1、 ENGINEERING MATERIAL SPECIFICATIONDate Action Revisions 2004 06 18 Revised Format Updated 2003 10 02 Activated M. Riley Printed copies are uncontrolled Copyright 2004, Ford Global Technologies, LLC Page 1 of 8 OIL, ENGINE, ILSAC GF-4, INITIAL FILL AND SERVICE FILL SAE 5W-30 WSS-M2C929-A SAE 5W-20 W
2、SS-M2C930-A 1. SCOPE These material specifications define the minimum acceptable performance requirements and physical/chemical properties of engine oils to be used by Ford Motor Company in its engine/vehicle manufacturing and service operations. 2. APPLICATION These specifications are released for
3、initial fill and service fill engine oils used for lubrication of spark ignition engines using gasoline. The Documentation, Performance Requirements and Quality Control subsections of the QUALIFICATION PROCEDURE apply only to engine oils supplied directly to Ford Motor Company 3. REQUIREMENTS 3.1 ST
4、ANDARD REQUIREMENTS FOR PRODUCTION MATERIALS Material suppliers and part producers must conform to the Companys Standard Requirements For Production Materials (WSS-M99P1111-A). 3.2 PERFORMANCE Shall meet all the requirements of the “ILSAC GF-4 Minimum Performance Standard for Passenger Car Engine Oi
5、ls“ plus the following: 3.2.1 ASTM Sequence VG Test Follower Pin Wear, average 30 m, max. (Cyl #8 intake and exhaust) Ring Gap Increase, average 225 m, max (Cyl #1 and #8) The following photographs of the VG test engine are required: Rocker arm cover and camshaft baffle Oil pan and baffle Oil pick-u
6、p screen Cylinder block underside Cylinder head valve decks Cylinder block front Timing chain cover Average and worst piston skirts, thrust sides Rear seal housing ENGINEERING MATERIAL SPECIFICATIONWSS-M2C929-AWSS-M2C930-APrinted copies are uncontrolled Copyright 2004, Ford Global Technologies, LLC
7、Page 2 of 8 All required engine tests shall be conducted in accordance with the most recently approved procedures as described in ASTM Standards and the applicable ASTM Standards Research Reports and Information Letters. All tests under surveillance by ASTM must be conducted using test equipment mon
8、itored by and calibrated to the requirements of the ASTM Test Monitoring Center. 3.3 PHYSICAL/CHEMICAL PROPERTIES 3.3.1 Copper Corrosion 1b max (ASTM D 130 or ISO 2160, 3 h at 100 C) (Dark Orange) 3.3.2 High Temperature Deposits, mg 30 max (TEOST MHT-4) 3.3.3 Physical Appearance and Odor Shall be cl
9、ear and bright with no objectionable odor. 3.3.4 Contaminants Shall be free of carcinogens, toxins, metals not removed in refining or from previous use. 3.4 QUALIFICATION PROCEDURE 3.4.1 Documentation Supplier must furnish to Fuels and Lubricants Engineering a completed and certified copy of the att
10、ached Supplement A, test reports demonstrating full compliance with all the requirements of this specification and a copy of the final ACC Monitoring Agency summary, if available. The need for ACC registration of tests will be determined by Fuels and Lubricants Engineering. The copy of the ACC Monit
11、oring Agency summary should be sent directly from Registration Systems Inc. to Fuels and Lubricants Engineering. The test reports must include results on both the candidate oil and the appropriate ASTM reference oils. The standard photographs of the test components are considered an essential part o
12、f the required test documentation. The oil sample code used for identification in each test document must be consistent. Any deviation in sample code uniformity must be explained and shown on the cover of each test report. All tests must be certified by a qualified and authorized representative of t
