1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS H ISO 3520 , KS H ISO 3520: 2008 2008 3 26 http:/www.kats.go.krKS H ISO 3520: 2008 : () ( ) F&B () ( ) : (http:/www.standard.go.kr) : :2008 3 26 2008-0126 : : ( 02-509-7266) (http:/www.kats.go.kr). 10 5 , . KS H ISO 3520: 2008 i .1 1 1 2 1 3 1 4 2 4.1 .2
2、4.2 .2 4.3 .2 4.4 (20 , ) 2 4.5 (20 )2 4.6 (20 ) 2 4.7 2 4.8 (20 ) 2 4.9 .2 4.10 2 4.11 (Bergaptene) 3 4.12 CD(Conjugated Diene) 3 4.13 3 4.14 .3 5 3 6 .4 7 4 7.1 (20 , ) 4 7.2 (20 )4 7.3 (20 ) 4 7.4 4 7.5 (20 ) 4 7.6 .4 7.7 .4 7.8 (Bergaptene) 4 7.9 CD(Conjugated Diene) 4 7.10 5 8 , , , 5 A( ) 6 B(
3、 ) .8 B.1 .8 B.2 8 2020d2020d KS H ISO 3520: 2008 , Oil of bergamot Citrus aurantium L. subsp. bergamia(Wight et Arnott) Engler, Italian type 1998 2 ISO 3520, Oil of bergamot Citrus aurantium L. subsp. bergamia (Wight et Arnott) Engler, Italian type , . 1 . 2 . . ( ) . KS H ISO 210, , KS H ISO 211,
4、KS H ISO 212, KS H ISO 279, 20 KS H ISO 280, KS H ISO 356, KS H ISO 592, KS H ISO 875, KS H ISO 1242, KS H ISO 4715, KS H ISO 11024 1, 1: KS H ISO 11024 2, 2: ISO 4735, Oils of citrus Determination of CD value by ultraviolet spectrophotometric analysis ISO 7358, Oils of bergamot, lemon, citron and l
5、ime, full or partially reduced in bergaptene Determination of bergaptene content by high-performance liquid chromatography 3 KS H ISO 3520: 2008 2 . 3.1 , (Rutaceae) Citrus aurantium L. subsp. bergamia (Wight et Arnott) Engler 4 4.1 . 4.2 4.3 4.4 (20 , 2020d ) : 0.876 : 0.883 4.5 (20 ) : 1.465 0 : 1
6、.470 0 4.6 (20 ) 15 32 4.7 : 4.50 % : 6.40 % 4.8 (20 ) 20 1 (85 % ) 1 . 4.9 : 2 4.10 KS H ISO 3520: 2008 3 : 86 : 129 4.11 (Bergaptene) : 0.18 % : 0.38 % 4.12 CD(Conjugated Diene) : 0.760 : 1.180 0.1 g/100 mL (95 % ) 4.13 . 1 . 1 . . 1 % % - (-Pinene) 5.5 9.5 (Limonene) 30 45 - (-Terpinene) 6 10 (Li
7、nalol) 3 15 (Linalyl acetate) 22 36 (Geranial) 0.25 0.50 - (-Bisabolene) 0.30 0.55 A , . 4.14 B . 5 KS H ISO 212 : 25 mL . . KS H ISO 3520: 2008 4 . . 6 KS H ISO 356 7 7.1 (20 , 2020d ) KS H ISO 279 7.2 (20 ) KS H ISO 280 7.3 (20 ) KS H ISO 592 7.4 KS H ISO 4715 : 5 g : 6 7.5 (20 ) KS H ISO 875 7.6
8、KS H ISO 1242 7.7 KS H ISO 709 : 30 7.8 (Bergaptene) KS H ISO 7358 7.9 CD(Conjugated Diene) KS H ISO 4735 KS H ISO 3520: 2008 5 point B: 278 nm (point D): 312 nm point A: 365 nm 7.10 KS H ISO 11024 1 KS H ISO 11024 2 8 , , , KS H ISO 210 KS H ISO 211 KS H ISO 3520: 2008 6 A ( ) 1 - 2 + - 3 4 5 - 6 7
9、 8 9 10 11 12 - : , 25 m, 0.32 mm : 0.4 0.45 m : SE 52 : 8 60 , 3 /min 100 , 2.5 /min 130 , 3 /min 160 : 280 : 280 : : : 1 L : 1/150 A.1 KS H ISO 3520: 2008 7 1 - 2 3 - 4 5 6 7 - 8 - 9 10 11 12 - 13 - 14 15 + + - 16 : , 50 m, 0.22 mm : 0.2 m : 20 000 : 5 65 , 2 /min 155 , 3 /min 200 : 230 : 250 : :
10、: 0.2 L : 0.40 m/s A.2 KS H ISO 3520: 2008 8 B ( ) B.1 , , , . (KS H ISO 110181) ) . , . , . . , , . . KS H ISO 110181) B.2 59 “ (Setaflash)” . 65 “ (Luchaire)” . 1) KS H ISO 11018: 2006, , 135513 7017 (02)60094114 (02)600948878 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS H ISO 3520: 2008KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Oil of bergamot Citrus aurantium L.subsp. bergamia(Wight et Arnott) Engler, Italian type ICS 71.100.60