Expansion (per condition) 1 3 3 3.4.2 Mold Shrinkage 1 5 5 3.4.3 Poissons Ratio 1 5 5 3.4.4 Impact Strength, Notched Izod (per condition) 1 10 10 3.4.5 Melt Volume Rate 1 3 3 3.4.6 Curves - IR - TGA - DSC - CLTE - Engineering Stress/Strain at 23 C 1 1 1 per test * For these requirements, the 3 Sigma value from the raw data is used to set the requirement max or min.
