KS I ISO 8518-2006 Workplace air-Determination of particulate lead and lead compounds(Flame electrothermal atomic absorption spectrometric method)《车间空气 铅颗粒及铅化合物的测定 火焰原子吸收光谱法》.pdf

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KS I ISO 8518-2006 Workplace air-Determination of particulate lead and lead compounds(Flame electrothermal atomic absorption spectrometric method)《车间空气 铅颗粒及铅化合物的测定 火焰原子吸收光谱法》.pdf_第1页
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KS I ISO 8518-2006 Workplace air-Determination of particulate lead and lead compounds(Flame electrothermal atomic absorption spectrometric method)《车间空气 铅颗粒及铅化合物的测定 火焰原子吸收光谱法》.pdf_第3页
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1、 KSKSKSKS SKSKSKS KSKSKS SKSKS KSKS SKS KS 2006 10 30 http:/www.kats.go.krKS I ISO 8518 ( ) KS I ISO 8518: 2006 (2011 ) I ISO 8518: 2006 : ( ) ( ) KIST ( ) : (http:/www.standard.go.kr) : :1996 1 5 :2006 10 30 :2011 12 26 2011-0622 : : ( 02- 509-7270) (http:/www.kats.go.kr). 10 5 , . ICS 13.040.30 KS

2、 ( ) I ISO 8518: 2006(2011 ) Workplace air Determination of particulate lead and lead compounds (Flame electrothermal atomic absorption spectrometric method) 2005 2 ISO 8518 Workplace air Determination of particulate lead and lead compounds(Flame electrothermal atomic absorption spectrometric method

3、) . 1. . 10 200 g . (6.1 ) . . (8.2.2) (4. ) . . (10.2 ) (EDTA) . 2. . . KS L 2302 KS L 2316 KS L 2317 KS L 2512 KS M 0012 KS M 0016 KS M 0129 ( ) KS M 9404 ISO 8655 1 Piston operated volumetric apparatus Part 1: Terminology general requirements and user recomm endations ISO 8655 2 Piston operated v

4、olumetric apparatus Part 2: Piston pipettes ISO 8655 5 Piston operated volumetric apparatus Part 5: Dispensers ISO 8655 6 Piston operated volumetric apparatus Part 6: Gravimetric methods for the determination of measurement error I ISO 8518: 2006 2 3. . . . 283.3 nm , . 4. 8.2.2 (Pb2+) . . (10.1 ) .

5、 5. (5.1) . 5.1 2 ( 0.1 mS/m 25 0.01 M m ) , 0.01 g/mL . 5.2 1.42 g/mL, 69 %(m/m) 71 %(m/m) 0.01 g/mL . 5.3 1: 9 . (5.1) 800 mL (5.2) 100 mL , 1 L . 5.4 1 000 mg 1 000 mg/L . . . a) 110 Pb(NO3)2 (1.5980.001) g (5.3) 1 000 mL 6.2.1 e) (5.3) . b) (5.1) 100 mL (5.2) 100 mL 1: 1 200 mL (1.0000.001) g ,

6、1 000 mL 6.2.1 e) , (5.1) . a) b) (6.2.2) 1 . 5.5 30 %(m/m) 0.01 g/mL . 5.6 5.7 . 6. 6.1 6.1.1 8.2.2 0.3 m (KS M 9404 ) 99.5 % . 0.1 g . 0.8 m 1.2 m . ( ) 99 % . . 6.1.2 KS M 9404 , I ISO 8518: 2006 3 . 1. , . 2. . , 82/605/ CEE(2)( ) . 6.1.3 (7.1.2 ) 5 % (7.1.1 ) , . . . 6.1.4 , 5 % (7.1.1 ) , 1 ,

7、. 1. , (7.2.2) 1 , . . 2. 1 . 3. , (7.1.3 ) . 6.1.5 . 6.1.6 6.1.7 1 0 50 6.2 . 6.2.1 KS L 2302 . (8.1.4) . a) 50 150 mL b) a) . c) KS L 2317 . d) 100 mL e) KS L 2317 10 1 000 mL 6.2.2 100 mL 1 L 6.2.3 ISO 8655 1 ISO 8655 6 . (8.3.2 ) (8.5.4 ) (8.2.2 8.2.3 ) 6.2.4 , 150 . . . 6.2.5 I ISO 8518: 2006 4

