1、 KS I 3203 KSKSKSKS SKSKSKS KSKSKS SKSKS KSKS SKS KS KS I 3203 :2007 (2012 ) 2007 6 29 http:/www.kats.go.krKS I 3203:2007 : ( ) ( ) ( ) : (http:/www.standard.go.kr) : : 1997 6 19 : 2007 6 29 :2012 12 31 : 20120844 : ( 02-509-7270) (http:/www.kats.go.kr). 10 5 , . KS I 3203:2007 1 1 2 1 3 2 3.1 .2 3.
2、2 .2 3.3 .2 3.4 2 3.5 .2 3.6 2 3.7 .2 3.8 .3 3.9 .3 3.10 3 3.11 ( , lCP , lCP , ) .3 3.12 3 3.13 3 4 4 4.1 4 4.2 .4 4.3 4 5 (Na).4 5.1 4 5.2 ICP .6 5.3 8 6 (K).9 6.1 9 6.2 10 7 (Ca) 11 7.1 11 7.2 ICP .12 8 (Mg).14 8.1 14 8.2 ICP .15 8.3 ICP .16 9 (Cu) 17 9.1 17 9.2 ICP .18 9.3 ICP .19 10 (Zn).20 10.
3、1 20 10.2 ICP .21 10.3 ICP .22 11 (Pb) 23 i KS I 3203:2007 ii 11.1 23 11.2 ICP .25 12 (Cd).26 12.1 26 12.2 ICP .27 12.3 ICP .28 13 (Ni) .29 13.1 29 13.2 ICP .30 14 (Co).31 14.1 31 14.2 ICP .32 15 (Mn)33 15.1 33 15.2 ICP .35 15.3 ICP .36 16 (Cr) .37 16.1 37 16.2 ICP .38 17 (AI) 39 17.1 39 17.2 ICP .4
4、0 18 (Fe) 41 18.1 41 18.2 ICP .42 A 44 A.1 .44 KS I 3203:2007 (2012 ) Testing methods for determination of metallic elements in highly purified water 1 (, , , , , , , , , , , , ) . . 2 . . ( ) . KS A 0001, KS A 2110, KS D 2302, KS D 2318, KS D 2352, KS L 2300, KS L 2303, KS L 2317, KS M 0001, KS M 0
5、016, KS M 0028, KS M 0035, KS M 0076, KS M 0100, KS M 0111, KS M 0124, ( ) KS M 0126, ( ) KS M 1001, KS M 1002, KS M 1003, KS M 1004, KS M 1005, KS M 1006, KS M 1007, KS I 3203:2007 KS M 1008, KS M 1122, () KS M 1131, KS M 8005, KS M 8234, (II)() KS M 8337, (12)() KS M 8355, KS M 8356, KS M 9900, KS
6、 M ISO 63532, 2:1 KS M ISO 63533, 2:2 3 3.1 KS M 0001 . 3.2 ( ICP .) KS M 0028 . 3.3 ( .) KS M 0016 . 3.4 KS M 0035 . 3.5 KS M 0100, KS M 0111, KS M 0124 KS M 0126 . ICP . 3.6 , ICP , ICP ( g/L ng/L) . 3.7 . 1)1) (%) 100 x : x :2 KS I 3203:2007 3.8 KS M 0076 A1A3 , . 3.9 . a) , . b) g/L( .) mol/L( m
7、mol/L) . , mg/mL, g/mL ng/mL . c) (, .) . , (100 g/L) 100 g/L . d) (a:b) . a mL b mL , KS M 0001 , . , . e) (IUPAC) KS . f) . 3.10 KS L 2303 KS L 2317 . , . ( 1) . 2 ) . 3.11 ( , lCP , lCP , ) 4 6 , . . , ICP , ICP . 3.12 KS M 9900 3 ( ) . 3.13 2 . 2) KS A 2110 A 1 .3 KS I 3203:2007 . , . . . 4 . 4.
