1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS D 1655 X KS D 1655: 2008 2008 6 13 http:/www.kats.go.krKS D 1655: 2008 : () ( ) () ( ) : (http:/www.standard.go.kr) : :1975 12 3 :2008 6 13 2008-0276 : : ( 02-509-7274) (http:/www.kats.go.kr). 10 5 , . KS D 1655: 2008 X Method for X-ray fluorescence spect
2、rometric analysis of iron and steel 1 , , , , , , , , , , , . 2 . . KS D 1654, X KS M 0017, X 3 3.1 1 , . 1 . 1 % % 0.004 4.5 0.02 0.2 0.003 15.0 0.002 7.0 0.001 0.3 0.004 1.1 0.001 0.5 0.002 0.35 0.004 7.0 0.003 0.4 0.02 20.0 0.002 0.15 0.008 85.0 0.003 0.1 0.003 40.0 0.001 0.1 0.002 13.0 0.002 0.1
3、 0.005 22.0 0.002 0.1 0.003 5.5 0.002 0.2 0.004 40.0 0.004 0.1 0.002 6.0 0.005 0.3 0.005 12.0 0.003 0.2 0.002 0.1 KS D 1655: 2008 2 3.2 KS M 0017 3.( ) KS D 1654 . 3.3 KS M 0017 7.( ) KS D 1654 . 3.4 2 . 2 nm nm Si K1, 20.712 6 Ta L10.152 2 Mn K1, 20.210 3 Ta L10.132 7 P K1, 20.615 8 Zr K1, 20.078 7
4、3 S K1, 20.537 3 Pb L10.117 5 Cu K1, 20.154 2 Pb L10.098 29 Fe K1, 20.193 7 Sn K1, 20.049 21 Fe K1, 30.175 7 Sn L10.360 0 Ni K1, 20.165 9 Sn L10.338 5 Cr K1, 20.229 1 Zn K1, 20.143 6 Mo K1, 20.071 07 Bi L10.114 4 WL10.147 6 Sb K1, 20.047 18 V K1, 20.250 5 Sb L10.343 9 Co K1, 20.179 0 As K1, 20.117 7
5、 Co K1, 30.162 1 As K1, 30.105 7 Ti K1, 20.275 0 Se K1, 20.110 6 Al K1, 20.834 0 Te K1, 20.045 28 Ca K1, 20.335 9 Te L10.328 9 Mg K1, 20.989 0 Ce L10.256 1 Nb K1, 20.074 76 Ce L10.235 6 La L10.266 6 La L10.245 9 3.5 a) , . b) ( ) 1), 2) 5) 11) . 2) a) , . KS D 1655: 2008 3 , .6) ( ) , 7), .8)3)4)5)b
6、) . . , . 3) , , . , . 4) . . 5) (target) . , , . 6) K K . CKaIKIK += )CrMn(Mn% IMnK : MnK ICrK : CrK K, a, C : K, a, C , ( 20 ) , . K K . 7) . 8) . a) , . b) , , , . , . (i) 1 ( ) , ( ) K , bKIaKIaKIa +=KNiNiMnMnCrCrCr% IMK : M K aM: M b : aM b , K IMK , . (ii) 2 ( ) . ijijiiDMaIM += )1(% Mi: i Ii:
7、 i i (Fe-i ) KS D 1655: 2008 4 aij: i j Mj: j . , i j , j i, j jFe Di : i (background) aij . (iii) 3 ( , ) . jfiifijiiiiMABIIAMM )()(1+=+ Mi: i (%) Mi: i Ii: i Ii: i fij: i j . , i j fii: i i Mj : j (iv) 4 ( ) 1 2 . (v) (drift) , (overlapping), (background), , . X 135513 7017 (02)60094114 (02)600948878 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS D 1655: 2008KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Method for X-ray fluorescence spectrometric analysis of iron and steel ICS 77.140.80