1、 ENGINEERING MATERIAL SPECIFICATION Date Action Revisions Rev. 1 2012 04 11 Revised Revisions: Title; 3.2, added 3.2.1, 3.2.2 and 3.2.2 subsections; deleted footnotes on pg 5 C. E. Richardson, FNA 2009 01 20 Activated C. E. Richardson, FNA Controlled document at www.MATS Copyright 2012, Ford Global
2、Technologies, LLC Page 1 of 10 OIL, ENGINE, SAE 10W-30, API CJ-4, INITIAL FILL WSS-M2C206-A 1. SCOPE This material specification defines the minimum acceptable performance requirements and physical/chemical properties of engine oils to be used by Ford Motor Company in its engine/vehicle manufacturin
3、g and service operations. 2. APPLICATION This specification was released originally for initial fill engine oil for diesel engines. This engine oil is used for lubrication of compression ignition engines using diesel fuel. The Section titled STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS applies onl
4、y to engine oils supplied directly to Ford Motor Company and its affiliates. 3. REQUIREMENTS 3.1 STANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Material suppliers and part producers must conform to the Companys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.2 PERFORMANCE 3.2.1 Sh
5、all meet all requirements of diesel engine test category for API CJ-4 and licensed by API. 3.2.2 Shall meet requirements of ILSAC GF-4 Standard for Passenger Car Engine Oils for following tests: 3.2.2.1 Sequence IIIG (ASTM D7320) 3.2.2.2 Sequence IVA (ASTM D6891) 3.2.2.3 Sequence VG (ASTM D6593) 3.2
6、.2.4 Sequence VIII (ASTM D6709) All required engine tests shall be conducted in accordance with the most recently approved procedures as described in ASTM Standards and the applicable ASTM Standards Research Reports and Information Letters. All tests under surveillance by ASTM must be conducted usin
7、g test equipment monitored by and calibrated to the requirements of the ASTM Test Monitoring Center. 3.3 PHYSICAL/CHEMICAL PROPERTIES 3.3.1 Physical Appearance and Odor Shall be clear and bright with no objectionable odor. 3.3.2 Contaminants Shall be free of carcinogens, toxins, metals not removed i
8、n refining or from previous use. ENGINEERING MATERIAL SPECIFICATION WSS-M2C206-A Copyright 2012, Ford Global Technologies, LLC Page 2 of 10 3.4 QUALIFICATION PROCEDURE 3.4.1 Documentation Supplier must furnish to Fuels and Lubricants Engineering a completed and certified copy of the attached Supplem
9、ent A, test reports demonstrating full compliance with all the requirements of this specification and a copy of the final ACC Monitoring Agency summary, if available. The need for ACC registration of tests will be determined by Fuels and Lubricants Engineering. The copy of the ACC Monitoring Agency
10、summary should be sent directly from Registration Systems Inc. to Fuels and Lubricants Engineering. The test reports must include results on both the candidate oil and the appropriate ASTM reference oils. The standard photographs of the test components are considered an essential part of the require
11、d test documentation. The oil sample code used for identification in each test document must be consistent. Any deviation in sample code uniformity must be explained and shown on the cover of each test report. All tests must be certified by a qualified and authorized representative of the test facil
12、ity. The supplier shall identify all the formulation changes and modifications that occurred in the test program that coincide with the tests listed in the ACC Monitoring Agency summary. Individual formulations should be listed in Supplement A, and for ACC registered tests, identified by the line it
