1、 ENGINEERING MATERIAL SPECIFICATIONDate Action Revisions 2009 10 27 N-STATUS No known use. No Replacement Named D. DiGregorio, NA 2004 05 27 Revised Para 3.0 inserted; para 3.1, 3.7 & 4 deleted 1995 02 28 Released C10460362Printed copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC
2、 Page 1 of 8 OIL - ENGINE, SAE 10W-30 API SG/CD, WSD-M2C904-B CONTROLLED VISCOSITY INITIAL FILL NOT TO BE USED FOR NEW DESIGN 1. SCOPE This material specification defines the minimum acceptable performance requirements and physical/chemical properties of engine oil to be used by Ford Motor Company i
3、n its worldwide engine/vehicle manufacturing operations. 2. APPLICATION This specification was released originally for initial fill engine oils used for lubrication of spark ignition engines using gasolines and for naturally aspirated and turbo-charged compression ignition engines using diesel fuels
4、. 3. REQUIREMENTS 3.0 STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Material suppliers and part producers must conform to the Companys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.2 PERFORMANCE Shall meet all the requirements of API service category “SG/CD“ as defined in SAE S
5、tandard J 183 (latest revision), “Engine Oil Performance and Engine Service Classification“, or in ASTM D 4485, “Standard Performance Specification for Automotive Engine Oils“. All required engine tests shall be conducted in accordance with the most recently approved procedures as described in ASTM
6、Special Technical Publications 315, 509 and applicable ASTM Research Reports and Information Letters. All tests under surveillance by ASTM must be conducted using test equipment monitored by and calibrated to the requirements of the ASTM Test Monitoring Center. 3.3 VISCOSITY GRADE Shall meet all the
7、 requirements of the applicable SAE viscosity grade as defined in SAE Standard J300 (latest revision), “Engine Oil Viscosity Classification“, except that the kinematic viscosity at 100 C shall be controlled within the limits 9.3 to 10.1 mm2/s. 3.4 ENERGY CONSERVING PERFORMANCE (ASTM Sequence VI) Ave
8、rage Improvement (EFEI), min 2.7% vs HR-2 or equiv. Shall meet all the requirements of the API “Energy Conserving II“ category as defined in SAE Recommended Practice J1423 (latest revision), “Passenger Car and Light Duty Truck Energy Conserving Oil Classification.“ All tests must be conducted using
9、test equipment monitored by and calibrated to the requirements of the ASTM Test Monitoring Center. ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-BPrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 2 of 8 3.5 PHYSICAL/CHEMICAL PROPERTIES 3.5.1 Viscosity at Temperature,
10、max (FLTM BJ 127-01, Scanning Brookfield) SAE 10W-30 30 Pa.s at -25 C Copy of curve plotted per FLTM BJ 127-01 (Figure 2) is required. 3.5.2 Viscosity (After Shear Evaluation) Report (mm2/s) (ASTM D 445 or ISO 3104 at 100 C) Sheared viscosity after each of the following tests: a. ASTM D 3945, or aft
11、er 30 cycles of CEC L-14A-78. b. ASTM STP 509 A, Part IV and ASTM D 3607, after 10 h in L-38 test and removal of volatile contaminants. 3.5.3 Viscosity at 150 C and 1E6/s, min (ASTM D 4683 or CEC L-36T-84) New Oil Sheared Oil* SAE 10W-30 2.9 mPa.s 2.6 mPa.s *Perform after item a. of para 3.5.2 3.5.4
12、 Volatility Shall meet either “Evaporative Loss“ or “Distillation by Gas Chromatography“ requirements as follows: Evaporative Loss (Noack), max (DIN 51581, 1 h at 250 C) SAE 10W-30 20% or Distillation by Gas Chromatography, max 20% (ASTM D 2887, Distilled at 371 C) 3.5.5 Flash Point, min 180 C (ASTM
13、 D 93 or ISO 2719) 3.5.6 Copper Corrosion, max 1b (Dark Orange) (ASTM D 130 or ISO 2160, 3 h at 100 C) 3.5.7 Filterability (FLTM BJ 124-01) Flow rate decrease, max 50% ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-BPrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 3 o
14、f 8 3.5.8 Foaming, max Foam Stability (ASTM D 892, Opt. A) Foaming Tendency 5 min Settling Sequence I 10 mL 0 mL Sequence II 50 mL 0 mL Sequence III 10 mL 0 mL Sequence IV* Rate and Rate and Report Report* * Same as Sequence I except at 150 +/- 3 C and 200 +/- 5 mL/min air flow rate. *5 s settling.
