KS D ISO 5194-2001 Aluminium alloys-Determination of zinc-Flame atomic absorption spectrometric method《铝和铝合金 锌含量的测定 火焰原子吸收光谱测定法》.pdf

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1、 KSKSKSKS SKSKSKS KSKSKS SKSKS KSKS SKS KS 2001 12 31 KS D ISO 5194 KS D ISO 5194: 2001 (2006 )(ISO 5194: 1981, IDT) ICS 77.120.10 KS D ISO 5194: 2001(2006 )(ISO 5194: 1981, IDT)Aluminium alloys Determination of zinc Flame atomic absorption spectrometric method 1981 ISO 5194(Aluminium alloys Determi

2、nation of zinc Flame atomic absorption spectrometric method) . 1. . 0.002 6 %(m/m) . 2. , ( 213.9 nm). 3. . 3.1 ( 99.99 %) . 3.2 , 6 mol/L 20 %(m/m), 1.10 g/mL 12 M ( 38 %, 1.19 g/mL) 500 mL 500 mL . 3.3 30 %(m/m) 3.4 , 9 mol/L 58 %(m/m) 96 % 18 mol/L ( 1.84 g/mL) 50 mL 40 mL . 100 mL . 3.5 1.13 g/m

3、L, 40 %(m/m) 3.6 , 15 mol/L 1.4 g/mL, 68 %(m/m) 50 g 100 mL . 3.7 , 20 g Al/L (3.1) 20 g 0.01 g 1 000 mL , (3.2) 600 mL . . . (3.3) . 1 000 mL . 3.8 , 2 g Al/L (3.7) 50 mL 500 mL (3.2) 270 mL . 3.9 , 1 g Zn/L ( 99.99 % ) 1 g 0.001 g 400 mL (3.2) 50 mL . 1 000 mL . D ISO 5194:2001 2 1 mL 1 mg . 3.10

4、, 0.05 g Zn/L (3.9) 50 mL 1 000 mL . 1 mL 0.05 mg . 3.11 , 0.01 mg Zn/L (3.9) 10 mL 1 000 mL . . 1 mL 0.01 mg . 4. 4.1 0.05 mL 4.2 / . 4.3 4.4 4.5 (ZnHCL) 5. 5.1 5.2 1 mm 6. 6.1 (5.2) 1 g 0.001 g . 6.2 6.2.1 6.2.1.1 0.002 0.03 %(m/m) 9 100 mL (4.1) 1 (3.10 3.11) . (3.7) 50 mL . 1 (3.11) mL mg %(m/m)

5、 0*1.0 3.0 5.0 10.0 (3.10) mL 0 0.01 0.03 0.05 0.10 0 0.001 0.003 0.005 0.010 3.0 4.0 5.0 6.0 0.15 0.20 0.25 0.30 0.015 0.020 0.025 0.030 * D ISO 5194:2001 3 6.2.1.2 0.02 0.3 %(m/m) 9 100 mL (4.1) 2 (3.10 3.11) . (3.7) 5 mL . 2 (3.11) mL mg %(m/m) 0*1.0 3.0 5.0 10.0 (3.10) mL 0 0.01 0.03 0.05 0.10 0

6、 0.01 0.03 0.05 0.10 3.0 4.0 5.0 6.0 0.15 0.20 0.25 0.30 0.15 0.20 0.25 0.30 * 6.2.1.3 0.2 3 %(m/m) 9 100 mL (4.1) 3 (3.10 3.11) . (3.7) 5 mL . 3 (3.11) mL mg %(m/m) 0*1.0 3.0 5.0 10.0 (3.10) mL 0 0.01 0.03 0.05 0.10 0 0.10 0.30 0.50 1.00 3.0 4.0 5.0 6.0 0.15 0.20 0.25 0.30 1.50 2.00 2.50 3.00 * 6.2

7、.1.4 3 6 %(m/m) 6 100 mL (4.1) 4 (3.10 3.11) . (3.8) 2.5 mL . D ISO 5194:2001 4 4 (3.10) mL mg %(m/m) 0*2.0 3.0 4.0 5.0 6.0 0 0.10 0.15 0.20 0.25 0.30 0 2.0 3.0 4.0 5.0 6.0 * 6.2.2 (4.2) (4.5) . . 213.9 nm . . (6.2.1.1, 6.2.1.2, 6.2.1.3, 6.2.1.4) . . . 6.2.3 100 mL (mg) . 6.3 6.3.1 (6.1) 250 mL , 30

8、 40 mL . (3.2) 30 mL . (3.3) , 10 . . . . 550 (3.4) 2 mL (3.5) 5 mL . ( 1 mL). , 700 . (3.2) . . . 6.3.1.1 0.002 0.03 %(m/m) (6.3.1) 100 mL . 6.2.1.1 . 6.3.1.2 0.02 0.3 %(m/m) (6.3.1) 1 000 mL . 6.2.1.2 . 6.3.1.3 0.2 3 %(m/m) (6.3.1) 500 mL . 50 mL 1 000 mL (3.2) 27 mL . 6.2.1.3 . 6.3.1.4 3 6 %(m/m)

9、 D ISO 5194:2001 5 (6.3.1) 1 000 mL . 50 mL 1 000 mL , (3.2) 13.5 mL . 6.2.1.4 . 6.3.2 . (3.1) 1 g 0.001 g . 6.3.3 (6.3.1.1, 6.3.1.2, 6.3.1.3, 6.3.1.4) (6.3.2), (6.2.1.1, 6.2.1.2, 6.2.1.3, 6.2.1.4) 6.2.2 . . 7. (Zn) . 01210)(mRmm m0: (g) m1: (mg) m2: ( ) (mg) R: ( , 6.3.1.1 R 1, 6.3.1.2 R 10, 6.3.1.

10、3 R100, 6.3.1.4 R 200 .) 8. . a) b) c) d) e) : : 2001 12 31 : 2006 10 2 2006-0451 : : ( ) ( 02 509 72547) . 7 5 , . 701-7 6009-4567, 6009-48878 http:/ KS D ISO 5194: 2001 (ISO 5194: 1981, IDT) Aluminium alloysDetermination ofzincFlame atomic absorptionspectrometric methodICS 77.120.10 : : 2006 10 2 : 2001 12 31 2006-0451 : : ( ) KSKSKSSKSKS KSKS SKS KSKS SKSKS KSKSKS

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