13、em number and the formulation code. 3.4.2 “Read Across“ Guidelines It is required that all performance tests be conducted on the final formulation. However, exceptions may be permitted with supportive supplementary data on similar formulations to allow for final approval in the absence of complete t
14、esting. 3.4.3 Fleet Testing Materials which constitute a significant departure from conventional formulations, whether in base stocks, refining processes or additive packages, must be fleet tested, in addition to the requirements outlined herein. These tests must include the type(s) of service judge
15、d to be affected by the difference in formulation technology. Fuels and Lubricants Engineering should be consulted prior to testing. 3.4.4 Verification Fuels and Lubricants Engineering reserves the right to conduct verification testing. If the test results do not support the originally submitted dat
16、a, the supplier must re-test the product in coordination with Fuels and Lubricants Engineering. This re-test must be conducted and certified by a mutually agreed upon test facility. 3.4.5 Chemical and Physical Properties Supplier shall furnish appropriate chemical and physical properties as required
17、 on Supplement A along with the manufacturing limits that apply to the material as requested. ENGINEERING MATERIAL SPECIFICATION WSS-M2C206-A Copyright 2012, Ford Global Technologies, LLC Page 3 of 10 3.4.6 Performance Requirements Conformance to the engine test requirements listed in Supplement A w
18、ill be determined by using Multiple Test Acceptance Criteria (MTAC) and Tiered Limit Methods (TLM) where applicable. All data and reports from the tests used for MTAC and TLM must be provided by the supplier. Identify the engine tests on Supplement A that have been used to determine the MTAC and TLM
19、 results by the corresponding line item number on the ACC Monitoring Agency summary. Fuels and Lubricants Engineering reserves the right to use all tests when averaging in place of MTAC. 3.4.7 Quality Control Upon engineering approval supplier and Fuels and Lubricants Engineering shall establish mut
20、ually agreed upon quality control limits to be listed in Supplement B. These will be used for ongoing product verifications at mutually agreed upon frequencies. The infrared absorption spectra of the approved material shall constitute the reference standard and shall be kept on file. All samples sha
21、ll produce infrared curves that correspond to the reference standard when tested under the same conditions as those specified on the master curve. ENGINEERING MATERIAL SPECIFICATION WSS-M2C206-A Copyright 2012, Ford Global Technologies, LLC Page 4 of 10 Supplement A Page 1 of 6 Oil Company_ Date_ Pr
22、oduct Name_ Viscosity Grade_ Product Code_ Blend Plant Location(s)_ Base Stocks Manufacturing Limits Nominal Base Oil Viscosity, mm2/s Cloud Point, C/ Type Vol. % 100 C 40 C Sulfur, % Pour Point, C A _ _ _ _ _ B _ _ _ _ _ C _ _ _ _ _ D _ _ _ _ _ Refinery Name “NiL“ or Trace“ are not permissible) S _
23、 _ _ _ _ P _ _ _ _ _ Zn _ _ _ _ _ Ba _ _ _ _ _ Ca _ _ _ _ _ Mg _ _ _ _ _ Na _ _ _ _ _ N _ _ _ _ _ B _ _ _ _ _ Cu _ _ _ _ _ Cl _ _ _ _ _ Sulfated Ash _ _ _ _ _ IV.Tests Conducted _ _ _ _ _ Comments: _ _ _ _ _ Comments: _ _ _ _ _ Comments: _ _ _ _ _ Signature_ Title_ ENGINEERING MATERIAL SPECIFICATION
24、 WSS-M2C206-A Copyright 2012, Ford Global Technologies, LLC Page 9 of 10 Supplement A Page 6 of 6 Oil Company_ Date_ Product Name_ Product Code _ Test Mfg. Physical/Chemical Property Requirements Specification Results Limits Viscosity at 150 C (ASTM D 445), mm2/s _ _ Viscosity at 100 C (ASTM D 445),
