KS D 1673-2007 Methods for inductively coupled plasma emission spectrochemical analysis of steel《钢的电感耦合等离子发射分光光谱测定分析法》.pdf

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1、 KS D 1673KSKSKSKSSKSKSKS KSKSKS SKSKS KSKS SKS KS KS D 1673: 2007 2007 11 30 http:/www.kats.go.krKS D 1673: 2007 : () ( ) () ( ) : (http:/www.standard.go.kr) : :1992 12 31 :2007 11 30 2007-1080 : : ( 02-509-7274) (http:/www.kats.go.kr ). 7 5 , . KS D 1673: 2007 Methods for inductively coupled plasm

2、a emission spectrochemical analysis of steel 1 92 %(m/m) . 1 . , 1 . ( ) 1.0 % ( 0.10 % ) . 1 % 0.01 0.60 0.01 2.00 0.003 0.10 0.01 4.00 0.01 3.00 0.01 1.20 0.01 0.50 0.002 0.50 0.003 0.20 0.001 0.30 0.004 0.10 2 . . KS A ISO 5725( ), ( ) KS D 1801, KS M 0028, 3 KS D 1673: 2007 2 KS D 1801 KS M 0028

3、 . 4 ( Y .) . , . 4.1 , . . , Y (Y) ICP . 4.2 a) (11) b) (2100) c) (11) d) ( 1, 1, 2) e) . f) g) (1 mg Y/mL) (99.9 % ) 1.269 9 g (1 1) 50 mL , (1 000 mL) . h) (100 g/L) (100 g/L) i) (250 g Si/mL) 1 000 1 , ( , ) 0.534 8 g ( ) 2.5 g . , 100 mL (200 mL) . , (5 B) (10 g/L) . (1 000 mL) . . j) (1 mg Mn/

4、mL) (99.9 % ) 1.000 g (200 mL) , (1 1) 30 mL . , (1 000 mL) . k) (100 g P/mL) 110 1 (KH2PO4) 0.439 3 g (200 mL) 100 mL . (1 000 mL) . l) (1 mg Ni/mL) (99.9 % ) 1.000 g (200 mL) (1 1) 30 mL . , (1 000 mL) . m) (1 mg Cr/mL) (99.9 % ) 1.000 g (200 mL) (1 1) 30 mL . (1 000 mL) . KS D 1673: 2007 3 n) (1

5、mg Mo/mL) (99.9 % ) 1.000 g (200 mL) (1 1) 30 mL . , (1 000 mL) . o) (500 g Cu/mL) (99.9 % ) 0.500 g (200 mL) (1 1) 30 mL . , (1 000 mL) . p) (500 g V/mL) (99.9 % ) 0.500 g (200 mL) 30 mL . 20 mL , , (1 000 mL) . q) (200 g Co/mL) (99.9 % ) 0.200 g (200 mL) (1 1) 30 mL . , (1 000 mL) . r) (250 g Ti/m

6、L) (99.9 % ) 0.100 g (200 mL) , (1 1) 80 mL . , (1 1) (100 mL) (1 1) (1 1) (1.00 mg Ti/mL) . (1 1) 4 . s) (100 g Al/mL) (99.9 % ) 0.100 g (200 mL) (1 1) 30 mL . , (1 000 mL) . 4.3 4.3.1 ICP ( , , ) . a) b) . a) 0.500 g (200 mL) 2 .1) 4.4.1 b) f) . 4.4.2 4.9 10 ( ) 4 . , 10 2 . b) 0.500 g (200 mL) 3

7、.1) 4.4.1 b) f) . 4.4.2 4.9 10 ( ) 4 . , 10 3 . 4.3.2 1) . KS D 1673: 2007 4 4.3.1 . . 2 g % 50(0.010) 50(0.010) 25(0.005) 50(0.010) 50(0.010) 50(0.010) 50(0.010) 10(0.002) 15(0.003) 10(0.002) 25(0.005) 0.001 5 0.001 0 0.001 0 0.001 0 0.001 0 0.001 5 0.001 0 0.000 3 0.000 3 0.000 3 0.000 3 ( ) % . 3

8、 mg % 3.0(0.60) 10.0(2.00) 0.5(0.10) 20.0(4.00) 15.0(3.00) 6.0(1.20) 2.5(0.50) 2.5(0.50) 1.0(0.20) 1.5(0.30) 0.5(0.10) 0.006 0.020 0.002 0.040 0.030 0.012 0.005 0.005 0.002 0.003 0.002 ( ) % . 4.4 4.4.1 . a) 0.50 g (200 mL) . b) 25 mL , . c) (5 C) (2 100) KS D 1673: 2007 5 (III) . (200 mL) . d) , .

