1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS M 1710 (FREON 113) (FREON 114) KS M 1710:2008 2008 12 19 http:/www.kats.go.krKS M 1710:2008 : ( ) ( ) ()MPT ( ) : (http:/www.standard.go.kr) : : 1983 11 30 : 2008 12 19 2008-0927 : : ( 025097301) (http:/www.kats.go.kr). 10 5 , . KS M 1710:2008 (FREON 113)
2、 (FREON 114) Fluoroethanes Trichlorotrifluoroethane(FREON 113) dichlorotetrafluoroethane(FREON 114) 1 ( , .) . 2 . . ( ) . KS M 0001, KS M 0010, KS M 0013, KS M 0031, KS M 8001, 3 1 . 1 113 114 4 5. 2 . KS M 1710:2008 2 2 113 114 . . . . % 99.5 99.5 0.01 0.01 (HCl ) % 0.000 1 0.000 1 % 0.002 0.002 .
3、 113 114 45.57 3.55 ( )(20 ) g/mL 1.577 1.471 5 5.1 KS M 0001 , KS M 0031 . 5.2 15 mm 10 mL , . 5.3 5.2 . 5.4 5.4.1 . 5.4.2 . KS M 1710:2008 3 a) 113 114 b) 99.0 % 5.4.3 a) b) 1) 105 297 m(145 48 ) Chromosorb W . 2) Silicone DC 200 . 3) 30 35 % c) 36 mm, 3 m , . d) 10 25 L . 5.4.4 , . 3 . 3 113 114
4、3 mm, 3 m 3 mm, 4 m 2.9 g 6.9 g 70 50 110 100 80 50 Ma 130 130 ( ) mL/min(kPa) 20(78) 13(88) L 7( ) 7( ) mm/mim 10 10 Chromosorb W(105 2 97 m) Silicone DC 200 . 5.4.5 5.4.4 1 2 . KS M 1710:2008 4 1 113 2 114 5.4.6 a) KS M 0031 . b) KS M 0031 . 5.5 5.5.1 . 113 114 112 0 5 10 15 20 25 (min) 1 mV 1 024
5、 mV 1 mV 114 1130 5 10 15 20 25 (min) 1 mV 1 024 mV 1 mV 115 KS M 1710:2008 5 5.5.2 a) 3 . 3 b) c) (1052) . 5.5.3 ( ) . 5.5.4 (1052) 30 , . 0.1 mg . 800 g , . 1.5 2.0 ( 90 ). 10 mL 90 . (1052) 30 , 0.1 mg . 5.5.5 . ( 800 mL)500 mL ( 15 g) KS M 1710:2008 6 10001=SmmR R : (%) m0: (g) m1: (g) S : (g) 5
6、.6 5.6.1 113 113 . a) , . b) 1) 300 mL . 2) 500 mL . c) 1) (0.1 w/v %) KS M 8001 . 2) 0.01 mol/L KS M 8001 (0.1 mol/L) 10 d) 100 mL 100 g . . . 3 . (0.1 w/v %) 23 , (0.01 mol/L) D(mL) . , 0.01 mol/L E(mL) . e) (HCl ) . 100365000.0)(=SEDO O : (HCl )(%) D : (0.01mol/L) (mL) E : (0.01mol/L) (mL) S : (g
7、) 5.6.2 114 114 . a) . b) 1) 4 KS M 1710:2008 7 : mm 4 5 2) 5 3) 500 mL . 4) 5.6.1 c) . c) 4 100 mL , 4 . d) 100 g . , , . (0.1 w/v %) 2 3 (0.01 mol/L) , D(mL) . , 0.01 mol/L E(mL) . e) 5.6.1 e) . 5.7 5.7.1 . 5.7.2 a) KS M 0010 . 68 41 114 20 65 50 100 68 155 14 65100 6 30 3 1.5 10 . KS M 1710:2008
8、8 b) 1) 6 . 2) 7 . : mm a) ( 2.94 MPa ) c) ( 200 mm, 0.5 mm) 6 7 80 mL 20 mL b) 4 27.2KS M 1710:2008 9 c) 1) KS M 0010 4.3.3 (6) 2) KS M 0010 4.3.3 (7) f 1 mg H2O/mL d) 1) 113 , . 114 , . , . , 80 % . . 2) , . 113 100 mL, 114 200 mL . e) . 100 g . 113 , 114 510 g/min . . f) . 100103=SfCH H : (%) C :
9、 (mL) f : 1 mL mg S : (g) 5.7.3 a) KS M 0013 . b) 1) 6 . 2) 8 . KS M 1710:2008 10 8 c) 1) KS M 0013 . 2) KS M 0013 . d) 1) 5.7.2 d) 1) . 2) 5 mL . . 113 100 mL, 114 200 mL . e) 5.7.2 e) . (C) (g) . f) . (C) , 10072.10103=SFQH (g) , 100106=SGH H : (%) Q : (C) (A) (s) G : (g) ( ) KS M 1710:2008 11 S :
10、 (g) F : 6 . a) b) c) d) (FREON 113) (FREON 114) 135513 7017 (02)60094114 (02)600948878 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS M 1710:2008KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Fluoroethanes Trichlorotrifluoroethane(FREON 113)dichlorotetrafluoroethane(FREON 114) ICS 71.100.20