1、 KSKSKSKS KSKSKSK KSKSKS KSKSK KSKS KSK KS KS M 6539 KS M 6539:2008 2008 5 28 http:/www.kats.go.krKS M 6539:2008 : ( ) ( ) () () () ( ) : (http:/www.standard.go.kr) : :1968 12 10 :2008 5 28 20080239 : : ( 025097301) (http:/www.kats.go.kr). 10 5 , . KS M 6539:2008 i 1 1 2 1 3 .2 4 ( )2 4.1 .2 4.2 .2
2、4.3 2 4.4 3 4.5 3 5 ( ) 3 5.1 .3 5.2 3 5.3 6 5.4 7 6 ( ) 7 6.1 .8 6.2 8 6.3 8 6.4 9 7 ( )9 7.1 .9 7.2 ( ).9 7.3 ( )10 7.4 11 8 ( ).11 8.1 .11 8.2 A 11 8.3 B 14 8.4 16 9 ( ).17 9.1 .17 9.2 .17 9.3 .17 9.4 17 9.5 .17 9.6 18 9.7 18 10 80 ( )18 10.1 .18 10.2 18 10.3 18 10.4 18 11 ( ) 20 11.1 .20 KS M 65
3、39:2008 ii 11.2 20 11.3 20 11.4 20 11.5 20 11.6 21 12 ( ) .21 12.1 .21 12.2 .21 12.3 .21 12.4 22 12.5 .23 12.6 24 12.7 .24 12.8 .25 12.9 26 12.10 26 A( ) 27 B( ) .29 .32 KS M 6539:2008 Rubber compounding ingredients Sulfur Methods of test . . . 1 , . . , ISO/IEC Guide 21 IDT( ), MOD( ), NEQ( ) . ISO
4、 8332: 2006, Rubber compounding ingredients Sulfur Methods of test(IDT) A . 2 . . ( ) . KS A 5101 1, 1: KS L 2317, KS M 0001, KS M 2160, KS M 6634, KS M 8088, ( ) KS M 8113, ( )( ) KS M 8221, N- ( ) KS M 8238, ( ) KS M 8241, ( ) KS M 8250, ( ) KS M 8460, ( ) KS M ISO 2590, KS M ISO 3425, ( ) 850 900
5、 200 KS M ISO 3426, ( ) 80 KS M ISO 3704, ( ) KS M ISO 3705, ( ) KS M ISO 6353 1, 1: 1 KS M 6539:2008 2 KS M ISO 6353 2, 2: 2 ISO 4793: 1980, Laboratory sintered(fritted) filter Porosity grading, classification and designation 3 KS M 6634 6. , . 4 ( ) . 4.1 , . 4.2 KS M 0001 8.3( ) . a) 50 g/dm3 , K
6、S M 8113 50 g 1 dm3 . b) 0.05 mol/dm3 , KS M ISO 6353 3 . . c) 0.1 mol/dm3 , KS M ISO 6353 2 . . d) 40 Vol % KS M ISO 6353 3 . e) KS M ISO 6353 2 . f) ( ) 20 g/dm3 g) KS M ISO 6353 3 . 4.3 . a) 0.2 g(m1) 0.1 mg . 4.2(f) 1 cm3 . 50 cm3 4.2(a) 200 cm3 . , . 130 . 1 . . , , 25 100 cm3 . b) 200 cm3 ( 0.
