1、 KS M 6558KSKSKSKSSKSKSKS KSKSKS SKSKS KSKS SKS KS KS M 6558:2008 2008 8 4 http:/www.kats.go.krKS M 6558:2008 : ( ) ( ) () () ( ) : (http:/www.standard.go.kr) : :1970 12 28 :2008 8 4 20080403 : : ( 02-509-7301) (http:/ www.kats.go.kr). 10 5 , . KS M 6558:2008 Testing methods of carbon black for rubb
2、er 1 . 2 . . ( ) . KS A 5101 1, 1: KS M 3302, (D.B.P) KS M 6782, 3 . a) b) c) d) DBP e) f) g) pH h) i) 4 4.1 . 4.2 4.2.1 2 2 L 20 L 5 . KS M 6558:2008 2 4.2.2 , . 4.3 20 1 . 5 5.1 . . 5.2 5.2.1 ( 1 2) 5.2.2 0.01 g 5.2.3 5.2.4 5.2.5 ( 45 m , 180 m, 250 m 500 m ) 5.3 5.3.1 45 m 0.140.34 MPa 3 , . 5.3.
3、2 100 g 0.01 g 0.140.34 MPa . 5.3.3 . KS M 6558:2008 3 : cm 1 BB CC 5.08 AA20.0 BBCCKS M 6558:2008 4 : cm 2 5.3.4 ( ) 35 . 5.3.5 (1251) 1 . 5.4 . 20.32 6.354.764.552.221.27 0.635 0.15 0.15 5.39 5.23 1.248 0.79 2.54 20 5.395.236.355.08 0.873 0.317 0.0791.27 4.124.28 4.28302.54 16 4.12 4.76 1.27 3.44
4、0.635 6.35 11.64 5.5 23.75 15.24 0.635 0.9573.81 73.81 1.2820.95 0.950.951.9052.54 1.9 2.54 0.950.951.27 1.27 1.158 0.95 7.7781.7271.580.950.962.54 11.738 6.474 1.2712.7 35.05 5.3 17.781 KS M 6558:2008 5 100=SWR R : (%) W : (g) S : (g) 6 6.1 . 6.2 6.2.1 1 7251 750 rpm , 140160 , 280300 , . 6.2.2 KS
5、A 5101 1 125 m 3 3 . 200 mm , 25 mm . 6.2.3 5 6.2.4 6.2.5 6.2.6 6.2.7 0.1 g 6.3 6.3.1 . , 150 m , , , , 125 m 3 , . 6.3.2 3.8 L 2228 g 0.1 g , (125 m) . 6.3.3 5 0.1 g . 6.4 0.1 % 3 . KS M 6558:2008 6 100=SWF F : (%) W : (g) S : (g) 7 7.1 ( ) . 7.2 7.2.1 7.2.2 ( ) 7.2.3 7.2.4 7.3 7.3.1 (1251) 30 , 0.
6、1 mg . 7.3.2 (20.002) g (1251) 1 , 0.1 mg 3 . . 100=SLSH H: (%) S: (g) L: (g) 7.3.3 . a) (50.05) g 100 V, 185 W (752) mm . 1 ( ) 0.1 % 2 . b) (50.05) g 100 V, 250 W KS M 6558:2008 7 (752) mm . 1 ( ) 0.1 % 2 . 8 DBP 8.1 DBP(dibutyl phthalate) . 8.2 8.2.1 6.8 kg 8.2.2 8.3 KS M 3302 8.4 8.4.1 KS A 5101
7、 1 2.00 mm 500 m . 8.4.2 (1251) 1 . 8.4.3 0.01 g . 15 g, SRF (N 765, N 785 ) 25 g, 20 g 8.4.4 a) 2 . b) . c) 0 . d) DBP . e) . f) . g) 5 . KS M 6558:2008 8 8.5 DBP 2 2 mL/100 g 2 4 . a) DBP (mL/100 g): 5 b) DBP (mL/100):320 9 9.1 . 9.2 9.2.1 30 mL . 9.2.2 9.2.3 (1251) . 9.2.4 0 . 9.2.5 0.1 mL 9.3 9.