15、3.5.9 Seal Compatibility Shall be compatible with all current production component materials. 3.5.10 Physical Appearance and Odor Shall be clear and bright with no objectionable odor. 3.5.11 Homogeneity and Miscibility (FTM 791C, Method 3470.1) Shall remain homogeneous and when mixed with SAE refere
16、nce oils shall remain miscible. 3.6 QUALIFICATION PROCEDURE 3.6.1 Documentation Supplier must furnish to the affected Materials Engineering activity a completed and certified copy of the attached Supplement A and test reports demonstrating full compliance with all the requirements of this specificat
17、ion. The test reports must include results on both the candidate oil and the appropriate ASTM reference oils. The standard photographs of the test components are considered an essential part of the required test documentation. The oil sample code used for identification in each test document must be
18、 consistent. Any deviation in sample code uniformity must be explained and shown on the cover of each test report. All tests must be certified by a qualified and authorized representative of the test facility. 3.6.2 “Read Across“ Guidelines It is recommended that all performance tests be conducted o
19、n the final formulation, however, some exceptions may be permitted on an individual basis. Supplementary supportive data on similar formulations may be necessary in determining final approval. Minimum Energy Conserving performance of the SAE 10W-30 oil may be established on the corresponding SAE 10W
20、-40 formulation. ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-BPrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 4 of 8 3.6.3 Fleet Testing Materials which, in the opinion of the affected Materials Engineering activity, constitute a significant departure from convent
21、ional formulations, whether in base stocks, refining processes or additive packages, must be fleet tested, in addition to the requirements outlined herein. These tests must include the type(s) of service judged to be affected by the difference in formulation technology. The affected Materials Engine
22、ering activity should be consulted prior to testing. 3.6.4 Verification The affected Materials Engineering activity reserves the right to conduct verification testing. If the test results do not support the originally submitted data, the supplier must re-test the product in coordination with the aff
23、ected Materials Engineering activity. This re-test must be conducted and certified by a mutually agreed upon test facility. 3.6.5 Chemical and Physical Properties Supplier shall furnish appropriate chemical and physical properties as required on Supplement A along with the manufacturing limits that
24、apply to the material upon which approval is requested. 3.6.6 Quality Control Upon engineering approval, supplier and affected Materials Engineering activity shall establish mutually agreed upon quality control limits, to be listed on Supplement B, and will be used for ongoing product verifications
25、at mutually agreed upon frequencies. The infrared absorption spectra of the approved material shall constitute the reference standard and shall be kept on file. All samples shall produce infrared curves that correspond to the reference standard when tested under the same conditions as those specifie
26、d on the master curve. ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-BPrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 5 of 8 API SG/CD SAE 10W30 Supplement A Page 1 of 3 Oil Company_ Date_ Product Name_ Viscosity Grade_ Product Code_ Blend Plant Location(s)_ Base St