8、 . 6.2.6 0.1 mg . 7. 7.1 7.1.1 KS M 9404 , (6.1.2) . 2 L/ . , , 82/605/CEE(2)( ) . 7.1.2 . , . (7.1.1 ) , (9.3.1 ) 10 g . , 0.03 mg/m3 2 L/ 3 . 7.1.3 a) . , . 5 % . (6.1.4 ) , (7.2.3 7.3.5 ) . 1. . 2. , 9.1.1 . b) . , (7.2.3 7.3.5 ) 9.1.2 . 7.1.4 ( ). 7.2 . 7.2.1 (6.2.1) , . 7.2.2 (7.2.1 ) (5.1.1) .

9、 , . . 7.2.3 (6.1.5) (7.2.2 ) (6.1.3) I ISO 8518: 2006 5 . , (6.1.4) 5 % (7.1.1 ) , . (7.1.3 ) . (6.1.3 ), 15 . . 1 . , . 7.3 7.3.1 , . . . 7.3.2 , . . 7.3.3 , 5 % . ( ) ( 1 ) . . . 7.3.4 7.3.3 . 7.3.5 (7.1.2 ) (6.1.4) 5 % , . (7.1.3 ) . , . 7.3.6 (11. ) . . (7.1.3 ) . , . 7.3.7 10 2 . . . 7.4 . . 8

10、. 8.1 8.1.1 . 1 . 8.1.2 (8.1.1 ) . (5.2) 1/3I ISO 8518: 2006 6 , (6.2.4) 140 (5.1) . 8.1.3 (8.1.1 ) (5.3) (5.1) . 8.1.4 8.1.1, 8.1.2 8.1.3 (5.3) (5.1) . 8.1.5 (5.3) (5.1) . 8.2 8.2.1 , 6.2.1 a) (7.3.7 ) . (6.1.2 1. ) , (5.1) . 8.2.2 (5.2) 3 mL , ( 1. ) (5.5) 1 mL 6.2.1 b) 140 ( 2. ) . 2 , 3 mL 1 mL

11、. 140 ( 3. ) . . , (5.3) 3 5 mL . 140 . 1. (5.5) . 2. . 140 . 3. . , . . 8.2.3 (5.2) 1 mL . 8.2.4 10 mL (6.2.1 e) (5.1) . , (5.3) ( ) (6.1.1) . 8.3 8.3.1 (5.3) . 8.3.2 (5.3) (5.4) “0” 6 . 283.3 nm (8.4.1 ) 0 g/mL 20 g/mL . . , . 8.4.1 . I ISO 8518: 2006 7 8.3.3 1 (6.2.2) . 8.4 8.4.1 . (8.5.1 ) (8.5.

12、4 ) 283.3 nm . 217.0 nm , , 217.0 nm . 283.3 nm 217.0 nm . , 283.3 nm . 283.3 nm , 217.0 nm 283.3 nm . 8.4.2 (8.4.1 ) , , . 8.4.3 (8.3.1 ) 0 . (8.3.2 ) . . 8.4.4 . . , . 20 % 20 % 70 % . , 8.3.2 . 8.5 8.5.1 (8.3.1 ) 0 . (8.3.4 ) , . (8.4.4 ) , . (8.4.4 ) . . 8.5.2 (8.3.1 ) , 5 10 . 0 . 5 % . , 8.4.3

13、 8.4.4 , . I ISO 8518: 2006 8 8.5.3 , . 8.5.4 . (5.3) , DF . . , 8.3.2 . 8.5.5 , . 8.6 8.6.1 , 8.6.2 8.6.3 . 8.6.2 (5.3) (5.4) 0.25 g/mL . 8.6.3 (8.6.2) 20 . k , k) 2 , 3 , k 2 . 9. 9.1 9.1.1 (Pb) . VVDFV )Pb()Pb()Pb(0011= (Pb)0: (8.5.5 ) (g/mL) (Pb)1: (g/mL) V: (L) V0: . 10 mL(8.2.4 ) V1: . 10 mL(8.2.4 ) DF: 8.5.4 (DF 1) 7.1.3 a)

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