7、05 mol/dm3)4.2(b) 30 cm3 4.2(e) 10 cm3 . c) 100 cm3 a) 100 cm3 10 cm3 10 cm3 4.2(d) 2 cm3 2 5 b) . . KS M 6539:2008 3 4.2(g) 1 cm3 0.1 mol/dm3 4.2(c) . V3 . d) . V2 . 4.4 (%) (1) (%) . 1322.3)(mfVVS= (1) S : (%) V2: 4.3(d) 0.1 mol/dm3 4.2(c) (cm3) V3: 4.3(a) 0.1 mol/dm3 4.2(c) (cm3) m1: (g)4.3(a) f
8、: 0.1 mol/dm3 4.2(c) 4.5 . a) b) c) d) e) 5 ( ) 5.1 . . a) b) . 5.2 A B . 5.2.1 A 5.2.1.1 . KS M 6539:2008 4 a) 200 mm ( 1 ) . 25 mm 5.2.1.1(b) . . . 200 kPa . . . . . b) 2 KS A 5101 1 180 m 125 m c) 7 mm . 1 5.2.1.2 5.2.1.1(b) . 3 . . (802) 0.1 mg . 25 g(m2) 0.1 g 300 cm3 , 5.2.1.1(a) . 1 ( 20 g/dm
9、3 ) . . . . . 2 . KS M 6539:2008 5 . . . . ( 34 .) . 5.2.1.1(c) . . . (802) 30 0.1 mg . (m3) . 5.2.1.3 (%) (%) . 10023mm (2) m2: (g) m3: (g) 5.2.2 B 5.2.2.1 . a) KS A 5101 1 180 m 125 m . b) c) 25 mm . 5.2.2.2 . 5.2.2.1(a) (802) 5.2.2.1(b) , 15 1 mg . 100 m 10 g(m4), 100 m 30 g(m4) 0.1 g 20 g/dm3 .
10、100 cm3 . 10 15 mm 5.2.2.1(c) . KS M 6539:2008 6 . (802) 30 . 0.1 mg (m5) . 5.2.2.3 (%) (3) , (%) . 10045mm (3) m4: (g) m5: (g) 5.3 5.3.1 . a) 200 mm KS A 5101 1 180 m, 125 m 63 m 3 . . b) a) , . c) 25 mm . d) 10 cm3 2 , 100 cm3 1 . e) A4 f) 5.3.2 3 5.3.1(a) 5.3.1(c) , . (180 m) , (125 m), (63 m) 3
11、. . KS M 6634 6. , . 50 g 100 cm3 5.3.1(d) 1 mg . . , (m6) . , ( 1 mg .) 5.3.1(b) 3 Hz(1 3 ) 5 . KS M 6539:2008 7 3 Hz, 150 mm 5 . 1 5.3.1(f) . , 180 m . 5.3.1(c) . (150 m) . 5 . . 1 mg . 10 cm3 180 m 125 m , 100 cm3 63 m . 5.3.1(e) . , . 1 mg (m7, m8 m9) . 5.3.3 180 m (%) (4) , (%) . 10067mm (4) 18
12、0 m 125 m (%) (5) , (%) . 100687+mmm (5) 3 (%) (6) (%) . 1006987+mmmm (6) m6 : (g) m7: 180 m (g) m8: 125 m (g) m9: 63 m (g) 5.4 . a) (A B ) b) c) (%) d) e) 6 ( ) KS M 6539:2008 8 6.1 . . a) b) 6.2 6.2.1 KS M 8221 . 6.2.2 10 g(m10) 1 mg 250 cm3 (6.2.1) 100 cm3 . 30 5 . 100 cm3 75 cm3 , 50 cm3 100 cm3
13、 . 50 cm3 . . 2 cm3 . . , . 1 mg 50 cm3 (m11) . 2 50 cm3 . , 80 1 . , 1 mg (m12). 6.2.3 (%) (7) (%) . 20.0100)(2101112mmm (7) m10: (g) m11: (g) m12: (g) 0.20 : 6.3 6.3.1 KS M 8088 ( ) 60 g 4 cm3 (6.2.1) , 24 . . 6.3.2 KS M 6539:2008 9 . a) (50.01) g(m13) 1 mg , 250 cm3 , (6.3.1) 25 cm3 . . b) 10 1 m
14、g (Porosity) P40(ISO 4793) , 100 cm3 . 2 25 cm3 (KS M 8101) . c) 80 1 1 mg (m15) 6.3.3 (%) (8) (%) . 10013151413+mmmm (8) m13: (g) m14: (g) m15: (g) 6.4 . a) ( ) b) c) d) e) 7 ( ) 7.1 . . . a) ( ) b) ( ) . 7.2 ( ) 7.2.1 KS M 8153 . KS M 6539:2008 10 7.2.2 2 g(m16) 1 mg 400 cm3 (7.2.1) 200 cm3 . 30 . 1 mg (Porosity) P40(ISO 4793) (m17) . 20 cm3 3 . 80 1 . 1 mg (m18). 1 . 2 . 7.2.3 (9) , (%) . 100161718mmm