27、ocks Manufacturing Limits Nominal Base Oil Viscosity, mm2/s Cloud Point, C/ Type Vol. % 100 C 40 C Sulphur, % Pour Point, C A _ _ _ _ _ _ B _ _ _ _ _ _ C _ _ _ _ _ _ D _ _ _ _ _ _ Refinery Name & Location Process Type Crude source A _ _ _ B _ _ _ C _ _ _ D _ _ _ Note: Viscosity Sulphur Cloud Point P
28、our Point (ASTM D 445) (ASTM D 129) (ASTM D 2500) (ASTM D 97) (ASTM D 1552) (ASTM D 2622) Additives Carrier Oil Additive In Type/ Manufacturer In Additive Finished Oil Function Name Code Description Vol. % Vol. % E _ _ _ _ _ _ F _ _ _ _ _ _ G _ _ _ _ _ _ H _ _ _ _ _ _ I _ _ _ _ _ _ Signature_ Title_
29、 ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-BPrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 6 of 8 API SG/CD SAE 10W-30 Supplement A Page 2 of 3 Oil Company_ Date_ Product Name_ Product Code_ Performance Requirements Lab./Date/ Test Number Specification Test Res
30、ults Sequence IID _ Average Engine Rust _ 8.5 min _ Stuck Valve Lifters 0 _ Sequence IIIE _ Viscosity Increase 64 h,% _ 375 max _ Hours To 375% viscosity Increase 64 min _ Average Engine Sludge 9.2 min _ Average Piston Skirt Varnish 8.9 min _ Average Oil Ring Land Deposit 3.5 min _ Stuck Piston Ring
31、s Report _ Stuck Valve Lifters 0 _ Scuffed and/or Worn Cam Lobes 0 _ Valve Lifters 0 _ Cam Plus Lifter Wear Average, micrometre 30 max _ Maximum, micrometre 64 max _ Oil Consumption, L 4.62 max _ Sequence VE _ Average Engine Sludge _ 9.0 min _ Rocker Arm Cover Sludge 7.0 min _ Average Piston Skirt V
32、arnish 6.5 min _ Average Engine Varnish 5.0 min _ Oil Ring Clogging, % 15 max _ Oil Screen Clogging, % 20 max _ Stuck Compression Rings (Hot) 0 _ Cam Wear Average, micrometre 130 max _ Maximum, micrometre 380 max _ Test Method L-38 _ Bearing Weight Loss, mg _ 40 max _ Piston Skirt Varnish 9.0 min _
33、Test Method 1H2 (if available) _ Groove #1 Carbon Fill Vol., % _ 45 max _ Weighted Total Demerits 140 max _ Ring Side Clearance Loss, micrometre 13 max _ Test Method 1G2 _ Groove #1 Carbon Fill Vol., % _ 80 max _ Weighted Total Demerits 300 max _ Ring Side Clearance Loss, micrometre 13 max _ Sequenc
34、e VI _ Average Improvement (EFEI) _ 2.7% vs HR-2 _ Signature_ Title_ ENGINEERING MATERIAL SPECIFICATIONWSD-M2C904-BPrinted copies are uncontrolled Copyright 2009, Ford Global Technologies, LLC Page 7 of 8 API SG/CD SAE 10W-30 Supplement A Page 3 of 3 Oil Company_ Date_ Product Name_ Product Code_ Sp
35、ecification Test Mfg. Physical/Chemical Properties Requirements Results Limits Viscosity at 150 C (ASTM D 445), mm2/s _ _ Viscosity at 100 C (ASTM D 445), mm2/s 9.3 - 10.1 _ _ Viscosity at 40 C (ASTM D 445), mm2/s _ _ Density (ASTM D 1298), kg/L _ _ Viscosity at 20 C (SAE J300 App. A), mPa.s 3,500 m
36、ax _ _ Viscosity at 25 C (SAE J300 App. A), mPa.s _ _ Borderline Pumping Temp. (ASTM D 4684), C -25 max _ _ Pour Point (ASTM D 97), C _ _ Stable Pour Point (SAE J300 App. B), C _ _ Viscosity at -25 C (FLTM BJ 127-01), Pa.s 30 max _ _ Flash Point (ASTM D 93), C 180 min _ _ Volatility Evap. Loss, 1 h
37、at 250 C (DIN 51581), % 20 max _ _ Dist. by GC at 371 C (ASTM D 2887), % 20 max _ _ Shear Stability (ASTM D 445), mm2/s After ASTM D 3945 or CEC L-14A-78 _ _ After 10 h in “L-38“ Test _ _ Viscosity at 150 C and 1E6/s (ASTM D 4683 or CEC L-36T-84), mPa.s New Oil 2.9 min _ _ After ASTM D 3945 or CEC L
38、-14A-78 2.6 min _ _ Copper Corrosion (ASTM D 130, 3 h at 100 C) 1b max _ _ Filterability (FLTM BJ 124-01), % 50 max _ _ Foaming Sequence I, mL 10/0 max _ _ Sequence II, mL 50/0 max _ _ Sequence III, mL 10/0 max _ _ Sequence IV, mL _ _ Total Acid Number (ASTM D 664), mg KOH/g _ _ Total Base Number (ASTM D 2896), mg KOH/g _ _ Sulfated Ash (ASTM D 874), % _ _ Barium, % _ _ Nitrogen, % _ _ Boron, % _ _ Phosphorus, % _ _ Calcium, % _ _ Potassium, % _ _ Chlorine, % _ _ Sodium, % _ _ Copper, % _ _ Sulphur, % _ _ Magnesium, % _ _ Zinc, % _