8、1 , , , . 4.2 a) (0.2 mo1/L)KS M ISO 63532 ( KS M 8355 ) A1 . 16 A1 . b) 1/4 A1 30 . 5 . c) A3 ( ) 16 . d) c) . 4.3 a) 3 ) A1 ( .) . 4)b) 4.2 b) . c) , 5 , 1 L (1:1)(KS M 8355 A3 .) 1 mL 5 ) . 5 (Na) , ICP . 5.1 589.0 nm . 3) .4) 5 . 1 L/min .5) , , (1:1) .4 KS I 3203:2007 :Na 550 ng/L, 6) : 1030 %
9、6)5.1.1 . a) A 3 ( ). . A3 10 ng/L . b) (1:1) KS M 8355 . c) (100 g Na/mL) KS M 8005 600 1 . 0.254 g (1 000 mL) . . d) (1 g Na/mL) (100 g Na/mL) 10 mL (1 000 mL) . . e) (10 ng Na/mL) (1 g Na/mL) 5 mL (500 mL) . . 5.1.2 . a) 1 L . b) c) d) e) KS M 1122 2 7)f) KS L 2300 2050 L 5.1.3 . a) (0.1 g .) (1:
10、1) 0.5 mL 8),9) 500 mL . 10)b) 7580 10 mL . c) 0.1 g , . = (mL) . (mL) KS M 9900 3 ( ) 6) 5.1.3 1/50 . , .7) KS M 1131 2 .8) 5) .9) 1 L (1:1) 1 mL .10) . . 5 KS I 3203:2007 . *) . 2*) (500 mL) (1:1) 3*), 4*)0.5 mL 200 mL , 50 mL 300 mL 10 mL . 5.1.3 c) . 5.1.4 . a) , 5.1.3 ( 50 L) , , , 11 ) 589.0 n
11、m 12) . 13)b) a) 12) , . c) (ng Na/L) (ng Na/L) . (10 ng Na/mL) 2.525 mL (100 mL) . a) . a) , (ng Na/L) . . 1 5.1.3 ( 50 L) , . 10 , . 2 50 ng/L 5.1.3 500 mL 10 mL . 5.2 ICP / . :Na 505 000 ng/L, 14) : 5 20 % 14) 5.2.1 . *) 10) . 2*) , . 3*) 5) . 4*) 9) .11) , , . .12) 13) a) 3 .14) , .6 KS I 3203:2
12、007 a) 5.1.1 a) . b) KS M 8355 c) (50 ng Na/mL) 5.1.1 d) (1 g Na/mL) 10 mL (200 mL) . . d) (50 ng Na, 20 ng Mg, 10 ng Cu, 20 ng Zn, 5 ng Pb, 5 ng Cd, 10 ng Ni, 10 ng Co, 10 ng Mn, 10 ng Cr, 50 ng Ai)/mL 5.1.1 d) (1 g Na/mL) 50 mL, 8.1.1 c) (1 g Mg/mL) 20 mL, 9.1.1 c) (1 g Cu/mL) 10 mL, 10.1.1 c) (1
13、g Zn/mL) 20 mL, 11.1.1 c) (1 g Pb/mL) 5 mL, 12.1.1 c) (1 g Cd/mL) 5 mL, 13.1.1 c) (1 g Ni/mL) 10 mL, 14.1.1 c) (1 g Co/mL) 10 mL, 15.1.1 c) (1 g Mn/mL) 10 mL, 16.1.1 c) (1 g Cr/mL) 10 mL, 17.1.1 c) (1 g A1/mL) 50 mL (1 000 mL) 1 mL . . 5.2.2 . a) ICP 1 . 2 . 1 . , . 5.2.3 . a) ICP / 15) . b) a) . 16
14、) 15) . c) (ng Na/L) , (ng Na/L) . (50 ng Na/mL) 0.110 mL 17 ) (100 mL) . a) . a) , (ng Na/L) . . 5.1.3 . 15) / 16) . 5.1.3 5 10 , a) . , , 2 . ( 0) .17) , , , , , , , , , (50 ng Na, 20 ng Mg, 10 ng Cu, 20 ng Zn, 5 ng Pb, 5 ng Cd, 10 ng Ni, 10 ng Co, 10 ng Mn, 10 ng Cr, 50 ng Al)/mL .7 KS I 3203:200
15、7 5.3 . :Na 501 000 ng/L, 18) : 5 20 % 18)5.3.1 . a) KS M 0076 A2 A3 . . . b) 19 ) 22) . c) 20 ) . 22) . d) (5 ng Na/mL) 5.1.1 e) (10 ng Na/mL) 50 mL (100 mL) . . e) (5 ng Na, 10 ng K)/mL 5.1.1 d) (1 g Na/mL) 5 mL 6.1.1 c) (1 g K/mL) 10 mL (1 000 mL) . . 5.3.2 . a) . 1) 1 5 mL/min . 2) 21) . b) , ,
16、, . 18) , .19) . . (20 mmol/L) 96.1 g( 64.9 mL) 1 L . 20 mL 1 L . (5 mmol/L) (0.5 mol/L)(KS M 8355 43 mL 1 L .) 10 mL 1 L . 2,62 (1 mmol/L (5 mmol/L) 2,62 0.167 g KS M 8359 L() 0.750 g 1 L .20) . . (40 mmol/L) (5) 7.25 g 1 L . (50 mmol/L) (1 mol/L)( 60 mL KS M ISO 63532 80 g . 25 mL 500 mL .) 50 mL , 1 L .21) , .8 KS I 3203:2007 1) 21) ( ) . 22)2) . . 3) c) KS M 0035 5.2 f) () . 5.3.3 . a) 19) ( 1 2 mL/min) . 20) . b) ( 4050 mL ) 23) a) . c) 24) . d) (ng Na) ( g Na/L) . (5 ng Na/mL) 25)1 20 mL (100 mL) . a)c) , 24) . a)c) (ng Na) . . 1 ( , ) , 10 . 2 22) . 10 22) . 6 (K)