13、he test facility. The supplier shall identify all the formulation changes and modifications that occurred in the test program that coincide with the tests listed in the ACC Monitoring Agency summary. Individual formulations should be listed in Supplement A, and for ACC registered tests, identified b
14、y the line item number and the formulation code. 3.4.2 “Read Across“ Guidelines It is required that all performance tests be conducted on the final formulation. However, exceptions may be permitted with supportive supplementary data on similar formulations to allow for final approval in the absence
15、of complete testing. 3.4.3 Fleet Testing Materials which constitute a significant departure from conventional formulations, whether in base stocks, refining processes or additive packages, must be fleet tested, in addition to the requirements outlined herein. These tests must include the type(s) of
16、service judged to be affected by the difference in formulation technology. Fuels and Lubricants Engineering should be consulted prior to testing. ENGINEERING MATERIAL SPECIFICATIONWSS-M2C929-AWSS-M2C930-APrinted copies are uncontrolled Copyright 2004, Ford Global Technologies, LLC Page 3 of 8 3.4.4
17、Verification Fuels and Lubricants Engineering reserves the right to conduct verification testing. If the test results do not support the originally submitted data, the supplier must re-test the product in coordination with Fuels and Lubricants Engineering. This re-test must be conducted and certifie
18、d by a mutually agreed upon test facility. 3.4.5 Chemical and Physical Properties Supplier shall furnish appropriate chemical and physical properties as required on Supplement A along with the manufacturing limits that apply to the material as requested. 3.4.6 Performance Requirements Conformance to
19、 the engine test requirements listed in Supplement A will be determined by using Multiple Test Acceptance Criteria (MTAC). All data and reports from the tests used for MTAC must be provided by the supplier. Identify the engine tests on Supplement A that have been used to determine the MTAC results b
20、y the corresponding line item number on the ACC Monitoring Agency summary. Fuels and Lubricants Engineering reserves the right to use all tests when averaging in place of MTAC. 3.4.7 Quality Control Upon engineering approval supplier and Fuels and Lubricants Engineering shall establish mutually agre
21、ed upon quality control limits to be listed in Supplement B. These will be used for ongoing product verifications at mutually agreed upon frequencies. The infrared absorption spectra of the approved material shall constitute the reference standard and shall be kept on file. All samples shall produce
22、 infrared curves that correspond to the reference standard when tested under the same conditions as those specified on the master curve. ENGINEERING MATERIAL SPECIFICATIONWSS-M2C929-AWSS-M2C930-APrinted copies are uncontrolled Copyright 2004, Ford Global Technologies, LLC Page 4 of 8 Supplement A Pa
23、ge 1 of 4 Oil Company_ Date_ Product Name_ Viscosity Grade_ Product Code_ Blend Plant Location(s)_ Base Stocks Manufacturing Limits Nominal Base Oil Viscosity, mm2/s Cloud Point, C/ Type Vol. % 100 C 40 C Sulfur, % Pour Point, C A _ _ _ _ _ B _ _ _ _ _ C _ _ _ _ _ D _ _ _ _ _ Refinery Name “NiL“ or
24、Trace“ are not permissible) S _ _ _ _ _ P _ _ _ _ _ Zn _ _ _ _ _ Ba _ _ _ _ _ Ca _ _ _ _ _ Mg _ _ _ _ _ Na _ _ _ _ _ N _ _ _ _ _ B _ _ _ _ _ Cu _ _ _ _ _ Cl _ _ _ _ _ Sulfated Ash _ _ _ _ _ IV.Tests Conducted _ _ _ _ _ Comments: _ _ _ _ _ Comments: _ _ _ _ _ Comments: _ _ _ _ _ Signature_ Title_ ENG
25、INEERING MATERIAL SPECIFICATIONWSS-M2C929-AWSS-M2C930-APrinted copies are uncontrolled Copyright 2004, Ford Global Technologies, LLC Page 7 of 8 Supplement A Page 4 of 4 Oil Company_ Date_ Product Name_ Product Code_ Test Mfg. Physical/Chemical Property Requirements Specification Results Limits Visc