8、3.1 (0.047 3 N) 57 g 30 mL , 6 g 1 000 mL . 9.3.2 (0.039 4 N) (Na2S2O35H2O) 9.781 0 g (1 000 mL) 500 mL nKS M 6558:2008 9 5 mL 1 000 mL . 9.3.3 2.5 g (HgI2) 2 mg 1 L 5 . 9.3.4 10 % 20 mg , (0.039 4 N) 20 mL 10 % 20 mL , 1015 . , . F . AFCF= C : (mL) F : A : (mL) 9.3.5 (0.047 3 N) . 9.4 9.4.1 (1251)
9、1 (0.50.000 5) g . . 9.4.2 25 mL , 1 , 1 , 3 . 9.4.3 20.0 mL (250 mL) , (0.039 4 N) , 2 mL . 9.4.4 9.4.3 . (mL) (240.1) mL . 9.5 2 . fNWVbsbI = 91.126 KS M 6558:2008 10 I : (mg/g) b : (mL) s : (mL) N : (0.047 3) W : V : (mL)(25 .) f : 10 10.1 . 10.2 10.2.1 (95020) . 10.2.2 20 mL 10.2.3 ( ) 10.2.4 (1
10、251) . 10.2.5 10.2.6 10.3 10.3.1 (95020) , , 6 mm 30 0.1 mg . 10.3.2 (1251) 1 . 10.3.3 2 mL , . 10.3.4 0.1 mg . KS M 6558:2008 11 10.3.5 (95020) 7 , 0.1 mg . 10.4 0.1 % 2 . 100=ABCBV V: (%) A: (g) B: (g) C: (g) 11 pH 11.1 pH 1 . 11.2 11.2.1 pH 11.2.2 11.2.3 11.2.4 11.3 11.3.1 . 11.3.2 1 g 10 mL . (
11、) . 11.3.3 1 g 15 . 11.3.4 . 11.3.5 pH . 11.4 pH 2 . KS M 6558:2008 12 11.5 a) . b) pH pH . c) . pH 6.97.1 . 12 12.1 . 12.2 12.2.1 (55025) . 12.2.2 12.2.3 12.2.4 12.2.5 (1251) . 12.3 12.3.1 (55025) 1 , 0.1 mg . 12.3.2 (1251) 1 . 12.3.3 2 g , (55025) 16 0.1 mg . 6 mm . 12.4 2 . 100=BCBDA A : (%) B :
12、(g) KS M 6558:2008 13 C : (g) D : (g) 13 13.1 . 13.2 , 10 mm (1251) 1 20 . 13.3 13.3.1 13.6 . 13.3.2 . a) ( ) ( ) 1 (RSS #1) 100.0 100.0 3.0 3.0 5.0 5.0 (MBTS) 0.6 1.0 2.5 3.0 50.0 50.0 (PBN) 1.0 161.1 163.0 b) (RSS #1) 100.0 3.0 0.6 2.5 5.0 111.1 111.1 50.0 161.1 13.4 (150155) mm(250280) mm (705) ,
13、 . 13.3.2 a) 13.3.2 b) 45 . KS M 6558:2008 14 13.4.1 a) 1.4 mm 3 . b) (0 ) 0.5 mm 2 . c) (2 ) 1.0 mm 2 . d) (4 ) , MBTS 2 . e) (6 ) 1.0 mm , 4 . f) (12 ) 1.0 mm 6 . 0.2 % . g) (14 ) 0.5 mm 6 . h) (16 ) 1.5 mm 2 , 30 ( 16 30 ). 3/4 . 13.4.2 a) 13.4.1 a)d) . b) 1.4 mm 3 . c) (0 ) 0.5 mm 6 . d) (2 ) 13
14、.4.1 e) . e) (8 ) 13.4.1 f) . f) (9 ) 13.4.1 g) . g) (12 ) 13.4.1 h) . ( 12 30 ) 13.5 13.5.1 3.45 MPa , 2.03.0 mm . (1452) 15 30 . , 1015 . 13.5.2 KS M 6782 , 300 % , 2 . 13.6 . KS M 6558:2008 15 99.50 % (100 ) 0.05 0.02 0.10 % 0.10 0.05 % ( ) 0.005 (150 m) (75 m) 510 % 65 2 (105 ) 0.5 % 0.1 195199
15、, 0.5 % 93 % (M) 0.50.75 % 0.5 0.7 % 2.0 165 (150 m) 99.9 % 92.0 0.5 % 0.5 0.000 4 % 0.000 5 % (45 m) 0.5 % 0.3 0.1 99.0 % 0.03 0.02 % DBP 102.1 mL/100 g 81.9 mg/g () 300 % 15 25.6 MPa 11.03.5 MPa 30 26.5 MPa 14.217.2 MPa * 13.5 . 135513 7017 (02)60094114 (02)600948878 http:/ KS M 6558:2008KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Testing methods of carbon black for rubber ICS 83.060 Korean Agency for Technology and Standards http:/www.kats.go.kr