KS M 8003-2006 General rules for test methods of highly purified reagents《高纯试剂试验方法通则》.pdf

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1、 KSKSKSKS KS M 8003SKSKSKS KSKSKS SKSKS KSKS SKS KS KS M 8003 : 2006 2006 11 10 M 8003: 2006 ( ) ( ) SK R&D center ( ) ( ) ( ) ( ) : : 1996 12 27 : 2006 11 10 2006 0647 : : ( ) ( 02 509 7299 7301) . 7 5 , . ICS 71.040.30 KS M 8003: 2006General rules for test methods of highly purified reagents 1. .

2、. 2. . . KS D 7041 KS D 7042 KS D 9008 KS L 2300 KS L 2302 KS M 0001 KS M 0012 KS M 0016 KS M 0028 KS M 0031 KS M 0035 KS M 0071 KS M 0072 (TOC) KS M 0073 KS M 0074 KS M 0075 KS M 0100 KS M 0111 KS M 0124 ( ) KS M 0126 ( ) KS M 0127 ( ) KS M 0129 ( ) KS M 8001 KS M 9900 KS M 9901 3. KS M 0012, KS M

3、0016, KS M 0028, KS M0031, M 8003: 2006 KS M 0035, KS M 0124, KS M 0126, KS M 0127 KS M 0129 . 3.1 , , , ( , , , ). 3.2 , . ( , ). 3.3 . , . 3.4 , . , . 3.5 3.6 3.7 , 3.8 , 3.9 ( ) 3.10 3.11 3.12 3.13 . 4. KS M 0001 . 5. 5.1 1 A1 A4 . A1 A3 , . 152 M 8003: 2006 1 A1 A2 A3 A4 (1)(mS/m)(25 ) 0.5 0.1(2

4、)(3) 0.1(2) 0.1(2) (TOC)(4)(mgC/L) 1 0.5 0.2 0.05 (5)(g Zn/L)0.5 0.5 0.1 0.1 (6)(g SiO2/L) 50 5.0 2.5 (7)(g Cl/L) 10 2 1 1 (7)(g SO24/L) 10 2 1 1 (mL)(8) 0.5 0.3 0.2 (1) KS M 0071 . (2) (3) 0.01 mS/m(25 ) . (4) KS M 0072 . (5) KS M 0073 . (6) KS M 0074 . (7) KS M 0075 . (8) 100 mL 5 mmol/L 30 5 mmol

5、/L (mL) A1 A4 . A1 A2 A4 . , . A2 A3 A4 . A1 , . A3 , . A1 A2 , . A4 (TOC), CODMn , . A1 A2 ( ) , . 5.2 KS . (9) , . (9) , , , , , , , , . 6. 6.1 KS L 2302 1 (10)(11)(12) . (10) , , , , . , . 3 M 8003: 2006 (11) . . (12) . 6.2 (11)(12) . 6.3 (13), (14), (15), (16) . (13) , . , , , , . , . (14) , . ,

6、 , , . . (15) , . , , . . (16) . . . 6.4 KS D 7041, KS D 7042 (17) KS D 9008 . (17) , , , , , , , . 6.5 (13) (14) . . 7. 7.1 (1: 1) . , , , . A1 A3 . 7.2 (1: 3) 0.5 . , , , (1: 3) 0.5 , 0.5 . A1 A3 . 7.3 (1: 3) 80 1 (18). A1 A3 . (18) , . 7.4 (19) , (1: 3) 0.5 , , (1: 1) , A1 A3 . (19) . 7.5 (20) .

7、4 M 8003: 2006 (20) . . . . 7.6 (20) . 8. 8.1 KS M 9900 , 0.5 m 350 000 /m3 (21) , . 15 (21) KS M 9900 7 . 8.2 KS M 9901 (22) . 15 (22) V . 9. 9.1 , , , . . 1. . , (30 50 mL) . 2. 8.2 . 9.2 . , , . . 9.2.1 (23) . . a) . b) . c) 10 mL (24) . d) , pH 2 (25). e) . f) . (23) KS M 8001 5.3 . KS . (24) 10

8、0 mL 1 000 mL . (25) 1 000 mL (1: 1) 3 mL . 1. . 2. , . 3. a) f) . 5 M 8003: 2006 4. . . 9.2.2 (26). . 9.2.1 . (26) , . . . 2 . . 2 A A1, Ca, Mg B Cd, Co, Cr, Cu, Fe, Mn, Mo, Ni, Pb, Zn, VC As, Ge, P, Se, Si 9.3 , . 1. . 2. . 3. . . 10. . KS M 8001 6. . 10.1 KS M 0012 . 10.2 KS M 0016 . 10.2.1 a) .

9、b) c) d) KS L 2300 . (27) (27) . 8.1 . 10.2.2 . a) b) c) d) 6 M 8003: 2006 e) f) g) h) i) j) k) , 10.2.3 . a) . b) 10.2.1 d) , . c) b) . d) KS M 0016 8.1 a) b) . 10.2.4 . . . 10.3 KS M 0028 . 10.3.1 . a) b) (27) 10.3.2 . a) b) c) d) e) f) g) h) i) j) k) 10.3.3 . a) (28). b) (29). 7 M 8003: 2006 c) ,

10、 , . d) c) . e) KS M 0028 9.2.1 . (28) . . (29) (1: 10) . , (1: 3) 0.5 , (1: 3) 2 A1 A2 . 10.3.4 . . A1 A2 , . 10.4 10.4.1 . a) b) (27) 10.4.2 . a) b) c) d) e) f) g) h) (30) (30) 1 . (dwell) . 10.4.3 . a) , (31). b) (29)(32). c) , (33) , (34) . d) c) . e) KS M 0028 9.2.1 . (31) . . . (32) (27) (1: 2

11、0) A1 A2 . 8 M 8003: 2006 (33) 1 . . (34) , . , , . 10.4.4 10.3.4 . 10.5 KS M 0035 . 10.5.1 . a) (35). , . b) (36). , . (35) (4 mmol/L) (4 mmol/L) (36) (15 mmol/L) 10.5.2 . a) b) . 10.5.3 (37). a) b) c) , d) , e) (38) f) (37) b), d) . (38) . , . 10.5.4 . a) (39) (40) , (41) . b) , . c) . d) b), c) . e) . (39) . (40) 1 3 mL/min (41) , 9 M 8003: 2006 . 1.

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