26、osity at 150 C (ASTM D 445), mm2/s _ _ Viscosity at 100 C (ASTM D 445), mm2/s, 5W-20 5.6 - 9.3 _ _ Viscosity at 100 C (ASTM D 445), mm2/s, 5W-30 9.3 - 12.5 _ _ Viscosity at 40 C (ASTM D 445), mm2/s _ _ Density (ASTM D 1298), kg/L _ _ Dry vapor pressure equivalence (D 4953 or D 5191), kPa _ _ Viscosi
27、ty at -25 C (ASTM D 5293), mPa.s 3,500 max _ _ Viscosity at -30 C (ASTM D 5293), mPa.s _ _ Low Temp. Pumping Viscosity at -30 C, mPa.s 30,000 max _ _ (ASTM D 4684) at -35 C, mPa.s 60,000 max _ _ Pour Point (ASTM D 97), oC _ _ Stable Pour Point (SAE J300 App. B), C _ _ Gelation Index (ASTM D 5133) 12
28、.0 max _ _ Volatility Evap. Loss, 1 h at 250 C (ASTM D 5800), % 15.0 max _ _ Dist. by GC at 371 C (ASTM D 5480), % 9.0 max _ _ Dist. by GC at 371 C (ASTM D 6417), % 10.0 max _ _ Shear Stability (ASTM D 445), mm2/s at 100 C After ASTM D 3945 or CEC L-14A-78 _ _ After 10 hr in “L-38“ Test 5W-20 5.6 -
29、9.3 _ _ After 10 hr in “L-38“ Test 5W-30 9.3 - 12.5 _ _ HTHS Viscosity, mPa-sec at 150 C & 1061/sec (ASTM D 4683 or CEC L-36T-84) New 5W-20 Oil 2.6 min _ _ New 5W-30 Oil 2.9 min _ _ After ASTM D 3945 or CEC L-14A-78 _ _ Copper Corrosion (ASTM D 130, 3 h at 100 C) 1b max _ _ Filterability with short
30、heating (ASTM D 6795), % 50 max _ _ Filterability with long heating (ASTM D 6794), % 50 max _ _ Foaming (ASTM D 892) Sequence I, mL 10/0 max _ _ Sequence II, mL 50/0 max _ _ Sequence III, mL 10/0 max _ _ High Temperature Foaming (ASTM D 6082), mL 100/0 max _ _ Phosphorus, (ASTM D 4951), % mass 0.08%
31、 max _ _ Sulfur, (ASTM D 4951 or D 5453), % mass 0.50% max _ _ Total Acid Number (ASTM D 664), mg KOH/g _ _ Total Base Number (ASTM D 2896), mg KOH/g _ _ Sulfated Ash (ASTM D 874), % _ _ Elemental, mass % Barium _ _ Nitrogen _ _ Boron _ _ Potassium _ _ Calcium _ _ Sodium _ _ Chlorine _ _ Copper _ _
32、Zinc _ _ Magnesium _ _ Other _ _ Signature_ Title_ ENGINEERING MATERIAL SPECIFICATIONWSS-M2C929-AWSS-M2C930-APrinted copies are uncontrolled Copyright 2004, Ford Global Technologies, LLC Page 8 of 8 Supplement B Page 1 of 1 Oil Company_ Date_ Product Name_ Product Code_ Blend Plant Location_ Quality
33、 Control Certification Physical/Chemical Properties Limits Frequency Viscosity at 150 C (ASTM D 445), mm2/s _ _ Viscosity at 100 C (ASTM D 445), mm2/s _ _ Viscosity at 40 C (ASTM D 445), mm2/s _ _ Density (ASTM D 1298), kg/L _ _ Viscosity at -25 C (ASTM D 5293), mPa.s _ _ Viscosity at -30 C (ASTM D
34、5293), mPa.s _ _ Low Temp. Pumping Viscosity at -30 C, mPa.s _ _ (ASTM D 4684) at -35 C, mPa.s _ _ Pour Point (ASTM D 97), oC _ _ Stable Pour Point (SAE J300 App. B), C _ _ Gelation Index (ASTM D 5133) _ _ Flash Point (ASTM D 93), C _ _ Volatility Evap. Loss, 1 h at 250 C (ASTM D 5800), % _ _ Dist.
35、by GC at 371 C (ASTM D 5480), % _ _ Dist. by GC at 371 C (ASTM D 6417), % _ _ Shear Stability (ASTM D 445), mm2/s at 100 C After ASTM D 3945 or CEC L-14A-78 _ _ After 10 h in “L-38“ test _ _ HTHS Viscosity, mPa-sec at 150 C & 1061/sec (ASTM D4683 or CEC L-36T-84) New Oil _ _ After ASTM D3945 or CEC
36、L-14A-78 _ _ Copper Corrosion (ASTM D 130, 3 h at 100 C) _ _ Filterability with short heating (ASTM D 6795), % _ _ Filterability with long heating (ASTM D 6794), % _ _ Foaming Sequence I, mL _ _ Sequence II, mL _ _ Sequence III, mL _ _ High Temperature Foaming (ASTM D 6082), mL _ _ TEOST MHT, mg _ _
37、 Total Acid Number (ASTM D 664), mg KOH/g _ _ Total Base Number (ASTM D 2896), mg KOH/g _ _ Sulfated Ash (ASTM D 874), % _ _ Elemental, mass % Phosphorus _ _ Barium _ _ Nitrogen _ _ Boron _ _ Potassium _ _ Calcium _ _ Sodium _ _ Chlorine _ _ Sulfur _ _ Copper _ _ Zinc _ _ Magnesium _ _ Other _ _ Signature_ Title_ Fuels and Lubricants Engineering concur