25、 mm2/s 9.3 to 12.5 _ _ Viscosity at 40 C (ASTM D 445), mm2/s _ _ Density (ASTM D 1298), kg/L _ _ Viscosity at -25 C (ASTM D 5293), mPa.s 7000 max _ _ Low Temp. Pumping Viscosity at -30 C (ASTM D 4684), mPa.s 60,000 max _ _ Pour Point (ASTM D 97), oC _ _ Stable Pour Point (SAE J300 App. B), C _ _ Gel
26、ation Index (ASTM D 5133) 12.0 max _ _ Volatility Evap. Loss, 1 h at 250 C (ASTM D 5800), % 15.0 max _ _ Dist. by GC at 371 C (ASTM D 6417), % 10.0 max _ _ Shear Stability (ASTM D 445), mm2/s at 100 C After 90 passes, ASTM D 7109 9.3 min _ _ Shear Stability (ASTM D 445), mm2/s at 100 C After ASTM D
27、3945 or CEC L-14-A-93 _ _ After 10 h in “L-38 or Sequence VIII“ Test 9.3-12.5 _ _ HTHS Viscosity, mPa-sec at 150 C & 106 1/sec (ASTM D 4683 or CEC L-36T-84) New 10W-30 Oil 3.5 min _ _ After ASTM D 3945 or CEC L-14A-78 _ _ HTCBT at 135C (ASTM D6594) Copper increase 20 ppm max _ _ Lead increase 120 pp
28、m max _ _ Copper Corrosion (ASTM D 130, 3 h at 100 C) 1b max _ _ Filterability with short heating (ASTM D 6795), % 50 max _ _ Filterability with long heating (ASTM D 6794), % 50 max _ _ Foaming (ASTM D 892) Sequence I, mL 10/0 max _ _ Sequence II, mL 50/0 max _ _ Sequence III, mL 10/0 max _ _ High T
29、emperature Foaming (ASTM D 6082), mL 100/0 max _ _ Phosphorus, (ASTM D 4951), % mass 0.12% max _ _ Sulfur, (ASTM D 4951 or D 5453), % mass 0.40% max _ _ Sulfated Ash (ASTM D 874), % 1.0 max _ _ Total Acid Number (ASTM D 664), mg KOH/g _ _ Total Base Number (ASTM D 2896), mg KOH/g _ _ Elemental, mass
30、 % Barium _ _ Nitrogen _ _ Boron _ _ Potassium _ _ Calcium _ _ Sodium _ _ Chlorine _ _ Copper _ _ Zinc _ _ Magnesium _ _ Other _ _ Signature_ Title_ ENGINEERING MATERIAL SPECIFICATION WSS-M2C206-A Copyright 2012, Ford Global Technologies, LLC Page 10 of 10 Supplement B Page 1 of 1 Oil Company_ Date_
31、 Product Name_ Product Code _ Blend Plant Location _ Quality Control Certification Physical/Chemical Properties Limits Frequency Viscosity at 150 C (ASTM D 445), mm2/s _ _ Viscosity at 100 C (ASTM D 445), mm2/s _ _ Viscosity at 40 C (ASTM D 445), mm2/s _ _ Density (ASTM D 1298), kg/L _ _ Viscosity a
32、t -25 C (ASTM D 5293), mPa.s _ _ Viscosity at -30 C (ASTM D 5293), mPa.s _ _ Low Temp. Pumping Viscosity at -30 C, mPa.s _ _ (ASTM D 4684) at -35 C, mPa.s _ _ Pour Point (ASTM D 97), oC _ _ Stable Pour Point (SAE J300 App. B), C _ _ Gelation Index (ASTM D 5133) _ _ Flash Point (ASTM D 93), C _ _ Vol
33、atility Evap. Loss, 1 h at 250 C (ASTM D 5800), % _ _ Dist. by GC at 371 C (ASTM D 6417), % _ _ Shear Stability (ASTM D 445), mm2/s at 100 C After 90 passes, ASTM D 7109 _ _ Shear Stability (ASTM D 445), mm2/s at 100 C After ASTM D 3945 or CEC L-14A-78 _ _ After 10 h in “L-38“ test _ _ HTHS Viscosit
34、y, mPa-sec at 150 C & 106 1/sec (ASTM D4683 or CEC L-36T-84) New Oil _ _ After ASTM D3945 or CEC L-14A-78 _ _ HTCBT at 135C (ASTM D6594) Copper increase _ _ Lead increase _ _ Copper Corrosion (ASTM D 130, 3 h at 100 C) _ _ Filterability with short heating (ASTM D 6795), % _ _ Filterability with long
35、 heating (ASTM D 6794), % _ _ Foaming Sequence I, mL _ _ Sequence II, mL _ _ Sequence III, mL _ _ High Temperature Foaming (ASTM D 6082), mL _ _ TEOST MHT, mg _ _ Total Acid Number (ASTM D 664), mg KOH/g _ _ Total Base Number (ASTM D 2896), mg KOH/g _ _ Sulfated Ash (ASTM D 874), % _ _ Elemental, mass % Phosphorus _ _ Barium _ _ Nitrogen _ _ Boron _ _ Potassium _ _ Calcium _ _ Sodium _ _ Chlorine _ _ Sulfur _ _ Copper _ _ Zinc _ _ Magnesium _ _ Other _ _ Signature_ Title _ Fuels and Lubricants Engineering concurrence _