9、1.0 g . e) , (1 1) 5 mL 2) c) .3)f) 10 mL 4) (100 mL) . 4.4.2 . a) 4.4.1 f) ICP . .5)b) a) (Y , ) . 1) 1.1) 1.1.1) , 1.1.2) 1.1.3) , 1.1.4) , 1.1.5) 1.2) 1.2.1) 1.2.2) 1.2.3) 1.2.4) 2) 2.1) 2.1.1) , 2.1.2) 2.1.3) , 2.1.4) , 2.1.5) 2.2) 2.2.1) 2.2.2) , 2.2.3) 2) 10 mL . 3) 4.4.1 d) e) . . 4) , . 5) .

10、 KS D 1673: 2007 6 4.5 , 0.500 g . 4.4.1 b) 4.4.2 b) . 4.6 6) 0.500 g (200 mL) 4 7) 4.4.1 b) 4.4.2 b) 8) . 4 (mL) 4.2 i) . 4.2 j) . 4.2 k) . 4.2 l) . 4.2 m) . 4.2 n) . 4.2 o) . 4.2 p) . 4.2 q) . 4.2 r) . 4.2 s) . 0, 0, 0, 0, 0, 0, 0, 0, 0, 0, 0, 2.0,2.0,1.0,1.0,1.0,1.0,1.0,1.0,1.0,1.0,1.0,4.0,4.0,2.

11、0,3.0,2.0,2.0,2.0,2.0,2.0,2.0,2.0,6.0,6.0,3.0,5.0,3.0,3.0,3.0,3.0,3.0,3.0,3.0,8.0, 8.0, 4.0, 10.0, 5.0, 4.0, 4.0, 4.0, 4.0, 4.0, 4.0, 10.0, 10.0 5.0 15.0, 10.0, 5.0, 5.0 5.0 5.0 5.0, 5.0 12.0 20.0 15.0 6.0 6.0 4.7 , , , . . 4.8 6) . 3 . 4.4 . 7) ( ) 4.4.1 f) . 8) . KS D 1673: 2007 7 ( 1 % %) . 4.9 4

12、.4.2 b) 4.5 4.6 4.7 .9)=jjWlSAAX 10021 X : (%) A1 : (g) A2 : (g)10)S : (g) lj : j Wj: j (%) 4.10 5 . 5 D2 KS A ISO 5725 6 4 . 9) . ICP . 10) . KS D 1673: 2007 8 5 % D20.007 1(Si ) 0.001 2 Y D20.008 0(Si ) 0.002 4 D20.008 9(Si ) 0.001 4 D20.013 6(Si ) 0.001 4 D20.002 7(Mn ) 0.001 1 Y D20.009 3(Mn ) 0

13、.002 9 D20.004 7(Mn ) 0.001 4 D20.012 5(Mn ) 0.002 0 D20.029 9(P ) 0.000 3 Y D20.003 8(P ) 0.000 9 D20.003 0(Ni ) 0.000 5 Y D20.009 9(Ni ) 0.002 3 D20.005 2(Cr ) 0.000 3 Y D20.007 9(Cr ) 0.002 4 D20.007 1(Cr ) 0.001 1 D20.018 8(Cr ) 0.000 6 D20.006 7(Mo ) 0.000 2 Y D20.018 4(Mo ) 0.001 0 D20.006 9(M

14、o ) 0.001 1 D20.022 0(Mo ) 0.002 0 D20.006 9(Cu ) 0.000 1 Y D20.016 0(Cu ) 0.000 6 D20.011 9(Cu ) 0.000 1 D20.018 5(Cu ) 0.000 3 D20.006 7(V ) 0.000 1 Y D20.007 1(V ) 0.000 9 D20.009 4(V ) 0.000 1 D20.014 5(V ) 0.000 3 D20.005 3(Co ) 0.000 4 Y D20.015 0(Co ) 0.000 6 D20.015 3(Co ) 0.000 3 D20.030 3(

15、Co ) 0.000 7 D20.002 1(Ti ) 0.000 2 Y D20.011 5(Ti ) 0.000 3 D20.006 7(Ti ) 0.000 2 D20.020 1(Ti ) 0.000 1 D2 0.001 9(Al ) 0.000 7 Y D20.008 4(Al ) 0.000 7 D20.006 2(Al ) 0.000 5 D20.021 4(Al ) 0.000 7 135513 7017 (02)60094114 (02)600948878 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS D 1673: 2007KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Methods for inductively coupled plasma emission spectrochemical analysis of steel ICS 71.040.40

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